Literature DB >> 27563976

Chromatic Aberration Correction for Atomic Resolution TEM Imaging from 20 to 80 kV.

Martin Linck1, Peter Hartel1, Stephan Uhlemann1, Frank Kahl1, Heiko Müller1, Joachim Zach1, Max Haider1, Marcel Niestadt2, Maarten Bischoff2, Johannes Biskupek3, Zhongbo Lee3, Tibor Lehnert3, Felix Börrnert3, Harald Rose3, Ute Kaiser3.   

Abstract

Atomic resolution in transmission electron microscopy of thin and light-atom materials requires a rigorous reduction of the beam energy to reduce knockon damage. However, at the same time, the chromatic aberration deteriorates the resolution of the TEM image dramatically. Within the framework of the SALVE project, we introduce a newly developed C_{c}/C_{s} corrector that is capable of correcting both the chromatic and the spherical aberration in the range of accelerating voltages from 20 to 80 kV. The corrector allows correcting axial aberrations up to fifth order as well as the dominating off-axial aberrations. Over the entire voltage range, optimum phase-contrast imaging conditions for weak signals from light atoms can be adjusted for an optical aperture of at least 55 mrad. The information transfer within this aperture is no longer limited by chromatic aberrations. We demonstrate the performance of the microscope using the examples of 30 kV phase-contrast TEM images of graphene and molybdenum disulfide, showing unprecedented contrast and resolution that matches image calculations.

Entities:  

Year:  2016        PMID: 27563976     DOI: 10.1103/PhysRevLett.117.076101

Source DB:  PubMed          Journal:  Phys Rev Lett        ISSN: 0031-9007            Impact factor:   9.161


  9 in total

1.  Tailoring electron beams with high-frequency self-assembled magnetic charged particle micro optics.

Authors:  R Huber; F Kern; D D Karnaushenko; E Eisner; P Lepucki; A Thampi; A Mirhajivarzaneh; C Becker; T Kang; S Baunack; B Büchner; D Karnaushenko; O G Schmidt; A Lubk
Journal:  Nat Commun       Date:  2022-06-09       Impact factor: 17.694

2.  Optimal acceleration voltage for near-atomic resolution imaging of layer-stacked 2D polymer thin films.

Authors:  Baokun Liang; Yingying Zhang; Christopher Leist; Zhaowei Ou; Miroslav Položij; Zhiyong Wang; David Mücke; Renhao Dong; Zhikun Zheng; Thomas Heine; Xinliang Feng; Ute Kaiser; Haoyuan Qi
Journal:  Nat Commun       Date:  2022-07-08       Impact factor: 17.694

3.  Automatic software correction of residual aberrations in reconstructed HRTEM exit waves of crystalline samples.

Authors:  Colin Ophus; Haider I Rasool; Martin Linck; Alex Zettl; Jim Ciston
Journal:  Adv Struct Chem Imaging       Date:  2016-11-30

4.  Non-diffracting multi-electron vortex beams balancing their electron-electron interactions.

Authors:  Maor Mutzafi; Ido Kaminer; Gal Harari; Mordechai Segev
Journal:  Nat Commun       Date:  2017-09-21       Impact factor: 14.919

5.  EELS at very high energy losses.

Authors:  Ian MacLaren; Kirsty J Annand; Colin Black; Alan J Craven
Journal:  Microscopy (Oxf)       Date:  2018-03-01       Impact factor: 1.571

6.  The energy dependence of contrast and damage in electron cryomicroscopy of biological molecules.

Authors:  Mathew J Peet; Richard Henderson; Christopher J Russo
Journal:  Ultramicroscopy       Date:  2019-02-07       Impact factor: 2.689

7.  CryoEM at 100 keV: a demonstration and prospects.

Authors:  K Naydenova; G McMullan; M J Peet; Y Lee; P C Edwards; S Chen; E Leahy; S Scotcher; R Henderson; C J Russo
Journal:  IUCrJ       Date:  2019-10-11       Impact factor: 4.769

8.  Aberration correction for low voltage optimized transmission electron microscopy.

Authors:  Jaromír Bačovský
Journal:  MethodsX       Date:  2018-08-25

9.  Imaging an unsupported metal-metal bond in dirhenium molecules at the atomic scale.

Authors:  Kecheng Cao; Stephen T Skowron; Johannes Biskupek; Craig T Stoppiello; Christopher Leist; Elena Besley; Andrei N Khlobystov; Ute Kaiser
Journal:  Sci Adv       Date:  2020-01-17       Impact factor: 14.136

  9 in total

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