Literature DB >> 23002789

Silver(I)-catalyzed deprotection of p-methoxybenzyl ethers: a mild and chemoselective method.

Nicolas Kern1, Thomas Dombray, Aurélien Blanc, Jean-Marc Weibel, Patrick Pale.   

Abstract

The p-methoxybenzyl protecting group (PMB) on various alcohols and an acid was efficiently and selectively cleaved by the action of a catalytic amount of silver(I) hexafluoroantimonate combined with 0.5 equiv of 1,3,5-trimethoxybenzene in dichloromethane at 40 °C.

Entities:  

Mesh：

Substances：

Year:  2012        PMID： 23002789     DOI： 10.1021/jo301787v

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  3 in total

1.  Total Synthesis of the Congested, Bisphosphorylated Morganella morganii Zwitterionic Trisaccharide Repeating Unit.

Authors:  D Jamin Keith; Steven D Townsend
Journal:  J Am Chem Soc       Date:  2019-08-01       Impact factor: 15.419

2.  Preparation and Applications of 4-Methoxybenzyl Esters in Organic Synthesis.

Authors:  Kyle T Howard; John D Chisholm
Journal:  Org Prep Proced Int       Date:  2016-01-29       Impact factor: 1.628

3.  Synthesis of Phosphatidyl Glycerol Containing Unsymmetric Acyl Chains Using H-Phosphonate Methodology.

Authors:  Zachary J Struzik; Shruti Biyani; Tim Grotzer; Judith Storch; David H Thompson
Journal:  Molecules       Date:  2022-03-28       Impact factor: 4.411
  3 in total

北京卡尤迪生物科技股份有限公司 © 2022-2023.