Literature DB >> 27138866

Very broadband diffusion-ordered NMR spectroscopy: (19)F DOSY.

Jane E Power1, Mohammadali Foroozandeh, Pinelopi Moutzouri, Ralph W Adams, Mathias Nilsson, Steven R Coombes, Andrew R Phillips, Gareth A Morris.   

Abstract

A new pulse sequence, CHORUS Oneshot, allows measurements of diffusion-ordered spectroscopy (DOSY) spectra over the full chemical shift range of (19)F for the first time. Swept-frequency pulses are used to give very broadband excitation; the sequence is a prototype for a large family of very broadband liquid state NMR methods.

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Year:  2016        PMID: 27138866     DOI: 10.1039/c6cc02917e

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN: 1359-7345            Impact factor:   6.222


  5 in total

1.  Optimization of phase dispersion enables broadband excitation without homonuclear coupling artifacts.

Authors:  Paul Coote; Wolfgang Bermel; Haribabu Arthanari
Journal:  J Magn Reson       Date:  2021-02-04       Impact factor: 2.229

2.  19F-centred NMR analysis of mono-fluorinated compounds.

Authors:  Alan J R Smith; Richard York; Dušan Uhrín; Nicholle G A Bell
Journal:  RSC Adv       Date:  2022-03-30       Impact factor: 3.361

3.  New 19F NMR methodology reveals structures of molecules in complex mixtures of fluorinated compounds.

Authors:  Alan J R Smith; Richard York; Dušan Uhrín; Nicholle G A Bell
Journal:  Chem Sci       Date:  2022-02-25       Impact factor: 9.825

4.  Durable Modification of Wood by Benzoylation-Proof of Covalent Bonding by Solution State NMR and DOSY NMR Quick-Test.

Authors:  Jan C Namyslo; Martin H H Drafz; Dieter E Kaufmann
Journal:  Polymers (Basel)       Date:  2021-06-30       Impact factor: 4.329

5.  Selective Nuclear Magnetic Resonance Experiments for Sign-Sensitive Determination of Heteronuclear Couplings: Expanding the Analysis of Crude Reaction Mixtures.

Authors:  Guilherme Dal Poggetto; João Vitor Soares; Cláudio F Tormena
Journal:  Anal Chem       Date:  2020-09-28       Impact factor: 6.986

  5 in total

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