Literature DB >> 27140166

A Johann-type X-ray emission spectrometer at the Rossendorf beamline.

Kristina O Kvashnina1, Andreas C Scheinost1.   

Abstract

This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (∼3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65°-89°. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.

Entities:  

Keywords:  HERFD; Johann geometry; RIXS; X-ray emission spectrometer; XANES; XES; actinides

Year:  2016        PMID: 27140166     DOI: 10.1107/S1600577516004483

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  8 in total

1.  Application of multi-edge HERFD-XAS to assess the uranium valence electronic structure in potassium uranate (KUO3).

Authors:  René Bes; Gregory Leinders; Kristina Kvashnina
Journal:  J Synchrotron Radiat       Date:  2022-01-01       Impact factor: 2.616

Review 2.  High-energy resolution X-ray spectroscopy at actinide M4,5 and ligand K edges: what we know, what we want to know, and what we can know.

Authors:  Kristina O Kvashnina; Sergei M Butorin
Journal:  Chem Commun (Camb)       Date:  2022-01-04       Impact factor: 6.222

3.  A multi-technique study of altered granitic rock from the Krunkelbach Valley uranium deposit, Southern Germany.

Authors:  Ivan Pidchenko; Stephen Bauters; Irina Sinenko; Simone Hempel; Lucia Amidani; Dirk Detollenaere; Laszlo Vinze; Dipanjan Banerjee; Roelof van Silfhout; Stepan N Kalmykov; Jörg Göttlicher; Robert J Baker; Kristina O Kvashnina
Journal:  RSC Adv       Date:  2020-07-06       Impact factor: 4.036

4.  X-ray studies bridge the molecular and macro length scales during the emergence of CoO assemblies.

Authors:  Lukas Grote; Cecilia A Zito; Kilian Frank; Ann-Christin Dippel; Patrick Reisbeck; Krzysztof Pitala; Kristina O Kvashnina; Stephen Bauters; Blanka Detlefs; Oleh Ivashko; Pallavi Pandit; Matthias Rebber; Sani Y Harouna-Mayer; Bert Nickel; Dorota Koziej
Journal:  Nat Commun       Date:  2021-07-20       Impact factor: 14.919

5.  Nanoscale mechanism of UO2 formation through uranium reduction by magnetite.

Authors:  Zezhen Pan; Barbora Bártová; Thomas LaGrange; Sergei M Butorin; Neil C Hyatt; Martin C Stennett; Kristina O Kvashnina; Rizlan Bernier-Latmani
Journal:  Nat Commun       Date:  2020-08-10       Impact factor: 14.919

6.  A Novel Metastable Pentavalent Plutonium Solid Phase on the Pathway from Aqueous Plutonium(VI) to PuO2 Nanoparticles.

Authors:  Kristina O Kvashnina; Anna Yu Romanchuk; Ivan Pidchenko; Lucia Amidani; Evgeny Gerber; Alexander Trigub; Andre Rossberg; Stephan Weiss; Karin Popa; Olaf Walter; Roberto Caciuffo; Andreas C Scheinost; Sergei M Butorin; Stepan N Kalmykov
Journal:  Angew Chem Int Ed Engl       Date:  2019-11-06       Impact factor: 15.336

7.  The Application of HEXS and HERFD XANES for Accurate Structural Characterisation of Actinide Nanomaterials: The Case of ThO2.

Authors:  Lucia Amidani; Gavin B M Vaughan; Tatiana V Plakhova; Anna Yu Romanchuk; Evgeny Gerber; Roman Svetogorov; Stephan Weiss; Yves Joly; Stepan N Kalmykov; Kristina O Kvashnina
Journal:  Chemistry       Date:  2020-11-12       Impact factor: 5.236

8.  New tools for calibrating diffraction setups.

Authors:  J Kieffer; V Valls; N Blanc; C Hennig
Journal:  J Synchrotron Radiat       Date:  2020-02-20       Impact factor: 2.616

  8 in total

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