| Literature DB >> 28319372 |
Niall P Macdonald1, Grace L Bunton1, Ah Young Park1, Michael C Breadmore1, Nathan L Kilah1.
Abstract
3D printed micrometer-scale polymer mounts for single crystal analysis have been prepared by photopolymerization using digital light projection stereolithography (DLP-SLA), with a commercially available digital light projection stereolithography printer (US$4000) and 3DM-ABS resin (US$150 per liter). The polymer mounts were prepared in batches of 49 in 1 h 15 min, which allowed for rapid prototyping and testing of new crystal mounting designs, with a resin cost of 0.2¢ US per mount. The suitability of the 3D printed mounts for single crystal crystallography has been demonstrated through their use in Cu Kα X-ray diffraction experiments of Rochelle salt (sodium potassium tartrate), the protein lysozyme, and has been employed for routine crystallographic analysis of organic and inorganic materials.Entities:
Year: 2017 PMID: 28319372 DOI: 10.1021/acs.analchem.7b00443
Source DB: PubMed Journal: Anal Chem ISSN: 0003-2700 Impact factor: 6.986