Literature DB >> 28099549

Warming up for mechanosynthesis - temperature development in ball mills during synthesis.

Hannes Kulla1, Manuel Wilke, Franziska Fischer, Mathias Röllig, Christiane Maierhofer, Franziska Emmerling.   

Abstract

We present a first direct measurement of the temperature during milling combined with in situ Raman spectroscopy monitoring. The data reveal a low temperature increase due to the mechanical impact and clear temperature increases as a consequence of the reaction heat. Based on the data, temperature rises as postulated in the magma plasma and hot spot theory can be excluded for soft matter milling syntheses.

Year:  2017        PMID： 28099549     DOI： 10.1039/c6cc08950j

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  17 in total

1.  Mechanochemical borylation of aryldiazonium salts; merging light and ball milling.

Authors:  José G Hernández
Journal:  Beilstein J Org Chem       Date:  2017-07-26       Impact factor: 2.883

2.  Enthalpy vs. friction: heat flow modelling of unexpected temperature profiles in mechanochemistry of metal-organic frameworks.

Authors:  Krunoslav Užarević; Nenad Ferdelji; Tomislav Mrla; Patrick A Julien; Boris Halasz; Tomislav Friščić; Ivan Halasz
Journal:  Chem Sci       Date:  2018-01-23       Impact factor: 9.825

3.  Mechanochemical Knoevenagel condensation investigated in situ.

Authors:  Sebastian Haferkamp; Franziska Fischer; Werner Kraus; Franziska Emmerling
Journal:  Beilstein J Org Chem       Date:  2017-09-26       Impact factor: 2.883

Review 4.  Mechanochemical synthesis of small organic molecules.

Authors:  Tapas Kumar Achar; Anima Bose; Prasenjit Mal
Journal:  Beilstein J Org Chem       Date:  2017-09-11       Impact factor: 2.883

5.  Understanding the unexpected effect of frequency on the kinetics of a covalent reaction under ball-milling conditions.

Authors:  Ana M Belenguer; Adam A L Michalchuk; Giulio I Lampronti; Jeremy K M Sanders
Journal:  Beilstein J Org Chem       Date:  2019-06-05       Impact factor: 2.883

6.  Mechanochemical Palladium-Catalyzed Carbonylative Reactions Using Mo(CO)6.

Authors:  Pit van Bonn; Carsten Bolm; José G Hernández
Journal:  Chemistry       Date:  2020-02-11       Impact factor: 5.236

Review 7.  Mechanochemistry: A Green Approach in the Preparation of Pharmaceutical Cocrystals.

Authors:  Mizraín Solares-Briones; Guadalupe Coyote-Dotor; José C Páez-Franco; Miriam R Zermeño-Ortega; Carmen Myriam de la O Contreras; Daniel Canseco-González; Alcives Avila-Sorrosa; David Morales-Morales; Juan M Germán-Acacio
Journal:  Pharmaceutics       Date:  2021-05-25       Impact factor: 6.321

8.  The effect of milling frequency on a mechanochemical organic reaction monitored by in situ Raman spectroscopy.

Authors:  Patrick A Julien; Ivani Malvestiti; Tomislav Friščić
Journal:  Beilstein J Org Chem       Date:  2017-10-18       Impact factor: 2.883

9.  Decoupling the Arrhenius equation via mechanochemistry.

Authors:  Joel M Andersen; James Mack
Journal:  Chem Sci       Date:  2017-05-30       Impact factor: 9.825

10.  Direct Access by Mechanochemistry or Sonochemistry to Protonated Merocyanines: Components of a Four-State Molecular Switch.

Authors:  Melwin Colaço; Andrea Carletta; Mégane Van Gysel; Koen Robeyns; Nikolay Tumanov; Johan Wouters
Journal:  ChemistryOpen       Date:  2018-07-02       Impact factor: 2.911
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