Nergiz Rona1, Murat Yenisey2, Gokhan Kucukturk3, Hakan Gurun4, Can Cogun5, Ziya Esen6. 1. Bafra Public Oral Health Center, Samsun, Turkey. Electronic address: dtnergiz@gmail.com. 2. Department of Prosthodontics, Faculty of Dentistry, Ondokuz Mayis University, Samsun, Turkey. Electronic address: muyenisey@omu.edu.tr. 3. Department of Mechanical Engineering, Faculty of Engineering, Gazi University, Ankara, Turkey. Electronic address: kucukturkg@gmail.com. 4. Department of Manufacturing Engineering, Faculty of Technology, Gazi University, Ankara, Turkey. Electronic address: hgurun@gazi.edu.tr. 5. Department of Mechatronics Engineering, Faculty of Engineering, Cankaya University, Ankara, Turkey. Electronic address: cogun@cankaya.edu.tr. 6. Department of Materials Science and Engineering, Faculty of Engineering, Cankaya University, Ankara, Turkey. Electronic address: ziyaesen@cankaya.edu.tr.
Abstract
PURPOSE: The study determined (i) the effects of electrical discharge machining (EDM) on the shear-bond strength (SBS) of the bond between luting resin and zirconia ceramic and (ii) zirconia ceramic's flexural strength with the three-point bending (TPB) test. METHODS: Sixty 4.8mm×4.8mm×3.2mm zirconia specimens were fabricated and divided into four groups (n=15): SBG: sandblasted+silane, TSCG: tribochemical silica coated+silane, LTG: Er:YAG laser treated+silane, EDMG: EDM+silane. The specimens were then bonded to a composite block with a dual-cure resin cement and thermal cycled (6000 times) prior to SBS testing. The SBS tests were performed in a universal testing machine. The SBS values were statistically analyzed using ANOVA and Tukey's test. To determine flexural strength, sixty zirconia specimens were prepared and assigned to the same groups (n=15) mentioned earlier. After surface treatment TPB tests were performed in a universal testing machine (ISO 6872). The flexural strength values were statistically analyzed using ANOVA and Tukey's test (α=0.05). RESULTS: The bond strengths for the four test groups (mean±SD; MPa) were as follows: SBG (Control), 12.73±3.41, TSCG, 14.99±3.14, LTG, 7.93±2.07, EDMG, 17.05±2.71. The bond strength of the EDMG was significantly higher than those of the SBG and LTG (p<0.01). The average flexural strength values for the groups SBG (Control), TSCG, LTG and EDMG were 809.47, 800.47, 679.19 and 695.71MPa, respectively (p>0.05). CONCLUSIONS: The EDM process improved the SBS. In addition, there was no significant adverse effect of EDM on the flexural strength of zirconia.
PURPOSE: The study determined (i) the effects of electrical discharge machining (EDM) on the shear-bond strength (SBS) of the bond between luting resin and zirconia ceramic and (ii) zirconia ceramic's flexural strength with the three-point bending (TPB) test. METHODS: Sixty 4.8mm×4.8mm×3.2mm zirconia specimens were fabricated and divided into four groups (n=15): SBG: sandblasted+silane, TSCG: tribochemical silica coated+silane, LTG: Er:YAG laser treated+silane, EDMG: EDM+silane. The specimens were then bonded to a composite block with a dual-cure resin cement and thermal cycled (6000 times) prior to SBS testing. The SBS tests were performed in a universal testing machine. The SBS values were statistically analyzed using ANOVA and Tukey's test. To determine flexural strength, sixty zirconia specimens were prepared and assigned to the same groups (n=15) mentioned earlier. After surface treatment TPB tests were performed in a universal testing machine (ISO 6872). The flexural strength values were statistically analyzed using ANOVA and Tukey's test (α=0.05). RESULTS: The bond strengths for the four test groups (mean±SD; MPa) were as follows: SBG (Control), 12.73±3.41, TSCG, 14.99±3.14, LTG, 7.93±2.07, EDMG, 17.05±2.71. The bond strength of the EDMG was significantly higher than those of the SBG and LTG (p<0.01). The average flexural strength values for the groups SBG (Control), TSCG, LTG and EDMG were 809.47, 800.47, 679.19 and 695.71MPa, respectively (p>0.05). CONCLUSIONS: The EDM process improved the SBS. In addition, there was no significant adverse effect of EDM on the flexural strength of zirconia.