Literature DB >> 27802722

Laboratory von Hámos X-ray spectroscopy for routine sample characterization.

Zoltán Németh1, Jakub Szlachetko2, Éva G Bajnóczi1, György Vankó1.   

Abstract

High energy resolution, hard X-ray spectroscopies are powerful element selective probes of the electronic and local structure of matter, with diverse applications in chemistry, physics, biology, and materials science. The routine application of these techniques is hindered by the complicated and slow access to synchrotron radiation facilities. Here we propose a new, economic, easily operated laboratory high resolution von Hámos type X-ray spectrometer, which offers rapid transmission experiments for X-ray absorption and is also capable of recording X-ray emission spectra. The use of a cylindrical analyzer crystal and a position sensitive detector enabled us to build a robust, flexible setup with low operational costs, while delivering synchrotron grade signal to noise measurements in reasonable acquisition times. We demonstrate the proof of principle and give examples for both measurement types. Finally, tracking of a several day long chemical transformation, a case better suited for laboratory than synchrotron investigation, is also presented.

Entities:  

Year:  2016        PMID: 27802722     DOI: 10.1063/1.4964098

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  5 in total

1.  Determination of Hexavalent Chromium Fractions in Plastics Using Laboratory-Based, High-Resolution X-ray Emission Spectroscopy.

Authors:  Evan P Jahrman; Gerald T Seidler; John R Sieber
Journal:  Anal Chem       Date:  2018-05-24       Impact factor: 6.986

2.  Characterization of Li-S Batteries Using Laboratory Sulfur X-ray Emission Spectroscopy.

Authors:  Matjaž Kavčič; Marko Petric; Ava Rajh; Kristina Isaković; Alen Vizintin; Sara Drvarič Talian; Robert Dominko
Journal:  ACS Appl Energy Mater       Date:  2021-02-23

3.  HERMES - a GUI-based software tool for pre-processing of X-ray absorption spectroscopy data from laboratory Rowland circle spectrometers.

Authors:  Marco E Seddon-Ferretti; Lucy M Mottram; Martin C Stennett; Claire L Corkhill; Neil C Hyatt
Journal:  J Synchrotron Radiat       Date:  2022-01-01       Impact factor: 2.616

4.  Multicolor single-analyzer high-energy-resolution XES spectrometer for simultaneous examination of different elements.

Authors:  Antal Mikeházi; Jihad El Guettioui; István B Földes; György Vankó; Zoltán Németh
Journal:  J Synchrotron Radiat       Date:  2022-08-12       Impact factor: 2.557

5.  The versatile X-ray beamline of the Munich Compact Light Source: design, instrumentation and applications.

Authors:  Benedikt Günther; Regine Gradl; Christoph Jud; Elena Eggl; Juanjuan Huang; Stephanie Kulpe; Klaus Achterhold; Bernhard Gleich; Martin Dierolf; Franz Pfeiffer
Journal:  J Synchrotron Radiat       Date:  2020-07-31       Impact factor: 2.616

  5 in total

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