Literature DB >> 24458213

Diastereomeric ratio determination by high sensitivity band-selective pure shift NMR spectroscopy.

Ralph W Adams1, Liam Byrne, Péter Király, Mohammadali Foroozandeh, Liladhar Paudel, Mathias Nilsson, Jonathan Clayden, Gareth A Morris.   

Abstract

An NMR method is reported that allows diastereomeric ratios to be determined even in crowded spectra or where chemical shift differences are small compared to multiplet widths. Band-selective pure shift NMR collapses multiplets to singlets, greatly improving spectral resolution while largely retaining, or even enhancing, signal-to-noise ratio.

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Year:  2014        PMID: 24458213     DOI: 10.1039/c3cc49659g

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN: 1359-7345            Impact factor:   6.222


  4 in total

1.  Ultrahigh-resolution NMR spectroscopy.

Authors:  Mohammadali Foroozandeh; Ralph W Adams; Nicola J Meharry; Damien Jeannerat; Mathias Nilsson; Gareth A Morris
Journal:  Angew Chem Int Ed Engl       Date:  2014-05-26       Impact factor: 15.336

2.  Real-time pure shift ¹⁵N HSQC of proteins: a real improvement in resolution and sensitivity.

Authors:  Peter Kiraly; Ralph W Adams; Liladhar Paudel; Mohammadali Foroozandeh; Juan A Aguilar; István Timári; Matthew J Cliff; Mathias Nilsson; Péter Sándor; Gyula Batta; Jonathan P Waltho; Katalin E Kövér; Gareth A Morris
Journal:  J Biomol NMR       Date:  2015-03-04       Impact factor: 2.835

3.  Precise measurement of long-range heteronuclear coupling constants by a novel broadband proton-proton-decoupled CPMG-HSQMBC method.

Authors:  István Timári; Tünde Z Illyés; Ralph W Adams; Mathias Nilsson; László Szilágyi; Gareth A Morris; Katalin E Kövér
Journal:  Chemistry       Date:  2015-01-08       Impact factor: 5.236

4.  The GNAT: A new tool for processing NMR data.

Authors:  Laura Castañar; Guilherme Dal Poggetto; Adam A Colbourne; Gareth A Morris; Mathias Nilsson
Journal:  Magn Reson Chem       Date:  2018-03-25       Impact factor: 2.447

  4 in total

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