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Literature DB >> 26171928

Sealed rotors for in situ high temperature high pressure MAS NMR.

Jian Zhi Hu¹, Mary Y Hu, Zhenchao Zhao, Suochang Xu, Aleksei Vjunov, Hui Shi, Donald M Camaioni, Charles H F Peden, Johannes A Lercher.

Abstract

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

Entities: Chemical Disease Gene Species

Mesh：

Substances：
Zirconium
zirconium oxide

Year: 2015 PMID： 26171928 PMCID： PMC4544657 DOI： 10.1039/c5cc03910j

Source DB: PubMed Journal: Chem Commun (Camb) ISSN： 1359-7345 Impact factor: 6.222

16 in total

1. Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems.

Authors: S P Brown; H W Spiess
Journal: Chem Rev Date: 2001-12 Impact factor: 60.622

2. In situ study on molecular diffusion phenomena in nanoporous catalytic solids.

Authors: Christian Chmelik; Jörg Kärger
Journal: Chem Soc Rev Date: 2010-10-25 Impact factor: 54.564

Review 3. Impact of in situ MAS NMR techniques to the understanding of the mechanisms of zeolite catalyzed reactions.

Authors: Irina I Ivanova; Yuriy G Kolyagin
Journal: Chem Soc Rev Date: 2010-11-01 Impact factor: 54.564

4. Methods for in situ spectroscopic probing of the synthesis of a zeolite.

Authors: Alexander Aerts; Christine E A Kirschhock; Johan A Martens
Journal: Chem Soc Rev Date: 2010-10-15 Impact factor: 54.564

5. In situ solid-state NMR for heterogeneous catalysis: a joint experimental and theoretical approach.

Authors: Weiping Zhang; Shutao Xu; Xiuwen Han; Xinhe Bao
Journal: Chem Soc Rev Date: 2011-07-11 Impact factor: 54.564

6. Following the transient reactions in lithium-sulfur batteries using an in situ nuclear magnetic resonance technique.

Authors: Jie Xiao; Jian Zhi Hu; Honghao Chen; M Vijayakumar; Jianming Zheng; Huilin Pan; Eric D Walter; Mary Hu; Xuchu Deng; Ju Feng; Bor Yann Liaw; Meng Gu; Zhiqun Daniel Deng; Dongping Lu; Suochang Xu; Chongmin Wang; Jun Liu
Journal: Nano Lett Date: 2015-04-06 Impact factor: 11.189

7. High-pressure magic angle spinning nuclear magnetic resonance.

Authors: David W Hoyt; Romulus V F Turcu; Jesse A Sears; Kevin M Rosso; Sarah D Burton; Andrew R Felmy; Jian Zhi Hu
Journal: J Magn Reson Date: 2011-07-31 Impact factor: 2.229

8. Following solid-acid-catalyzed reactions by MAS NMR spectroscopy in liquid phase--zeolite-catalyzed conversion of cyclohexanol in water.

Authors: Aleksei Vjunov; Mary Y Hu; Ju Feng; Donald M Camaioni; Donghai Mei; Jian Z Hu; Chen Zhao; Johannes A Lercher
Journal: Angew Chem Int Ed Engl Date: 2013-11-26 Impact factor: 15.336

Review 3. Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions.

Authors: Mohamed Haouas
Journal: Materials (Basel) Date: 2018-08-12 Impact factor: 3.623

3 in total