Literature DB >> 23605394

Simultaneous determination of type A-& B-trichothecenes and zearalenone in cereals by High Performance Liquid Chromatography - Tandem Mass Spectrometry.

R Schuhmacher1, F Berthiller, G Buttinger, R Krska.   

Abstract

A rapid quantitative method for the simultaneous determination of the majorFusarium mycotoxins nivalenol, deoxynivalenol, fusarenon-X, 3-acetyl-deoxynivalenol, 15-acetyl-deoxynivalenol, diacetoxyscirpenol, HT-2 toxin, T-2 toxin and zearalenone in maize and wheat was developed. Raw extracts (acetonitrile/water 84/16) are cleaned-up with MycoSep(®) columns., Chromatographic separation and end determination is carried out by HPLC-APCI-MS/MS.HPLC run times of 10 minutes considerably increases sample throughput and make this method suitable for routine analysis. The use of a triple quadrupole mass spectrometer allows the selective detection of the mycotoxins and their quantification in the low μg/kg-range.

Entities:  

Year:  2005        PMID： 23605394     DOI： 10.1007/BF02957584

Source DB:  PubMed          Journal:  Mycotoxin Res        ISSN： 0178-7888            Impact factor:   3.833


  4 in total

Review 1.  The state-of-the-art in the analysis of type-A and -B trichothecene mycotoxins in cereals.

Authors:  R Krska; S Baumgartner; R Josephs
Journal:  Fresenius J Anal Chem       Date:  2001-10

2.  Quantitative determination and structure elucidation of type A- and B-trichothecenes by HPLC/ion trap multiple mass spectrometry.

Authors:  U Berger; M Oehme; F Kuhn
Journal:  J Agric Food Chem       Date:  1999-10       Impact factor: 5.279

3.  Determination of zearalenone in grains by high-performance liquid chromatography-tandem mass spectrometry after solid-phase extraction with RP-18 columns or immunoaffinity columns.

Authors:  P Zöllner; J Jodlbauer; W Lindner
Journal:  J Chromatogr A       Date:  1999-10-15       Impact factor: 4.759

4.  Simultaneous determination of major B-trichothecenes and the de-epoxy-metabolite of deoxynivalenol in pig urine and maize using high-performance liquid chromatography-mass spectrometry.

Authors:  E Razzazi-Fazeli; J Böhm; K Jarukamjorn; J Zentek
Journal:  J Chromatogr B Analyt Technol Biomed Life Sci       Date:  2003-10-25       Impact factor: 3.205
  4 in total
  1 in total

1.  The prevalence and impact of Fusarium head blight pathogens and mycotoxins on malting barley quality in UK.

Authors:  L K Nielsen; D J Cook; S G Edwards; R V Ray
Journal:  Int J Food Microbiol       Date:  2014-03-28       Impact factor: 5.277
  1 in total

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