Literature DB >> 24056323

Efficient and fast sign-sensitive determination of heteronuclear coupling constants.

Josep Saurí1, Pau Nolis, Teodor Parella.   

Abstract

Two complementary 1D NMR approaches for the fast and easy determination of the magnitude and the sign of heteronuclear J(XH) coupling constants are proposed: The Up&Down technique relies on the direct analysis of anti-phase multiplets whereas the Left&Right technique is based on the relative displacement between separate IPAP components.
Copyright © 2013 Elsevier Inc. All rights reserved.

Entities:  

Keywords:  HSQMBC-TOCSY; Heteronuclear coupling constants; IPAP; Sign of coupling constants

Year:  2013        PMID: 24056323     DOI: 10.1016/j.jmr.2013.08.013

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  1 in total

1.  Selective Nuclear Magnetic Resonance Experiments for Sign-Sensitive Determination of Heteronuclear Couplings: Expanding the Analysis of Crude Reaction Mixtures.

Authors:  Guilherme Dal Poggetto; João Vitor Soares; Cláudio F Tormena
Journal:  Anal Chem       Date:  2020-09-28       Impact factor: 6.986

  1 in total

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