Literature DB >> 24574244

In situ total X-ray scattering study of WO₃ nanoparticle formation under hydrothermal conditions.

Dipankar Saha1, Kirsten M Ø Jensen, Christoffer Tyrsted, Espen D Bøjesen, Aref Hasen Mamakhel, Ann-Christin Dippel, Mogens Christensen, Bo B Iversen.   

Abstract

Pair distribution function analysis of in situ total scattering data recorded during formation of WO3 nanocrystals under hydrothermal conditions reveal that a complex precursor structure exists in solution. The WO6 polyhedra of the precursor cluster undergo reorientation before forming the nanocrystal. This reorientation is the critical element in the formation of different hexagonal polymporphs of WO3.
© 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Entities:  

Keywords:  hydrothermal synthesis; nanoparticles; pair distribution functions; powder X-ray diffraction; tungsten

Year:  2014        PMID： 24574244     DOI： 10.1002/anie.201311254

Source DB:  PubMed          Journal:  Angew Chem Int Ed Engl        ISSN： 1433-7851            Impact factor:   15.336


  6 in total

1.  Growth kinetics determine the polydispersity and size of PbS and PbSe nanocrystals.

Authors:  Michael P Campos; Jonathan De Roo; Matthew W Greenberg; Brandon M McMurtry; Mark P Hendricks; Ellie Bennett; Natalie Saenz; Matthew Y Sfeir; Benjamin Abécassis; Sanjit K Ghose; Jonathan S Owen
Journal:  Chem Sci       Date:  2022-03-17       Impact factor: 9.969

2.  Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction.

Authors:  Ann-Christin Dippel; Hanns-Peter Liermann; Jan Torben Delitz; Peter Walter; Horst Schulte-Schrepping; Oliver H Seeck; Hermann Franz
Journal:  J Synchrotron Radiat       Date:  2015-04-14       Impact factor: 2.616

3.  Unique and facile solvothermal synthesis of mesoporous WO3 using a solid precursor and a surfactant template as a photoanode for visible-light-driven water oxidation.

Authors:  Dong Li; Debraj Chandra; Kenji Saito; Tatsuto Yui; Masayuki Yagi
Journal:  Nanoscale Res Lett       Date:  2014-10-02       Impact factor: 4.703

4.  The chemistry of ZnWO4 nanoparticle formation.

Authors:  Espen D Bøjesen; Kirsten M Ø Jensen; Christoffer Tyrsted; Aref Mamakhel; Henrik L Andersen; Hazel Reardon; Jacques Chevalier; Ann-Christin Dippel; Bo B Iversen
Journal:  Chem Sci       Date:  2016-07-05       Impact factor: 9.825

5.  Structure-mining: screening structure models by automated fitting to the atomic pair distribution function over large numbers of models.

Authors:  Long Yang; Pavol Juhás; Maxwell W Terban; Matthew G Tucker; Simon J L Billinge
Journal:  Acta Crystallogr A Found Adv       Date:  2020-04-28       Impact factor: 2.290

Review 6.  There's no place like real-space: elucidating size-dependent atomic structure of nanomaterials using pair distribution function analysis.

Authors:  Troels Lindahl Christiansen; Susan R Cooper; Kirsten M Ø Jensen
Journal:  Nanoscale Adv       Date:  2020-05-06
  6 in total

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