Literature DB >> 23278006

Portable double-sided laser-heating system for Mössbauer spectroscopy and X-ray diffraction experiments at synchrotron facilities with diamond anvil cells.

I Kupenko1, L Dubrovinsky, N Dubrovinskaia, C McCammon, K Glazyrin, E Bykova, T Boffa Ballaran, R Sinmyo, A I Chumakov, V Potapkin, A Kantor, R Rüffer, M Hanfland, W Crichton, M Merlini.   

Abstract

The diamond anvil cell (DAC) technique coupled with laser heating is a major method for studying materials statically at multimegabar pressures and at high temperatures. Recent progress in experimental techniques, especially in high-pressure single crystal X-ray diffraction, requires portable laser heating systems which are able to heat and move the DAC during data collection. We have developed a double-sided laser heating system for DACs which can be mounted within a rather small (~0.1 m(2)) area and has a weight of ~12 kg. The system is easily transferable between different in-house or synchrotron facilities and can be assembled and set up within a few hours. The system was successfully tested at the High Pressure Station of White Beam (ID09a) and Nuclear Resonance (ID18) beamlines of the European Synchrotron Radiation Facility. We demonstrate examples of application of the system to a single crystal X-ray diffraction investigation of (Mg(0.87),Fe(3+) (0.09),Fe(2+) (0.04))(Si(0.89),Al(0.11))O(3) perovskite (ID09a) and a Synchrotron Mössbauer Source (SMS) study of (Mg(0.8)Fe(0.2))O ferropericlase (ID18).

Entities:  

Year:  2012        PMID: 23278006     DOI: 10.1063/1.4772458

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  6 in total

1.  Structural complexity of simple Fe2O3 at high pressures and temperatures.

Authors:  E Bykova; L Dubrovinsky; N Dubrovinskaia; M Bykov; C McCammon; S V Ovsyannikov; H-P Liermann; I Kupenko; A I Chumakov; R Rüffer; M Hanfland; V Prakapenka
Journal:  Nat Commun       Date:  2016-02-11       Impact factor: 14.919

2.  Laser-heating system for high-pressure X-ray diffraction at the Extreme Conditions beamline I15 at Diamond Light Source.

Authors:  Simone Anzellini; Annette K Kleppe; Dominik Daisenberger; Michael T Wharmby; Ruggero Giampaoli; Silvia Boccato; Marzena A Baron; Francesca Miozzi; Dean S Keeble; Allan Ross; Stuart Gurney; Jon Thompson; Giles Knap; Mark Booth; Lee Hudson; Dave Hawkins; Michael J Walter; Heribert Wilhelm
Journal:  J Synchrotron Radiat       Date:  2018-10-24       Impact factor: 2.616

3.  Stability of iron-bearing carbonates in the deep Earth's interior.

Authors:  Valerio Cerantola; Elena Bykova; Ilya Kupenko; Marco Merlini; Leyla Ismailova; Catherine McCammon; Maxim Bykov; Alexandr I Chumakov; Sylvain Petitgirard; Innokenty Kantor; Volodymyr Svitlyk; Jeroen Jacobs; Michael Hanfland; Mohamed Mezouar; Clemens Prescher; Rudolf Rüffer; Vitali B Prakapenka; Leonid Dubrovinsky
Journal:  Nat Commun       Date:  2017-07-19       Impact factor: 14.919

4.  High-Pressure NiAs-Type Modification of FeN.

Authors:  William P Clark; Simon Steinberg; Richard Dronskowski; Catherine McCammon; Ilya Kupenko; Maxim Bykov; Leonid Dubrovinsky; Lev G Akselrud; Ulrich Schwarz; Rainer Niewa
Journal:  Angew Chem Int Ed Engl       Date:  2017-05-18       Impact factor: 15.336

5.  Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains.

Authors:  M Bykov; E Bykova; G Aprilis; K Glazyrin; E Koemets; I Chuvashova; I Kupenko; C McCammon; M Mezouar; V Prakapenka; H-P Liermann; F Tasnádi; A V Ponomareva; I A Abrikosov; N Dubrovinskaia; L Dubrovinsky
Journal:  Nat Commun       Date:  2018-07-16       Impact factor: 14.919

6.  A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide.

Authors:  Georg Spiekermann; Ilya Kupenko; Sylvain Petitgirard; Manuel Harder; Alexander Nyrow; Christopher Weis; Christian Albers; Nicole Biedermann; Lélia Libon; Christoph J Sahle; Valerio Cerantola; Konstantin Glazyrin; Zuzana Konôpková; Ryosuke Sinmyo; Wolfgang Morgenroth; Ilya Sergueev; Hasan Yavaş; Leonid Dubrovinsky; Metin Tolan; Christian Sternemann; Max Wilke
Journal:  J Synchrotron Radiat       Date:  2020-02-13       Impact factor: 2.616

  6 in total

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