Literature DB >> 26911554

Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion.

D E Crawford1, L A Wright2, S L James1, A P Abbott2.   

Abstract

Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods.

Entities:  

Year:  2016        PMID： 26911554     DOI： 10.1039/c5cc09685e

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  10 in total

Review 1.  Extrusion - back to the future: Using an established technique to reform automated chemical synthesis.

Authors:  Deborah E Crawford
Journal:  Beilstein J Org Chem       Date:  2017-01-11       Impact factor: 2.883

2.  Solvent-free sonochemistry: Sonochemical organic synthesis in the absence of a liquid medium.

Authors:  Deborah E Crawford
Journal:  Beilstein J Org Chem       Date:  2017-09-04       Impact factor: 2.883

3.  Mechanochemical Catalytic Transfer Hydrogenation of Aromatic Nitro Derivatives.

Authors:  Tomislav Portada; Davor Margetić; Vjekoslav Štrukil
Journal:  Molecules       Date:  2018-11-30       Impact factor: 4.411

Review 4.  Deep Eutectic Solvents for Pretreatment, Extraction, and Catalysis of Biomass and Food Waste.

Authors:  Payam Kalhor; Khashayar Ghandi
Journal:  Molecules       Date:  2019-11-06       Impact factor: 4.411

Review 5.  Deep Eutectic Solvents in Solar Energy Technologies.

Authors:  Chiara Liliana Boldrini; Andrea Francesca Quivelli; Norberto Manfredi; Vito Capriati; Alessandro Abbotto
Journal:  Molecules       Date:  2022-01-21       Impact factor: 4.411

Review 6.  Mechanochemistry: A Green Approach in the Preparation of Pharmaceutical Cocrystals.

Authors:  Mizraín Solares-Briones; Guadalupe Coyote-Dotor; José C Páez-Franco; Miriam R Zermeño-Ortega; Carmen Myriam de la O Contreras; Daniel Canseco-González; Alcives Avila-Sorrosa; David Morales-Morales; Juan M Germán-Acacio
Journal:  Pharmaceutics       Date:  2021-05-25       Impact factor: 6.321

Review 7.  The Mechanochemical Synthesis and Activation of Carbon-Rich π-Conjugated Materials.

Authors:  Mingjun Xuan; Christian Schumacher; Carsten Bolm; Robert Göstl; Andreas Herrmann
Journal:  Adv Sci (Weinh)       Date:  2022-01-20       Impact factor: 17.521

8.  Green Method for the Synthetic Ugi Reaction by Twin Screw Extrusion without a Solvent and Catalyst.

Authors:  Mahmoud Abd El Aleem Ali Ali El-Remaily; Ahmed M M Soliman; Omar M Elhady
Journal:  ACS Omega       Date:  2020-03-12

9.  Sustainable mechanochemical synthesis of β-cyclodextrin polymers by twin screw extrusion.

Authors:  Alberto Rubin Pedrazzo; Francesco Trotta; Gjylije Hoti; Federico Cesano; Marco Zanetti
Journal:  Environ Sci Pollut Res Int       Date:  2021-08-23       Impact factor: 4.223

Review 10.  Deep Eutectic Solvent as Green Solvent in Extraction of Biological Macromolecules: A Review.

Authors:  Jordy Kim Ung Ling; Kunn Hadinoto
Journal:  Int J Mol Sci       Date:  2022-03-21       Impact factor: 5.923
  10 in total

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