Literature DB >> 28613325

Elucidation of the elusive structure and formula of the active pharmaceutical ingredient bismuth subgallate by continuous rotation electron diffraction.

Yunchen Wang1, Sofia Takki1, Ocean Cheung2, Hongyi Xu1, Wei Wan1, Lars Öhrström3, A Ken Inge1.   

Abstract

Bismuth subgallate has been used in wound and gastrointestinal therapy for over a century. The combination of continuous rotation electron diffraction and sample cooling finally revealed its structure as a coordination polymer. The structure provides insight regarding its formula, poor solubility, acid resistance and previously unreported gas sorption properties.

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Year:  2017        PMID： 28613325     DOI： 10.1039/c7cc03180g

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  15 in total

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2.  Atomic-resolution structures from polycrystalline covalent organic frameworks with enhanced cryo-cRED.

Authors:  Jian Li; Cong Lin; Tianqiong Ma; Junliang Sun
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3.  An Expandable Hydrogen-Bonded Organic Framework Characterized by Three-Dimensional Electron Diffraction.

Authors:  Peng Cui; Erik Svensson Grape; Peter R Spackman; Yue Wu; Rob Clowes; Graeme M Day; A Ken Inge; Marc A Little; Andrew I Cooper
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4.  Metal-Organic Frameworks with Hexakis(4-carboxyphenyl)benzene: Extensions to Reticular Chemistry and Introducing Foldable Nets.

Authors:  Francoise M Amombo Noa; Erik Svensson Grape; Steffen M Brülls; Ocean Cheung; Per Malmberg; A Ken Inge; Christine J McKenzie; Jerker Mårtensson; Lars Öhrström
Journal:  J Am Chem Soc       Date:  2020-05-05       Impact factor: 15.419

5.  High-throughput continuous rotation electron diffraction data acquisition via software automation.

Authors:  Magdalena Ola Cichocka; Jonas Ångström; Bin Wang; Xiaodong Zou; Stef Smeets
Journal:  J Appl Crystallogr       Date:  2018-11-22       Impact factor: 3.304

Review 6.  3D Electron Diffraction: The Nanocrystallography Revolution.

Authors:  Mauro Gemmi; Enrico Mugnaioli; Tatiana E Gorelik; Ute Kolb; Lukas Palatinus; Philippe Boullay; Sven Hovmöller; Jan Pieter Abrahams
Journal:  ACS Cent Sci       Date:  2019-07-19       Impact factor: 14.553

Review 7.  Three-dimensional electron diffraction for porous crystalline materials: structural determination and beyond.

Authors:  Zhehao Huang; Tom Willhammar; Xiaodong Zou
Journal:  Chem Sci       Date:  2020-12-15       Impact factor: 9.825

8.  Serial electron crystallography for structure determination and phase analysis of nanocrystalline materials.

Authors:  Stef Smeets; Xiaodong Zou; Wei Wan
Journal:  J Appl Crystallogr       Date:  2018-08-09       Impact factor: 3.304

9.  Polymorph evolution during crystal growth studied by 3D electron diffraction.

Authors:  Edward T Broadhurst; Hongyi Xu; Max T B Clabbers; Molly Lightowler; Fabio Nudelman; Xiaodong Zou; Simon Parsons
Journal:  IUCrJ       Date:  2020-01-01       Impact factor: 4.769

10.  A Robust and Biocompatible Bismuth Ellagate MOF Synthesized Under Green Ambient Conditions.

Authors:  Erik Svensson Grape; J Gabriel Flores; Tania Hidalgo; Eva Martínez-Ahumada; Aída Gutiérrez-Alejandre; Audrey Hautier; Daryl R Williams; Michael O'Keeffe; Lars Öhrström; Tom Willhammar; Patricia Horcajada; Ilich A Ibarra; A Ken Inge
Journal:  J Am Chem Soc       Date:  2020-09-17       Impact factor: 15.419
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