Literature DB >> 28162833

Optimizing disk registration algorithms for nanobeam electron diffraction strain mapping.

Thomas C Pekin1, Christoph Gammer2, Jim Ciston3, Andrew M Minor1, Colin Ophus4.   

Abstract

Scanning nanobeam electron diffraction strain mapping is a technique by which the positions of diffracted disks sampled at the nanoscale over a crystalline sample can be used to reconstruct a strain map over a large area. However, it is important that the disk positions are measured accurately, as their positions relative to a reference are directly used to calculate strain. In this study, we compare several correlation methods using both simulated and experimental data in order to directly probe susceptibility to measurement error due to non-uniform diffracted disk illumination structure. We found that prefiltering the diffraction patterns with a Sobel filter before performing cross correlation or performing a square-root magnitude weighted phase correlation returned the best results when inner disk structure was present. We have tested these methods both on simulated datasets, and experimental data from unstrained silicon as well as a twin grain boundary in 304 stainless steel.
Copyright © 2017 Elsevier B.V. All rights reserved.

Entities:  

Keywords:  Nanobeam electron diffraction; Strain measurement

Year:  2017        PMID: 28162833     DOI: 10.1016/j.ultramic.2016.12.021

Source DB:  PubMed          Journal:  Ultramicroscopy        ISSN: 0304-3991            Impact factor:   2.689


  5 in total

1.  A symmetry-derived mechanism for atomic resolution imaging.

Authors:  Matus Krajnak; Joanne Etheridge
Journal:  Proc Natl Acad Sci U S A       Date:  2020-10-22       Impact factor: 11.205

2.  Making the Most of your Electrons: Challenges and Opportunities in Characterizing Hybrid Interfaces with STEM.

Authors:  Stephanie M Ribet; Akshay A Murthy; Eric W Roth; Roberto Dos Reis; Vinayak P Dravid
Journal:  Mater Today (Kidlington)       Date:  2021-06-19       Impact factor: 31.041

3.  A fast image simulation algorithm for scanning transmission electron microscopy.

Authors:  Colin Ophus
Journal:  Adv Struct Chem Imaging       Date:  2017-05-10

4.  Cryogenic 4D-STEM analysis of an amorphous-crystalline polymer blend: Combined nanocrystalline and amorphous phase mapping.

Authors:  Jennifer Donohue; Steven E Zeltmann; Karen C Bustillo; Benjamin Savitzky; Mary Ann Jones; Gregory F Meyers; Colin Ophus; Andrew M Minor
Journal:  iScience       Date:  2022-02-05

5.  Characterizing transition-metal dichalcogenide thin-films using hyperspectral imaging and machine learning.

Authors:  Brian Shevitski; Christopher T Chen; Christoph Kastl; Tevye Kuykendall; Adam Schwartzberg; Shaul Aloni; Alex Zettl
Journal:  Sci Rep       Date:  2020-07-14       Impact factor: 4.996

  5 in total

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