Literature DB >> 25085185

A versatile photoelectron spectrometer for pressures up to 30 mbar.

Susanna K Eriksson1, Maria Hahlin2, Juhan Matthias Kahk3, Ignacio J Villar-Garcia3, Matthew J Webb4, Helena Grennberg4, Rositza Yakimova5, Håkan Rensmo2, Kristina Edström1, Anders Hagfeldt1, Hans Siegbahn2, Mårten O M Edwards6, Patrik G Karlsson6, Klas Backlund6, John Åhlund6, David J Payne3.   

Abstract

High-pressure photoelectron spectroscopy is a rapidly developing technique with applications in a wide range of fields ranging from fundamental surface science and catalysis to energy materials, environmental science, and biology. At present the majority of the high-pressure photoelectron spectrometers are situated at synchrotron end stations, but recently a small number of laboratory-based setups have also emerged. In this paper we discuss the design and performance of a new laboratory based high pressure photoelectron spectrometer equipped with an Al Kα X-ray anode and a hemispherical electron energy analyzer combined with a differentially pumped electrostatic lens. The instrument is demonstrated to be capable of measuring core level spectra at pressures up to 30 mbar. Moreover, valence band spectra of a silver sample as well as a carbon-coated surface (graphene) recorded under a 2 mbar nitrogen atmosphere are presented, demonstrating the versatility of this laboratory-based spectrometer.

Entities:  

Year:  2014        PMID: 25085185     DOI: 10.1063/1.4890665

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  2 in total

1.  Recent approaches for bridging the pressure gap in photoelectron microspectroscopy.

Authors:  Andrei Kolmakov; Luca Gregoratti; Maya Kiskinova; Sebastian Günther
Journal:  Catal Letters       Date:  2016-01-29       Impact factor: 3.186

2.  Probing a battery electrolyte drop with ambient pressure photoelectron spectroscopy.

Authors:  Julia Maibach; Ida Källquist; Margit Andersson; Samuli Urpelainen; Kristina Edström; Håkan Rensmo; Hans Siegbahn; Maria Hahlin
Journal:  Nat Commun       Date:  2019-07-12       Impact factor: 14.919

  2 in total

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