| Literature DB >> 25016585 |
Jesus Cantu-Valle1, Francisco Ruiz-Zepeda1, Fernando Mendoza-Santoyo1, Miguel Jose-Yacaman1, Arturo Ponce2.
Abstract
In this work the calibration of a medium resolution off-axis electron holography using a dual-lens imaging system in a JEOL ARM 200F is shown. The objective dual-lens configuration allows adjusting the field of view from 35nm to 2.5μm. Subsequently, the parameters used in phase shift reconstruction were calibrated considering biprism voltage versus fringe spacing (σ) and versus fringe width (W). The reliability of the transmission electron microscope performance using these parameters was achieved using gold nanoparticles of known size and adjusting the excitation voltage of the lenses.Entities:
Keywords: Dual-lens imaging; Electron holography; Electron optics; Metallic nanoparticles; Phase reconstruction
Mesh:
Year: 2014 PMID: 25016585 PMCID: PMC4307790 DOI: 10.1016/j.ultramic.2014.06.003
Source DB: PubMed Journal: Ultramicroscopy ISSN: 0304-3991 Impact factor: 2.689