UNLABELLED: There are concerns regarding the longevity of resin composite restorations and the clinical relevance of in vitro bond strength testing to the durability of dentin bonds in vivo. OBJECTIVE: The objectives of this investigation were to: (1) develop a new method of experimental evaluation for quantifying the durability of dentin bonds, (2) apply this method to characterize the interfacial strength of a selected commercial system under both monotonic and cyclic loading, and (3) distinguish mechanisms contributing to the interface degradation and failure. METHODS: A new method for fatigue testing the resin-dentin interface was developed based on a four-point flexure arrangement that includes two identical bonded interfaces. Cyclic loading of specimens comprised of coronal dentin bonded to a commercial resin composite and controls of resin composite was performed to failure within a hydrated environment. Scanning electron microscopy and nanoscopic dynamic mechanical analysis were used to evaluate failure mechanisms. RESULTS: The fatigue strength of the resin-dentin interface was significantly lower (p≤0.0001) than that of the resin composite and reported for dentin over the entire finite life regime. Defined at 1×10(7) cycles, the apparent endurance limit of the resin-dentin interface was 13MPa, in comparison to 48MPa and 44MPa for the resin composite and dentin, respectively. The ratio of fully reversed endurance limit to ultimate strength of the interface (0.26) was the lowest of the three materials. SIGNIFICANCE: The proposed approach for characterizing the fatigue strength of resin-dentin bonds may offer new insights concerning durability of the bonded interface.
UNLABELLED: There are concerns regarding the longevity of resin composite restorations and the clinical relevance of in vitro bond strength testing to the durability of dentin bonds in vivo. OBJECTIVE: The objectives of this investigation were to: (1) develop a new method of experimental evaluation for quantifying the durability of dentin bonds, (2) apply this method to characterize the interfacial strength of a selected commercial system under both monotonic and cyclic loading, and (3) distinguish mechanisms contributing to the interface degradation and failure. METHODS: A new method for fatigue testing the resin-dentin interface was developed based on a four-point flexure arrangement that includes two identical bonded interfaces. Cyclic loading of specimens comprised of coronal dentin bonded to a commercial resin composite and controls of resin composite was performed to failure within a hydrated environment. Scanning electron microscopy and nanoscopic dynamic mechanical analysis were used to evaluate failure mechanisms. RESULTS: The fatigue strength of the resin-dentin interface was significantly lower (p≤0.0001) than that of the resin composite and reported for dentin over the entire finite life regime. Defined at 1×10(7) cycles, the apparent endurance limit of the resin-dentin interface was 13MPa, in comparison to 48MPa and 44MPa for the resin composite and dentin, respectively. The ratio of fully reversed endurance limit to ultimate strength of the interface (0.26) was the lowest of the three materials. SIGNIFICANCE: The proposed approach for characterizing the fatigue strength of resin-dentin bonds may offer new insights concerning durability of the bonded interface.
Authors: D H Pashley; R M Carvalho; H Sano; M Nakajima; M Yoshiyama; Y Shono; C A Fernandes; F Tay Journal: J Adhes Dent Date: 1999 Impact factor: 2.359
Authors: Roland Frankenberger; Wolfgang O Strobel; Norbert Krämer; Ulrich Lohbauer; Jens Winterscheidt; Britta Winterscheidt; Anselm Petschelt Journal: J Biomed Mater Res B Appl Biomater Date: 2003-11-15 Impact factor: 3.368
Authors: Mustafa Murat Mutluay; Ke Zhang; Heonjune Ryou; Mobin Yahyazadehfar; Hessam Majd; Hockin H K Xu; Dwayne Arola Journal: J Mech Behav Biomed Mater Date: 2012-11-17
Authors: Zihou Zhang; Dylan Beitzel; Mustafa Mutluay; Franklin R Tay; David H Pashley; Dwayne Arola Journal: Dent Mater Date: 2015-07-10 Impact factor: 5.304
Authors: Zihou Zhang; Dylan Beitzel; Hessam Majd; Mustafa Mutluay; Arzu Tezvergil-Mutluay; Franklin R Tay; David H Pashley; Dwayne Arola Journal: Dent Mater Date: 2015-12-29 Impact factor: 5.304