| Literature DB >> 24161681 |
R Narkowicz1, H Ogata2, E Reijerse2, D Suter3.
Abstract
Cryogenic probes have significantly increased the sensitivity of NMR. Here, we present a compact EPR receiver design capable of cryogenic operation. Compared to room temperature operation, it reduces the noise by a factor of ≈2.5. We discuss in detail the design and analyze the resulting noise performance. At low microwave power, the input noise density closely follows the emission of a cooled 50Ω resistor over the whole measurement range from 20K up to room temperature. To minimize the influence of the microwave source noise, we use high microwave efficiency (≈1.1-1.7mTW(-1/2)) planar microresonators. Their efficient conversion of microwave power to magnetic field permits EPR measurements with very low power levels, typically ranging from a few μW down to fractions of nW.Keywords: Cryogenic receiver; Planar microresonators; Sensitivity; Signal-to-noise ratio
Year: 2013 PMID: 24161681 DOI: 10.1016/j.jmr.2013.09.017
Source DB: PubMed Journal: J Magn Reson ISSN: 1090-7807 Impact factor: 2.229