| Literature DB >> 22938312 |
Saul J Moorhouse1, Nenad Vranješ, Andrew Jupe, Michael Drakopoulos, Dermot O'Hare.
Abstract
A versatile, infrared-heated, chemical reaction cell has been assembled and commissioned for the in situ study of a range of chemical syntheses using time-resolved energy-dispersive X-ray diffraction (EDXRD) on Beamline I12 at the Diamond Light Source. Specialized reactor configurations have been constructed to enable in situ EDXRD investigation of samples under non-ambient conditions. Chemical reactions can be studied using a range of sample vessels such as alumina crucibles, steel hydrothermal autoclaves, and glassy carbon tubes, at temperatures up to 1200 °C.Entities:
Year: 2012 PMID： 22938312 DOI： 10.1063/1.4746382
Source DB: PubMed Journal: Rev Sci Instrum ISSN： 0034-6748 Impact factor: 1.523