Literature DB >> 27212021

Quantitative analysis of methyl and propyl parabens in neonatal DBS using LC-MS/MS.

Shirish Yakkundi1, Hussain Mulla2, Hitesh Pandya3, Mark A Turner4, James McElnay1.   

Abstract

AIM: Excipients are used to overcome the chemical, physical and microbiological challenges posed by developing formulated medicines. Both methyl and propyl paraben are commonly used in pediatric liquid formulations. There is no data on systemic exposure to parabens in neonates. The European Study of Neonatal Exposure to Excipients project has investigated this. Results & methodology: DBS sampling was used to collect opportunistic blood samples. Parabens were extracted from the DBS and analyzed using a validated LC-MS/MS assay. DISCUSSION &
CONCLUSION: The above assay was applied to analyze neonatal DBS samples. The blood concentrations of parabens in neonates confirm systemic exposure to parabens following administration of routine medicines.

Entities:  

Keywords:  DBS; acceptable daily intake; excipient kinetics; internal standard; parabens; solid phase extraction

Mesh:

Substances:

Year:  2016        PMID: 27212021     DOI: 10.4155/bio-2016-0029

Source DB:  PubMed          Journal:  Bioanalysis        ISSN: 1757-6180            Impact factor:   2.681


  4 in total

Review 1.  The Current States, Challenges, Ongoing Efforts, and Future Perspectives of Pharmaceutical Excipients in Pediatric Patients in Each Country and Region.

Authors:  Jumpei Saito; Anjali Agrawal; Vandana Patravale; Anjali Pandya; Samuel Orubu; Min Zhao; Gavin P Andrews; Caroline Petit-Turcotte; Hannah Landry; Alysha Croker; Hidefumi Nakamura; Akimasa Yamatani; Smita Salunke
Journal:  Children (Basel)       Date:  2022-03-23

2.  Trace Level Detection of Bisphenol A Analogues and Parabens by LC-MS/MS in Human Plasma from Malaysians.

Authors:  Idha Arfianti Wiraagni; Mustafa Ali Mohd; Rusdi Abdul Rashid; Didi Erwandi Bin Mohamad Haron
Journal:  Biomed Res Int       Date:  2020-04-29       Impact factor: 3.411

3.  Excipients in Neonatal Medicinal Products: Never Prescribed, Commonly Administered.

Authors:  Kristine Svinning Valeur; Helle Holst; Karel Allegaert
Journal:  Pharmaceut Med       Date:  2018-08-10

4.  A 'Dilute and Shoot' Liquid Chromatography-Mass Spectrometry Method for Multiclass Drug Analysis in Pre-Cut Dried Blood Spots.

Authors:  Lucia Mainero Rocca; Nunziata L'Episcopo; Andrea Gordiani; Matteo Vitali; Alessandro Staderini
Journal:  Int J Environ Res Public Health       Date:  2021-03-16       Impact factor: 3.390

  4 in total

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