Literature DB >> 24763642

Characterization of an in-vacuum PILATUS 1M detector.

Jan Wernecke1, Christian Gollwitzer1, Peter Müller1, Michael Krumrey1.   

Abstract

A dedicated in-vacuum X-ray detector based on the hybrid pixel PILATUS 1M detector has been installed at the four-crystal monochromator beamline of the PTB at the electron storage ring BESSY II in Berlin, Germany. Owing to its windowless operation, the detector can be used in the entire photon energy range of the beamline from 10 keV down to 1.75 keV for small-angle X-ray scattering (SAXS) experiments and anomalous SAXS at absorption edges of light elements. The radiometric and geometric properties of the detector such as quantum efficiency, pixel pitch and module alignment have been determined with low uncertainties. The first grazing-incidence SAXS results demonstrate the superior resolution in momentum transfer achievable at low photon energies.

Entities:  

Keywords:  ASAXS; GISAXS; PILATUS detector; SAXS; detector design; detector quantum efficiency; hybrid pixel detector; nanometrology; small-angle X-ray scattering; solid-state detectors

Year:  2014        PMID: 24763642     DOI: 10.1107/S160057751400294X

Source DB:  PubMed          Journal:  J Synchrotron Radiat        ISSN: 0909-0495            Impact factor:   2.616


  8 in total

1.  Changes in silica nanoparticles upon internalisation by cells: size, aggregation/agglomeration state, mass- and number-based concentrations.

Authors:  Dorota Bartczak; Julie Davies; Christian Gollwitzer; Michael Krumrey; Heidi Goenaga-Infante
Journal:  Toxicol Res (Camb)       Date:  2018-01-23       Impact factor: 3.524

Review 2.  Advanced grazing-incidence techniques for modern soft-matter materials analysis.

Authors:  Alexander Hexemer; Peter Müller-Buschbaum
Journal:  IUCrJ       Date:  2015-01-01       Impact factor: 4.769

3.  In-vacuum long-wavelength macromolecular crystallography.

Authors:  Armin Wagner; Ramona Duman; Keith Henderson; Vitaliy Mykhaylyk
Journal:  Acta Crystallogr D Struct Biol       Date:  2016-03-01       Impact factor: 7.652

4.  Grazing-incidence small-angle X-ray scattering (GISAXS) on small periodic targets using large beams.

Authors:  Mika Pflüger; Victor Soltwisch; Jürgen Probst; Frank Scholze; Michael Krumrey
Journal:  IUCrJ       Date:  2017-05-24       Impact factor: 4.769

Review 5.  Evolving SAXS versatility: solution X-ray scattering for macromolecular architecture, functional landscapes, and integrative structural biology.

Authors:  Chris A Brosey; John A Tainer
Journal:  Curr Opin Struct Biol       Date:  2019-06-13       Impact factor: 6.809

6.  Synchrotron total-scattering data applicable to dual-space structural analysis.

Authors:  Jonas Beyer; Kenichi Kato; Bo Brummerstedt Iversen
Journal:  IUCrJ       Date:  2021-03-06       Impact factor: 4.769

7.  Small-angle X-ray scattering: characterization of cubic Au nanoparticles using Debye's scattering formula.

Authors:  Jérôme Deumer; Brian R Pauw; Sylvie Marguet; Dieter Skroblin; Olivier Taché; Michael Krumrey; Christian Gollwitzer
Journal:  J Appl Crystallogr       Date:  2022-07-15       Impact factor: 4.868

8.  The modular small-angle X-ray scattering data correction sequence.

Authors:  B R Pauw; A J Smith; T Snow; N J Terrill; A F Thünemann
Journal:  J Appl Crystallogr       Date:  2017-11-29       Impact factor: 3.304

  8 in total

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