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Literature DB >> 26650072

High-Resolution Imaging and Spectroscopy at High Pressure: A Novel Liquid Cell for the Transmission Electron Microscope.

Mihaela Tanase¹, Jonathan Winterstein¹, Renu Sharma¹, Vladimir Aksyuk¹, Glenn Holland¹, James A Liddle¹.

Abstract

We demonstrate quantitative core-loss electron energy-loss spectroscopy of iron oxide nanoparticles and imaging resolution of Ag nanoparticles in liquid down to 0.24 nm, in both transmission and scanning transmission modes, in a novel, monolithic liquid cell developed for the transmission electron microscope (TEM). At typical SiN membrane thicknesses of 50 nm the liquid-layer thickness has a maximum change of only 30 nm for the entire TEM viewing area of 200×200 µm.

Entities: Chemical Disease Species

Keywords: zzm321990 in zzm321990 situzzm321990 ; EELS; TEM; liquid; windowed cell

Year: 2015 PMID： 26650072 PMCID： PMC4763102 DOI： 10.1017/S1431927615015482

Source DB: PubMed Journal: Microsc Microanal ISSN： 1431-9276 Impact factor: 4.127

28 in total

1. Design and Applications of Environmental Cell Transmission Electron Microscope for In Situ Observations of Gas-Solid Reactions.

Authors: Renu Sharma
Journal: Microsc Microanal Date: 2001-11 Impact factor: 4.127

2. In situ study of the growth kinetics of individual island electrodeposition of copper.

Authors: A Radisic; F M Ross; P C Searson
Journal: J Phys Chem B Date: 2006-04-20 Impact factor: 2.991

3. Fourier-ratio deconvolution and its Bayesian equivalent.

Authors: R F Egerton; F Wang; M Malac; M S Moreno; F Hofer
Journal: Micron Date: 2007-10-22 Impact factor: 2.251

4. Quantifying electrochemical nucleation and growth of nanoscale clusters using real-time kinetic data.

Authors: Aleksandar Radisic; Philippe M Vereecken; James B Hannon; Peter C Searson; Frances M Ross
Journal: Nano Lett Date: 2006-02 Impact factor: 11.189

5. Novel microchip for in situ TEM imaging of living organisms and bio-reactions in aqueous conditions.

Authors: Kuo-Liang Liu; Chien-Chen Wu; Ying-Jung Huang; Hwei-Ling Peng; Hwan-You Chang; Pin Chang; Long Hsu; Tri-Rung Yew
Journal: Lab Chip Date: 2008-09-12 Impact factor: 6.799

6. Atomic-scale electron microscopy at ambient pressure.

Authors: J F Creemer; S Helveg; G H Hoveling; S Ullmann; A M Molenbroek; P M Sarro; H W Zandbergen
Journal: Ultramicroscopy Date: 2008-05-02 Impact factor: 2.689

7. The influence of the sample thickness on the lateral and axial resolution of aberration-corrected scanning transmission electron microscopy.

Authors: Ranjan Ramachandra; Hendrix Demers; Niels de Jonge
Journal: Microsc Microanal Date: 2013-01-07 Impact factor: 4.127

8. Visualizing nanoparticle mobility in liquid at atomic resolution.

Authors: Madeline J Dukes; Benjamin W Jacobs; David G Morgan; Harshad Hegde; Deborah F Kelly
Journal: Chem Commun (Camb) Date: 2013-04-14 Impact factor: 6.222

9. An environmental cell for the examination of wet biological specimens at atmospheric pressure by transmission scanning electron microscopy.

Authors: J A Swift; A C Brown
Journal: J Phys E Date: 1970-11