Literature DB >> 28319372

3D Printed Micrometer-Scale Polymer Mounts for Single Crystal Analysis.

Niall P Macdonald1, Grace L Bunton1, Ah Young Park1, Michael C Breadmore1, Nathan L Kilah1.   

Abstract

3D printed micrometer-scale polymer mounts for single crystal analysis have been prepared by photopolymerization using digital light projection stereolithography (DLP-SLA), with a commercially available digital light projection stereolithography printer (US$4000) and 3DM-ABS resin (US$150 per liter). The polymer mounts were prepared in batches of 49 in 1 h 15 min, which allowed for rapid prototyping and testing of new crystal mounting designs, with a resin cost of 0.2¢ US per mount. The suitability of the 3D printed mounts for single crystal crystallography has been demonstrated through their use in Cu Kα X-ray diffraction experiments of Rochelle salt (sodium potassium tartrate), the protein lysozyme, and has been employed for routine crystallographic analysis of organic and inorganic materials.

Entities:  

Year:  2017        PMID: 28319372     DOI: 10.1021/acs.analchem.7b00443

Source DB:  PubMed          Journal:  Anal Chem        ISSN: 0003-2700            Impact factor:   6.986


  3 in total

1.  A Printed Equilibrium Dialysis Device with Integrated Membranes for Improved Binding Affinity Measurements.

Authors:  Cody W Pinger; Andrew A Heller; Dana M Spence
Journal:  Anal Chem       Date:  2017-07-06       Impact factor: 6.986

2.  3D-printed equipment to decouple (powder) X-ray diffraction sample preparation and measurement.

Authors:  Friederike Fuß; Max Rieckert; Simon Steinhauer; Moritz Liesegang; Günther Thiele
Journal:  J Appl Crystallogr       Date:  2022-04-29       Impact factor: 4.868

3.  A cross-linking strategy with moderated pre-polymerization of resin for stereolithography.

Authors:  Rongping Ni; Bin Qian; Chang Liu; Xiaofeng Liu; Jianrong Qiu
Journal:  RSC Adv       Date:  2018-08-21       Impact factor: 4.036

  3 in total

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