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Literature DB >> 24308719

Three-component reaction between alkynes, elemental sulfur, and aliphatic amines: a general, straightforward, and atom economical approach to thioamides.

Thanh Binh Nguyen¹, Minh Quan Tran, Ludmila Ermolenko, Ali Al-Mourabit.

Abstract

A general, straightforward, and atom-economical three-component synthesis of thioamides from alkynes, elemental sulfur, and aliphatic amines has been developed.

Entities: Chemical

Mesh：

Substances：

Year: 2013 PMID： 24308719 DOI： 10.1021/ol403345e

Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005

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Cited

8 in total

1. Synthesis of primary N-arylthioglyoxamides from anilines, elemental sulfur and primary C-H bonds in acetophenones.

Authors: Khoa M Tran; Nguyen H K Nguyen; Thuy T Bui; Tuong A To; Nam T S Phan; Ha V Le; Tung T Nguyen
Journal: RSC Adv Date: 2020-12-18 Impact factor: 4.036

Review 2. Elemental sulphur in the synthesis of sulphur-containing polymers: reaction mechanisms and green prospects.

Authors: Natalia P Tarasova; Alexey A Zanin; Efrem G Krivoborodov; Yaroslav O Mezhuev
Journal: RSC Adv Date: 2021-03-01 Impact factor: 3.361

3. Cellulose-reinforced poly(ethylene-co-vinyl acetate)-supported Ag nanoparticles with excellent catalytic properties: synthesis of thioamides using the Willgerodt-Kindler reaction.

Authors: Anoop Singh; Sanjeev Saini; Narinder Singh; Navneet Kaur; Doo Ok Jang
Journal: RSC Adv Date: 2022-02-25 Impact factor: 3.361

4. Stabilities of Three Key Biological Trisulfides with Implications for Their Roles in the Release of Hydrogen Sulfide and Bioaccumulation of Sulfane Sulfur.

Authors: Eric M Brown; Ned B Bowden
Journal: ACS Omega Date: 2022-03-22

Three-component reaction between alkynes, elemental sulfur, and aliphatic amines: a general, straightforward, and atom economical approach to thioamides.

1. Synthesis of primary N-arylthioglyoxamides from anilines, elemental sulfur and primary C-H bonds in acetophenones.

Review 2. Elemental sulphur in the synthesis of sulphur-containing polymers: reaction mechanisms and green prospects.

3. Cellulose-reinforced poly(ethylene-co-vinyl acetate)-supported Ag nanoparticles with excellent catalytic properties: synthesis of thioamides using the Willgerodt-Kindler reaction.

4. Stabilities of Three Key Biological Trisulfides with Implications for Their Roles in the Release of Hydrogen Sulfide and Bioaccumulation of Sulfane Sulfur.

5. A more sustainable isothiocyanate synthesis by amine catalyzed sulfurization of isocyanides with elemental sulfur.

6. Dimethylamine as the key intermediate generated in situ from dimethylformamide (DMF) for the synthesis of thioamides.

7. K₂S₂O₈-Promoted Aryl Thioamides Synthesis from Aryl Aldehydes Using Thiourea as the Sulfur Source.

8. Microwave-assisted synthesis of 2-substituted 4,5,6,7-tetrahydro-1,3-thiazepines from 4-aminobutanol.