Literature DB >> 22719468

4-[(5-Bromo-2-hy-droxy-benzyl-idene)amino]-3-propyl-1H-1,2,4-triazole-5(4H)-thione.

Xin Wu, Cai-Xia Yuan, Ling Ma, Kai-Lu Zhai, Miao-Li Zhu.   

Abstract

The asymmetric unit of the title compound, C(12)H(13)BrN(4)OS, contains two independent mol-ecules in which the dihedral angles between the triazole and benzene rings are 2.9 (3) and 7.5 (3)°. The thione group is of the form R(2)C=S. An intra-molecular O-H⋯N hydrogen bond occurs in each mol-ecule. The crystal structure features weak N-H⋯S inter-actions and π-π stacking of the benzene rings [centroid-centroid distance = 3.667 (3) Å].

Entities:  

Year:  2012        PMID: 22719468      PMCID: PMC3379270          DOI: 10.1107/S1600536812019745

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


  3 in total

1.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290

2.  Regioselective reaction: synthesis, characterization and pharmacological studies of some new Mannich bases derived from 1,2,4-triazoles.

Authors:  Arun M Isloor; Balakrishna Kalluraya; Prashanth Shetty
Journal:  Eur J Med Chem       Date:  2009-05-05       Impact factor: 6.514

3.  Mononuclear copper(II) complexes with 3,5-substituted-4-salicylidene-amino-3,5-dimethyl-1,2,4-triazole: synthesis, structure and potent inhibition of protein tyrosine phosphatases.

Authors:  Ling Ma; Liping Lu; Miaoli Zhu; Qingming Wang; Ying Li; Shu Xing; Xueqi Fu; Zengqiang Gao; Yuhui Dong
Journal:  Dalton Trans       Date:  2011-05-24       Impact factor: 4.390

  3 in total
  2 in total

1.  4-[(5-Chloro-2-hy-droxy-benzyl-idene)amino]-3-ethyl-1H-1,2,4-triazole-5(4H)-thione.

Authors:  Cai-Xia Yuan; Xu-Mei Yao; Miao-Li Zhu; Hong-Mei Zhu
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2014-04-18

2.  4-[(5-Bromo-2-hy-droxy-benzyl-idene)amino]-3-ethyl-1H-1,2,4-triazole-5(4H)-thione.

Authors:  Cai-Xia Yuan; Shu-Fen Lan; Xin-Yu Liu; Miao-Li Zhu
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2014-07-26
  2 in total

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