Literature DB >> 23605196

[Determination of zearalenone in edible oils with SEC and LC-ESI-MS/MS].

O Kappenstein1, H St Klaffke, I Mehlitz, R Tiebach, R Weber, J Lepschy, R Wittkowski.   

Abstract

A new method for the determination of zearalenone in edible oils with size exclusion chromatography (SEC) followed by LC-MS/MS as well as HPLC-FLD was developed and validated. By using the LC-MS/MS determination no further clean up step is necessary after the SEC. The correlation coefficient of 0.999 for the two detection systems is acceptable. In this research 77 edible oils were analyzed. The mean average value of 38 corn germ oils was 169 μg/kg, the maximum value amounted up to 921 μg/kg.

Entities:  

Year:  2005        PMID： 23605196     DOI： 10.1007/BF02954804

Source DB:  PubMed          Journal:  Mycotoxin Res        ISSN： 0178-7888            Impact factor:   3.833


  5 in total

1.  Determination of the fate of three Fusarium mycotoxins through wet-milling of maize using an improved HPLC analytical technique.

Authors:  D R Lauren; M A Ringrose
Journal:  Food Addit Contam       Date:  1997-07

2.  Determination of zearalenone in cornflakes and other corn-based foods by thin layer chromatography, high pressure liquid chromatography, and gas-liquid chromatography/high resolution mass spectrometry.

Authors:  P M Scott; T Panalaks; S Kanhere; W F Miles
Journal:  J Assoc Off Anal Chem       Date:  1978-05

3.  Determination of zearalenone in corn by high pressure liquid chromatography and fluorescence detection.

Authors:  G M Ware; C W Thorpe
Journal:  J Assoc Off Anal Chem       Date:  1978-09

4.  Determination of zearalenone in corn by means of immunoaffinity clean-up and high-performance liquid chromatography with fluorescence detection.

Authors:  A Visconti; M Pascale
Journal:  J Chromatogr A       Date:  1998-07-31       Impact factor: 4.759

5.  A simple quantitative HPLC method for determination of aflatoxins in cereals and animal feedstuffs using gel permeation chromatography clean-up.

Authors:  M T Hetmanski; K A Scudamore
Journal:  Food Addit Contam       Date:  1989 Jan-Mar
  5 in total
  3 in total

1.  Rapid determination of zearalenone in edible oils by HPLC with fluorescence detection.

Authors:  Paul Majerus; Norbert Graf; Maria Krämer
Journal:  Mycotoxin Res       Date:  2009-07-09       Impact factor: 3.833

2.  [Survey on deoxynivalenol, zearalenone, and HT-2/T-2 contamination of cereals and products derived from cereals].

Authors:  S Biselli
Journal:  Mycotoxin Res       Date:  2005-12       Impact factor: 3.833

3.  Mycotoxins in foods in Lower Saxony (Germany): results of official control analyses performed in 2009.

Authors:  Lilli Reinhold; Katja Reinhardt
Journal:  Mycotoxin Res       Date:  2011-02-06       Impact factor: 3.833
  3 in total

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