| Literature DB >> 22984846 |
Young Lok Choi1, Hye Sun Lim, Hwan Jung Lim, Jung-Nyoung Heo.
Abstract
A one-pot transition-metal-free, base-mediated synthesis of dibenzo[b,f]oxepins was developed. The reaction of 2-halobenzaldehydes with (2-hydroxyphenyl)acetonitriles proceeds via a sequential aldol condensation and intramolecular ether formation reaction in the presence of Cs(2)CO(3) and molecular sieves in toluene.Entities:
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Year: 2012 PMID： 22984846 DOI： 10.1021/ol302371s
Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005