Literature DB >> 26166887

Ultrasound-mediated synthesis of N,N-bis(phenacyl)aniline under solvent-free conditions.

Jingyu He1, Lanxiang Shi1, Sijie Liu1, Peng Jia1, Juan Wang1, Ruisheng Hu1.   

Abstract

ABSTRACT: An efficient method for the synthesis of N,N-bis(phenacyl)anilines was developed via smooth condensation of anilines with α-bromoacetophenones in the presence of sodium carbonate as acid acceptor and polyethylene glycol 400 (PEG 400) as catalyst at room temperature under solvent-free conditions by using 350 W ultrasound irradiation. In addition to experimental simplicity, the main advantages of the procedure are mild conditions, short reaction times (30-45 min), and high yields (73-83 %).

Entities:  

Keywords:  N,N-bis(phenacyl)aniline; Solvent free synthesis; Ultrasound irradiation

Year:  2013        PMID： 26166887      PMCID： PMC4495021          DOI： 10.1007/s00706-013-0978-7

Source DB:  PubMed          Journal:  Monatsh Chem        ISSN： 0026-9247            Impact factor:   1.451


  7 in total

1.  Ultrasound assisted PTC catalyzed saponification of vegetable oils using aqueous alkali.

Authors:  B S Bhatkhande; S D Samant
Journal:  Ultrason Sonochem       Date:  1998-03       Impact factor: 7.491

2.  Ultrasound-promoted alkynylation of ethynylbenzene to ketones under solvent-free condition.

Authors:  Shun-Jun Ji; Zhi-Liang Shen; Da-Gong Gu; Xiao-Ying Huang
Journal:  Ultrason Sonochem       Date:  2005-02       Impact factor: 7.491

Review 3.  Power ultrasound in organic synthesis: moving cavitational chemistry from academia to innovative and large-scale applications.

Authors:  Giancarlo Cravotto; Pedro Cintas
Journal:  Chem Soc Rev       Date:  2005-10-10       Impact factor: 54.564

4.  An efficient and practical synthesis of 2,3-epoxyl-1,3-diaryl-1-propanone by combination of phase transfer catalyst and ultrasound irradiation.

Authors:  Ji-Tai Li; Xian-Feng Liu
Journal:  Ultrason Sonochem       Date:  2007-07-28       Impact factor: 7.491

5.  Convenient ultrasound mediated synthesis of substituted pyrazolones under solvent-free conditions.

Authors:  Mohammad M Mojtahedi; Mashal Javadpour; M Saeed Abaee
Journal:  Ultrason Sonochem       Date:  2008-02-29       Impact factor: 7.491

6.  Convenient ultrasound-mediated synthesis of 1,4-diazabutadienes under solvent-free conditions.

Authors:  Jing-Yu He; Hong-Xing Xin; Hong Yan; Xiu-Qing Song; Ru-Gang Zhong
Journal:  Ultrason Sonochem       Date:  2010-08-07       Impact factor: 7.491

7.  A novel and facile synthesis of 3-(2-benzofuroyl)- and 3,6-bis(2-benzofuroyl)carbazole derivatives.

Authors:  Wentao Gao; Meiru Zheng; Yang Li
Journal:  Beilstein J Org Chem       Date:  2011-11-17       Impact factor: 2.883
  7 in total
  1 in total

1.  Crystal structure and Hirshfeld surface analysis of 2,2'-(phenyl-aza-nedi-yl)bis-(1-phenyl-ethan-1-one).

Authors:  Farid N Naghiyev; Victor N Khrustalev; Marina G Safronenko; Mehmet Akkurt; Ali N Khalilov; Ajaya Bhattarai; İbrahim G Mamedov
Journal:  Acta Crystallogr E Crystallogr Commun       Date:  2022-06-07
  1 in total

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