A very simple and high-yield method to synthesize nanolayered Mn oxide.

Nanolayered Mn oxides have been prepared by a very simple, low-cost and high-yield method using soap, KOH, MnCl2 and H2O2. Scanning electron microscopy, transmission electron microscopy, dynamic light scattering, thermogravimetric analysis, Fourier transform infrared spectroscopy, and X-ray diffraction spectrometry have been used to characterize the phase and the morphology of the nanolayered Mn oxide. The nanolayered Mn oxide shows good catalytic activity toward water oxidation in the presence of cerium(iv) ammonium nitrate.