Literature DB >> 23552189

Practical applications of small-angle neutron scattering.

Martin J Hollamby1.   

Abstract

Recent improvements in beam-line accessibility and technology have led to small-angle neutron scattering (SANS) becoming more frequently applied to materials problems. SANS has been used to study the assembly, dispersion, alignment and mixing of nanoscale condensed matter, as well as to characterise the internal structure of organic thin films, porous structures and inclusions within steel. Using time-resolved SANS, growth mechanisms in materials systems and soft matter phase transitions can also be explored. This review is intended for newcomers to SANS as well as experts. Therefore, the basic knowledge required for its use is first summarised. After this introduction, various examples are given of the types of soft and hard matter that have been studied by SANS. The information that can be extracted from the data is highlighted, alongside the methods used to obtain it. In addition to presenting the findings, explanations are provided on how the SANS measurements were optimised, such as the use of contrast variation to highlight specific parts of a structure. Emphasis is placed on the use of complementary techniques to improve data quality (e.g. using other scattering methods) and the accuracy of data analysis (e.g. using microscopy to separately determine shape and size). This is done with a view to providing guidance on how best to design and analyse future SANS measurements on materials not listed below.

Year:  2013        PMID: 23552189     DOI: 10.1039/c3cp50293g

Source DB:  PubMed          Journal:  Phys Chem Chem Phys        ISSN: 1463-9076            Impact factor:   3.676


  9 in total

1.  Small-Angle Neutron Scattering of Liposomes: Sample Preparation to Simple Modeling.

Authors:  Kathleen Wood
Journal:  Methods Mol Biol       Date:  2022

2.  Directed assembly of optoelectronically active alkyl-π-conjugated molecules by adding n-alkanes or π-conjugated species.

Authors:  Martin J Hollamby; Maciej Karny; Paul H H Bomans; Nico A J M Sommerdijk; Nico A J M Sommerdjik; Akinori Saeki; Shu Seki; Hiroyuki Minamikawa; Isabelle Grillo; Brian R Pauw; Paul Brown; Julian Eastoe; Helmuth Möhwald; Takashi Nakanishi
Journal:  Nat Chem       Date:  2014-06-22       Impact factor: 24.427

3.  1D vs. 2D shape selectivity in the crystallization-driven self-assembly of polylactide block copolymers.

Authors:  Maria Inam; Graeme Cambridge; Anaïs Pitto-Barry; Zachary P L Laker; Neil R Wilson; Robert T Mathers; Andrew P Dove; Rachel K O'Reilly
Journal:  Chem Sci       Date:  2017-04-13       Impact factor: 9.825

4.  Effect of Formulation Method, Lipid Composition, and PEGylation on Vesicle Lamellarity: A Small-Angle Neutron Scattering Study.

Authors:  Valeria Nele; Margaret N Holme; Ulrike Kauscher; Michael R Thomas; James J Doutch; Molly M Stevens
Journal:  Langmuir       Date:  2019-04-12       Impact factor: 3.882

5.  PffBT4T-2OD Based Solar Cells with Aryl-Substituted N-Methyl-Fulleropyrrolidine Acceptors.

Authors:  Hugo Gaspar; Flávio Figueira; Karol Strutyński; Manuel Melle-Franco; Dzmitry Ivanou; João P C Tomé; Carlos M Pereira; Luiz Pereira; Adélio Mendes; Júlio C Viana; Gabriel Bernardo
Journal:  Materials (Basel)       Date:  2019-12-08       Impact factor: 3.623

6.  Isotopic Control over Self-Assembly in Supramolecular Gels.

Authors:  Kate McAulay; Han Wang; Ana M Fuentes-Caparrós; Lisa Thomson; Nikul Khunti; Nathan Cowieson; Honggang Cui; Annela Seddon; Dave J Adams
Journal:  Langmuir       Date:  2020-07-14       Impact factor: 3.882

7.  Table-top combined scanning X-ray small angle scattering and transmission microscopies of lipid vesicles dispersed in free-standing gel.

Authors:  Francesco Scattarella; Emiliano Altamura; Paola Albanese; Dritan Siliqi; Massimo Ladisa; Fabio Mavelli; Cinzia Giannini; Davide Altamura
Journal:  RSC Adv       Date:  2020-12-23       Impact factor: 3.361

8.  Computational Reverse-Engineering Analysis for Scattering Experiments (CREASE) with Machine Learning Enhancement to Determine Structure of Nanoparticle Mixtures and Solutions.

Authors:  Christian M Heil; Anvay Patil; Ali Dhinojwala; Arthi Jayaraman
Journal:  ACS Cent Sci       Date:  2022-07-01       Impact factor: 18.728

9.  The modular small-angle X-ray scattering data correction sequence.

Authors:  B R Pauw; A J Smith; T Snow; N J Terrill; A F Thünemann
Journal:  J Appl Crystallogr       Date:  2017-11-29       Impact factor: 3.304

  9 in total

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