| Literature DB >> 25085185 |
Susanna K Eriksson1, Maria Hahlin2, Juhan Matthias Kahk3, Ignacio J Villar-Garcia3, Matthew J Webb4, Helena Grennberg4, Rositza Yakimova5, Håkan Rensmo2, Kristina Edström1, Anders Hagfeldt1, Hans Siegbahn2, Mårten O M Edwards6, Patrik G Karlsson6, Klas Backlund6, John Åhlund6, David J Payne3.
Abstract
High-pressure photoelectron spectroscopy is a rapidly developing technique with applications in a wide range of fields ranging from fundamental surface science and catalysis to energy materials, environmental science, and biology. At present the majority of the high-pressure photoelectron spectrometers are situated at synchrotron end stations, but recently a small number of laboratory-based setups have also emerged. In this paper we discuss the design and performance of a new laboratory based high pressure photoelectron spectrometer equipped with an Al Kα X-ray anode and a hemispherical electron energy analyzer combined with a differentially pumped electrostatic lens. The instrument is demonstrated to be capable of measuring core level spectra at pressures up to 30 mbar. Moreover, valence band spectra of a silver sample as well as a carbon-coated surface (graphene) recorded under a 2 mbar nitrogen atmosphere are presented, demonstrating the versatility of this laboratory-based spectrometer.Entities:
Year: 2014 PMID: 25085185 DOI: 10.1063/1.4890665
Source DB: PubMed Journal: Rev Sci Instrum ISSN: 0034-6748 Impact factor: 1.523