Redetermination of Mg(2)B(25) based on single-crystal X-ray data.

The crystal structure of Mg(2)B(25), dimagnesium penta-eicosa-boride, was reexamined from single-crystal X-ray diffraction data. The structural model previously reported on the basis of powder X-ray diffraction data [Giunchi et al. (2006 ▶). Solid State Sci.8, 1202-1208] has been confirmed, although a much higher precision refinement was achieved, leading to much smaller standard uncertainties on bond lengths and refined occupancy factors. Moreover, all atoms were refined with anisotropic displacement parameters. Mg(2)B(25) crystallizes in the β-boron structure type and is isostructural with other rhombohedral compounds of the boron-rich metal boride family. Magnesium atoms are found in inter-stitial sites on special positions (two with site symmetry .m, one with .2 and one with 3m), all with partial occupancies.

Related literature

For background to this class of compounds, see: Nagamatsu et al. (2001 ▶); Giunchi (2003 ▶), Giunchi et al. (2006 ▶). For related phases in the Mg–B system, see: Adasch et al. (2006 ▶); Brutti et al. (2002 ▶); Guette et al. (1981 ▶); Jones & Marsh (1954 ▶); Naslain et al. (1973 ▶); Russell et al. (1953 ▶); Pediaditakis et al. (2010 ▶).

Experimental

Crystal data

Mg2B25

M = 318.87

Hexagonal,

a = 11.0398 (5) Å

c = 24.195 (1) Å

V = 2553.75 (19) Å3

Z = 12

Mo Kα radiation

μ = 0.23 mm−1

T = 298 K

0.08 × 0.07 × 0.07 mm

Data collection

Oxford Xcalibur 3 CCD diffractometer

Absorption correction: gaussian (ABSPACK; Oxford Diffraction, 2006 ▶) T min = 0.982, T max = 0.984

4794 measured reflections

799 independent reflections

724 reflections with I > 2σ(I)

R int = 0.045

Refinement

R[F 2 > 2σ(F 2)] = 0.021

wR(F 2) = 0.049

S = 1.13

799 reflections

122 parameters

Δρmax = 0.14 e Å−3

Δρmin = −0.31 e Å−3

Data collection: CrysAlis CCD (Oxford Diffraction, 2006 ▶); cell refinement: CrysAlis CCD; data reduction: CrysAlis RED (Oxford Diffraction, 2006 ▶); program(s) used to solve structure: SHELXS97 (Sheldrick, 2008 ▶); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶); molecular graphics: DIAMOND (Brandenburg, 2001 ▶); software used to prepare material for publication: SHELXL97.

Crystal structure: contains datablock(s) global, I. DOI: 10.1107/S1600536812023768/wm2631sup1.cif

Structure factors: contains datablock(s) I. DOI: 10.1107/S1600536812023768/wm2631Isup2.hkl

Additional supplementary materials: crystallographic information; 3D view; checkCIF report

Mg2B25	Dx = 2.488 Mg m−3
Mr = 318.87	Mo Kα radiation, λ = 0.71073 Å
Hexagonal, R3m	Cell parameters from 562 reflections
Hall symbol: -R 3 2"	θ = 10.6–26.2°
a = 11.0398 (5) Å	µ = 0.23 mm−1
c = 24.195 (1) Å	T = 298 K
V = 2553.75 (19) Å3	Block, black
Z = 12	0.08 × 0.07 × 0.07 mm
F(000) = 1788

Oxford Xcalibur 3 CCD diffractometer	799 independent reflections
Radiation source: fine-focus sealed tube	724 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.045
ω scans	θmax = 28.0°, θmin = 2.3°
Absorption correction: gaussian (ABSPACK; Oxford Diffraction, 2006)	h = −14→14
Tmin = 0.982, Tmax = 0.984	k = −14→14
4794 measured reflections	l = −31→31

Refinement on F2	0 restraints
Least-squares matrix: full	Primary atom site location: structure-invariant direct methods
R[F2 > 2σ(F2)] = 0.021	Secondary atom site location: difference Fourier map
wR(F2) = 0.049	w = 1/[σ2(Fo2) + (0.0342P)2] where P = (Fo2 + 2Fc2)/3
S = 1.13	(Δ/σ)max = 0.001
799 reflections	Δρmax = 0.14 e Å−3
122 parameters	Δρmin = −0.31 e Å−3

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

	x	y	z	Uiso*/Ueq	Occ. (<1)
B1	0.17051 (6)	0.16425 (6)	0.17121 (2)	0.01393 (14)
B2	0.31095 (6)	0.29537 (6)	0.13087 (2)	0.01500 (14)
B3	0.25656 (6)	0.21074 (6)	0.41962 (2)	0.01482 (14)
B4	0.24302 (14)	0.2507 (2)	0.34557 (4)	0.0146 (4)	0.836 (7)
B5	0.05447 (4)	0.10893 (8)	0.94321 (3)	0.01410 (18)
B6	0.08455 (4)	0.16910 (8)	0.01360 (3)	0.01402 (18)
B7	0.10819 (4)	0.21638 (9)	0.88662 (3)	0.01461 (18)
B8	0.17148 (4)	0.34295 (8)	0.02961 (3)	0.01510 (18)
B9	0.13101 (4)	0.26201 (9)	0.76761 (3)	0.01487 (17)
B10	0.10643 (4)	0.21286 (8)	0.70081 (3)	0.01434 (18)
B11	0.05625 (4)	0.11249 (9)	0.32568 (3)	0.01443 (17)
B12	0.08963 (4)	0.17926 (8)	0.40273 (3)	0.01459 (18)
B13	0.05471 (9)	0.10941 (17)	0.55309 (6)	0.0136 (5)	0.493 (4)
B14	0.0000	0.0000	0.38677 (6)	0.0148 (3)
B15	0.0000	0.0000	0.5000	0.0148 (4)
MgN	0.12339 (3)	0.24679 (6)	0.25266 (2)	0.01846 (19)	0.5000 (14)
MgD	0.20089 (3)	0.40178 (6)	0.17677 (2)	0.0185 (2)	0.5019 (14)
MgE	0.0000	0.0000	0.23530 (4)	0.0190 (3)	0.501 (2)
MgF	0.37439 (15)	0.0000	0.0000	0.0182 (13)	0.166 (4)

	U11	U22	U33	U12	U13	U23
B1	0.0141 (3)	0.0141 (3)	0.0135 (2)	0.0071 (2)	−0.00003 (19)	0.00011 (19)
B2	0.0150 (3)	0.0153 (3)	0.0149 (2)	0.0077 (2)	0.00008 (19)	0.00003 (18)
B3	0.0151 (3)	0.0146 (3)	0.0147 (3)	0.0074 (2)	0.0002 (2)	0.00001 (19)
B4	0.0147 (5)	0.0152 (9)	0.0140 (4)	0.0075 (6)	−0.0001 (3)	0.0001 (4)
B5	0.0141 (3)	0.0143 (4)	0.0140 (4)	0.00715 (19)	0.00002 (14)	0.0000 (3)
B6	0.0140 (3)	0.0147 (4)	0.0136 (4)	0.00735 (19)	0.00002 (12)	0.0000 (2)
B7	0.0149 (3)	0.0150 (4)	0.0140 (4)	0.0075 (2)	0.00010 (14)	0.0002 (3)
B8	0.0153 (3)	0.0150 (4)	0.0149 (4)	0.0075 (2)	−0.00003 (13)	−0.0001 (3)
B9	0.0151 (3)	0.0151 (4)	0.0144 (3)	0.00757 (19)	−0.00008 (13)	−0.0002 (3)
B10	0.0147 (3)	0.0146 (4)	0.0137 (4)	0.0073 (2)	0.00022 (14)	0.0004 (3)
B11	0.0144 (3)	0.0144 (4)	0.0144 (3)	0.00722 (18)	0.00000 (14)	0.0000 (3)
B12	0.0145 (3)	0.0147 (4)	0.0147 (4)	0.00735 (19)	0.00012 (14)	0.0002 (3)
B13	0.0138 (7)	0.0139 (8)	0.0133 (7)	0.0069 (4)	0.0004 (3)	0.0008 (5)
B14	0.0146 (4)	0.0146 (4)	0.0152 (6)	0.0073 (2)	0.000	0.000
B15	0.0149 (6)	0.0149 (6)	0.0146 (8)	0.0075 (3)	0.000	0.000
MgN	0.0187 (2)	0.0185 (3)	0.0181 (3)	0.00925 (15)	0.00013 (9)	0.00025 (19)
MgD	0.0185 (2)	0.0192 (3)	0.0180 (3)	0.00961 (16)	0.00006 (9)	0.00011 (18)
MgE	0.0190 (4)	0.0190 (4)	0.0188 (5)	0.00951 (19)	0.000	0.000
MgF	0.0187 (11)	0.017 (3)	0.0183 (9)	0.0086 (16)	0.0005 (7)	0.0010 (14)

B1—B7i	1.7061 (9)	B11—B4iii	1.9145 (16)
B1—B1ii	1.7441 (12)	B11—B12	1.9703 (11)
B1—B2	1.7909 (8)	B11—MgN	2.1840 (9)
B1—B9i	1.9279 (10)	B11—MgE	2.4370 (12)
B1—B1iii	1.9515 (12)	B11—MgFix	2.5328 (11)
B1—B2iv	2.0394 (8)	B11—MgFxii	2.5329 (11)
B1—MgN	2.3363 (7)	B12—B3iii	1.7446 (6)
B1—MgE	2.4130 (8)	B12—B14	1.7568 (8)
B1—MgD	2.4754 (8)	B12—B13i	1.8389 (11)
B2—B3v	1.7785 (8)	B12—B13xiii	1.8389 (11)
B2—B2iv	1.7842 (11)	B12—B4iii	2.0165 (16)
B2—B7i	1.8389 (8)	B12—MgDx	2.2623 (9)
B2—B9vi	1.9266 (8)	B12—MgNx	2.3166 (9)
B2—B1iv	2.0394 (8)	B12—MgFix	2.6289 (11)
B2—MgD	2.3488 (7)	B12—MgFxii	2.6290 (11)
B2—MgDvii	2.3988 (6)	B13—B15	1.6566 (16)
B2—MgNvii	2.5803 (6)	B13—B14xxv	1.792 (2)
B3—B12	1.7446 (6)	B13—B3xx	1.8010 (15)
B3—B8viii	1.7667 (9)	B13—B3xiii	1.8010 (15)
B3—B2viii	1.7785 (8)	B13—B13xv	1.812 (3)
B3—B13i	1.8010 (15)	B13—B13xvi	1.812 (3)
B3—B3ii	1.8205 (12)	B13—B12xiii	1.8389 (11)
B3—B4	1.8690 (14)	B13—B12i	1.8389 (11)
B3—MgDviii	2.3723 (7)	B13—MgDx	2.1326 (17)
B3—MgFix	2.4108 (6)	B13—MgDviii	2.4373 (9)
B3—MgDx	2.4382 (7)	B13—MgDxxvii	2.4374 (9)
B3—MgNx	2.6082 (7)	B14—B12xvi	1.7568 (8)
B4—MgFix	0.848 (2)	B14—B12xv	1.7568 (8)
B4—B8viii	1.6753 (12)	B14—B13i	1.792 (2)
B4—B4xi	1.687 (4)	B14—B13xiii	1.792 (2)
B4—B10i	1.8378 (12)	B14—B13xxv	1.792 (2)
B4—B11	1.9145 (16)	B14—B11xv	1.8279 (15)
B4—B12	2.0165 (16)	B14—B11xvi	1.8279 (15)
B4—MgN	2.5964 (9)	B15—B13xxv	1.6566 (16)
B4—MgNx	2.6540 (10)	B15—B13i	1.6566 (16)
B4—MgFxii	2.8150 (16)	B15—B13xiii	1.6566 (16)
B5—B7	1.7117 (11)	B15—B13xvi	1.6566 (16)
B5—B6i	1.7626 (8)	B15—B13xv	1.6566 (16)
B5—B6xiii	1.7626 (8)	B15—MgDxxviii	2.5443 (6)
B5—B6xiv	1.7976 (11)	B15—MgDviii	2.5443 (6)
B5—B5xv	1.8039 (14)	B15—MgDx	2.5443 (6)
B5—B5xvi	1.8039 (14)	B15—MgDxxix	2.5443 (6)
B6—B8	1.7067 (12)	B15—MgDxxx	2.5444 (6)
B6—B6xvii	1.7455 (9)	B15—MgDxxvii	2.5444 (6)
B6—B6xviii	1.7455 (9)	MgN—B12x	2.3166 (9)
B6—B5xiii	1.7626 (8)	MgN—B1iii	2.3363 (7)
B6—B5i	1.7626 (8)	MgN—MgD	2.3596 (7)
B6—B5xix	1.7976 (11)	MgN—MgE	2.3966 (6)
B6—MgFxv	2.8691 (16)	MgN—B9i	2.4844 (6)
B6—MgFxvii	2.8691 (16)	MgN—B9xiii	2.4844 (6)
B7—B1xiii	1.7061 (9)	MgN—B10i	2.4848 (6)
B7—B1xx	1.7061 (9)	MgN—B10xiii	2.4848 (6)
B7—B9xxi	1.8250 (12)	MgN—MgFix	2.5333 (10)
B7—B2xx	1.8389 (8)	MgN—MgFxii	2.5333 (10)
B7—B2xiii	1.8389 (8)	MgD—B13x	2.1326 (17)
B8—B4xxii	1.6753 (12)	MgD—B12x	2.2623 (9)
B8—B4v	1.6754 (12)	MgD—B2iii	2.3488 (7)
B8—B3xxii	1.7667 (9)	MgD—B3xxii	2.3723 (7)
B8—B3v	1.7668 (9)	MgD—B3v	2.3724 (7)
B8—B10x	1.8715 (11)	MgD—B2iv	2.3987 (6)
B8—MgFxvii	2.2078 (10)	MgD—B2xxxi	2.3988 (6)
B8—MgFxv	2.2078 (10)	MgD—B13xxxii	2.4373 (9)
B9—B10	1.6831 (11)	MgD—B13v	2.4373 (9)
B9—B7xxi	1.8250 (12)	MgD—B3x	2.4382 (7)
B9—B2xxiii	1.9266 (8)	MgE—MgNxv	2.3966 (6)
B9—B2xxiv	1.9267 (8)	MgE—MgNxvi	2.3966 (6)
B9—B1xiii	1.9279 (10)	MgE—B1xxxiii	2.4130 (8)
B9—B1xx	1.9279 (10)	MgE—B1xvi	2.4130 (8)
B9—MgNxiii	2.4844 (6)	MgE—B1xv	2.4130 (8)
B9—MgNi	2.4844 (6)	MgE—B1ii	2.4130 (8)
B9—MgExxv	2.5060 (8)	MgE—B1iii	2.4130 (8)
B10—B4xx	1.8378 (12)	MgE—B11xvi	2.4370 (12)
B10—B4xiii	1.8378 (12)	MgE—B11xv	2.4370 (12)
B10—B8x	1.8715 (11)	MgF—B4ix	0.848 (2)
B10—B11xiii	1.8763 (7)	MgF—B4xxxiv	0.848 (2)
B10—B11i	1.8763 (7)	MgF—B8xviii	2.2078 (10)
B10—MgFxxiv	2.3515 (5)	MgF—B8xvi	2.2078 (10)
B10—MgFxxvi	2.3516 (5)	MgF—B10xxx	2.3516 (5)
B10—MgNxiii	2.4848 (6)	MgF—B10vi	2.3516 (5)
B10—MgNi	2.4848 (6)	MgF—B3xxxiv	2.4108 (6)
B10—MgExxv	2.5556 (10)	MgF—B3ix	2.4108 (6)
B11—B14	1.8279 (15)	MgF—B11ix	2.5328 (11)
B11—B11xv	1.8629 (14)	MgF—B11xxxv	2.5329 (11)
B11—B11xvi	1.8629 (14)	MgF—MgNix	2.5333 (10)
B11—B10i	1.8763 (7)	MgF—MgNxxxv	2.5333 (10)
B11—B10xiii	1.8763 (7)
B7i—B1—B1ii	59.26 (2)	B11—B12—MgNx	115.67 (4)
B7i—B1—B2	63.40 (4)	B4—B12—MgNx	75.18 (5)
B1ii—B1—B2	112.05 (3)	B4iii—B12—MgNx	75.19 (5)
B7i—B1—B9i	106.37 (4)	MgDx—B12—MgNx	62.02 (3)
B1ii—B1—B9i	63.11 (2)	B3—B12—MgFix	63.15 (4)
B2—B1—B9i	104.36 (4)	B3iii—B12—MgFix	123.89 (5)
B7i—B1—B1iii	118.57 (3)	B14—B12—MgFix	113.97 (5)
B1ii—B1—B1iii	120.0	B13i—B12—MgFix	118.31 (6)
B2—B1—B1iii	117.49 (3)	B13xiii—B12—MgFix	173.69 (6)
B9i—B1—B1iii	128.25 (3)	B11—B12—MgFix	65.00 (3)
B7i—B1—B2iv	104.44 (4)	B4—B12—MgFix	14.64 (6)
B1ii—B1—B2iv	109.25 (2)	B4iii—B12—MgFix	73.26 (5)
B2—B1—B2iv	55.06 (3)	MgDx—B12—MgFix	113.12 (3)
B9i—B1—B2iv	58.03 (3)	MgNx—B12—MgFix	61.23 (2)
B1iii—B1—B2iv	125.95 (2)	B3—B12—MgFxii	123.89 (5)
B7i—B1—MgN	176.04 (4)	B3iii—B12—MgFxii	63.15 (4)
B1ii—B1—MgN	120.089 (18)	B14—B12—MgFxii	113.97 (5)
B2—B1—MgN	114.58 (3)	B13i—B12—MgFxii	173.69 (6)
B9i—B1—MgN	70.53 (3)	B13xiii—B12—MgFxii	118.31 (6)
B1iii—B1—MgN	65.314 (16)	B11—B12—MgFxii	65.00 (3)
B2iv—B1—MgN	71.90 (3)	B4—B12—MgFxii	73.26 (5)
B7i—B1—MgE	121.06 (4)	B4iii—B12—MgFxii	14.64 (6)
B1ii—B1—MgE	68.814 (15)	MgDx—B12—MgFxii	113.12 (3)
B2—B1—MgE	172.93 (4)	MgNx—B12—MgFxii	61.24 (2)
B9i—B1—MgE	69.50 (3)	MgFix—B12—MgFxii	63.67 (6)
B1iii—B1—MgE	66.147 (15)	B15—B13—B14xxv	105.13 (9)
B2iv—B1—MgE	117.87 (4)	B15—B13—B3xx	141.03 (6)
MgN—B1—MgE	60.59 (2)	B14xxv—B13—B3xx	99.11 (7)
B7i—B1—MgD	121.42 (3)	B15—B13—B3xiii	141.03 (6)
B1ii—B1—MgD	172.571 (15)	B14xxv—B13—B3xiii	99.11 (7)
B2—B1—MgD	64.49 (3)	B3xx—B13—B3xiii	60.72 (7)
B9i—B1—MgD	110.71 (3)	B15—B13—B13xv	56.85 (4)
B1iii—B1—MgD	66.785 (15)	B14xxv—B13—B13xv	59.63 (5)
B2iv—B1—MgD	63.32 (2)	B3xx—B13—B13xv	158.31 (5)
MgN—B1—MgD	58.65 (2)	B3xiii—B13—B13xv	115.07 (4)
MgE—B1—MgD	113.75 (3)	B15—B13—B13xvi	56.85 (4)
B3v—B2—B2iv	128.25 (3)	B14xxv—B13—B13xvi	59.63 (5)
B3v—B2—B1	122.06 (4)	B3xx—B13—B13xvi	115.07 (4)
B2iv—B2—B1	69.56 (4)	B3xiii—B13—B13xvi	158.31 (5)
B3v—B2—B7i	117.24 (4)	B13xv—B13—B13xvi	60.0
B2iv—B2—B7i	109.96 (3)	B15—B13—B12xiii	112.69 (6)
B1—B2—B7i	56.05 (4)	B14xxv—B13—B12xiii	57.86 (5)
B3v—B2—B9vi	117.38 (4)	B3xx—B13—B12xiii	105.97 (8)
B2iv—B2—B9vi	104.67 (4)	B3xiii—B13—B12xiii	57.27 (4)
B1—B2—B9vi	104.63 (4)	B13xv—B13—B12xiii	60.49 (5)
B7i—B2—B9vi	57.92 (4)	B13xvi—B13—B12xiii	108.33 (5)
B3v—B2—B1iv	126.37 (4)	B15—B13—B12i	112.69 (6)
B2iv—B2—B1iv	55.37 (3)	B14xxv—B13—B12i	57.86 (5)
B1—B2—B1iv	108.97 (4)	B3xx—B13—B12i	57.27 (4)
B7i—B2—B1iv	103.61 (4)	B3xiii—B13—B12i	105.97 (8)
B9vi—B2—B1iv	58.09 (3)	B13xv—B13—B12i	108.33 (5)
B3v—B2—MgD	68.57 (3)	B13xvi—B13—B12i	60.49 (5)
B2iv—B2—MgD	69.42 (3)	B12xiii—B13—B12i	107.64 (9)
B1—B2—MgD	72.02 (3)	B15—B13—MgDx	83.34 (7)
B7i—B2—MgD	121.72 (4)	B14xxv—B13—MgDx	171.52 (10)
B9vi—B2—MgD	173.85 (4)	B3xx—B13—MgDx	73.64 (6)
B1iv—B2—MgD	117.63 (3)	B3xiii—B13—MgDx	73.64 (6)
B3v—B2—MgDvii	69.62 (3)	B13xv—B13—MgDx	127.13 (4)
B2iv—B2—MgDvii	66.45 (3)	B13xvi—B13—MgDx	127.13 (4)
B1—B2—MgDvii	126.89 (3)	B12xiii—B13—MgDx	119.24 (6)
B7i—B2—MgDvii	170.76 (4)	B12i—B13—MgDx	119.24 (6)
B9vi—B2—MgDvii	113.96 (4)	B15—B13—MgDviii	74.11 (4)
B1iv—B2—MgDvii	67.24 (3)	B14xxv—B13—MgDviii	113.53 (4)
MgD—B2—MgDvii	65.80 (3)	B3xx—B13—MgDviii	68.35 (3)
B3v—B2—MgNvii	70.80 (3)	B3xiii—B13—MgDviii	122.73 (7)
B2iv—B2—MgNvii	104.50 (4)	B13xv—B13—MgDviii	121.88 (4)
B1—B2—MgNvii	167.03 (4)	B13xvi—B13—MgDviii	68.18 (4)
B7i—B2—MgNvii	118.51 (4)	B12xiii—B13—MgDviii	169.64 (8)
B9vi—B2—MgNvii	65.03 (3)	B12i—B13—MgDviii	62.03 (3)
B1iv—B2—MgNvii	59.39 (2)	MgDx—B13—MgDviii	68.35 (4)
MgD—B2—MgNvii	117.48 (3)	B15—B13—MgDxxvii	74.11 (4)
MgDvii—B2—MgNvii	56.43 (2)	B14xxv—B13—MgDxxvii	113.53 (4)
B12—B3—B8viii	108.67 (5)	B3xx—B13—MgDxxvii	122.73 (7)
B12—B3—B2viii	122.77 (5)	B3xiii—B13—MgDxxvii	68.35 (3)
B8viii—B3—B2viii	120.34 (5)	B13xv—B13—MgDxxvii	68.18 (4)
B12—B3—B13i	62.46 (5)	B13xvi—B13—MgDxxvii	121.88 (4)
B8viii—B3—B13i	107.94 (5)	B12xiii—B13—MgDxxvii	62.03 (3)
B2viii—B3—B13i	120.86 (6)	B12i—B13—MgDxxvii	169.63 (8)
B12—B3—B3ii	109.21 (3)	MgDx—B13—MgDxxvii	68.35 (4)
B8viii—B3—B3ii	58.99 (2)	MgDviii—B13—MgDxxvii	128.28 (7)
B2viii—B3—B3ii	120.11 (3)	B12xvi—B14—B12	115.31 (4)
B13i—B3—B3ii	59.64 (3)	B12xvi—B14—B12xv	115.31 (4)
B12—B3—B4	67.74 (5)	B12—B14—B12xv	115.31 (4)
B8viii—B3—B4	54.79 (3)	B12xvi—B14—B13i	62.41 (4)
B2viii—B3—B4	119.05 (7)	B12—B14—B13i	62.41 (4)
B13i—B3—B4	115.90 (8)	B12xv—B14—B13i	113.02 (9)
B3ii—B3—B4	106.03 (5)	B12xvi—B14—B13xiii	113.02 (9)
B12—B3—MgDviii	111.91 (4)	B12—B14—B13xiii	62.41 (4)
B8viii—B3—MgDviii	120.43 (3)	B12xv—B14—B13xiii	62.41 (4)
B2viii—B3—MgDviii	67.17 (3)	B13i—B14—B13xiii	60.73 (9)
B13i—B3—MgDviii	59.60 (5)	B12xvi—B14—B13xxv	62.41 (4)
B3ii—B3—MgDviii	67.438 (14)	B12—B14—B13xxv	113.02 (9)
B4—B3—MgDviii	173.19 (6)	B12xv—B14—B13xxv	62.41 (4)
B12—B3—MgFix	76.64 (5)	B13i—B14—B13xxv	60.73 (9)
B8viii—B3—MgFix	61.54 (3)	B13xiii—B14—B13xxv	60.73 (9)
B2viii—B3—MgFix	101.38 (3)	B12xvi—B14—B11xv	117.69 (5)
B13i—B3—MgFix	132.10 (6)	B12—B14—B11xv	117.69 (5)
B3ii—B3—MgFix	118.66 (2)	B12xv—B14—B11xv	66.65 (4)
B4—B3—MgFix	17.68 (6)	B13i—B14—B11xv	179.67 (7)
MgDviii—B3—MgFix	168.08 (4)	B13xiii—B14—B11xv	119.00 (5)
B12—B3—MgDx	62.94 (3)	B13xxv—B14—B11xv	119.00 (5)
B8viii—B3—MgDx	171.58 (4)	B12xvi—B14—B11xvi	66.65 (4)
B2viii—B3—MgDx	67.25 (3)	B12—B14—B11xvi	117.69 (5)
B13i—B3—MgDx	68.29 (4)	B12xv—B14—B11xvi	117.69 (5)
B3ii—B3—MgDx	121.747 (19)	B13i—B14—B11xvi	119.00 (5)
B4—B3—MgDx	119.30 (4)	B13xiii—B14—B11xvi	179.67 (8)
MgDviii—B3—MgDx	64.83 (2)	B13xxv—B14—B11xvi	119.00 (5)
MgFix—B3—MgDx	114.86 (4)	B11xv—B14—B11xvi	61.27 (6)
B12—B3—MgNx	60.51 (3)	B12xvi—B14—B11	117.69 (5)
B8viii—B3—MgNx	121.91 (3)	B12—B14—B11	66.65 (4)
B2viii—B3—MgNx	69.11 (3)	B12xv—B14—B11	117.69 (5)
B13i—B3—MgNx	112.51 (4)	B13i—B14—B11	119.00 (5)
B3ii—B3—MgNx	169.708 (15)	B13xiii—B14—B11	119.00 (5)
B4—B3—MgNx	70.52 (4)	B13xxv—B14—B11	179.67 (8)
MgDviii—B3—MgNx	115.55 (2)	B11xv—B14—B11	61.27 (6)
MgFix—B3—MgNx	60.47 (3)	B11xvi—B14—B11	61.27 (6)
MgDx—B3—MgNx	55.630 (19)	B13—B15—B13xxv	180.0
MgFix—B4—B8viii	118.33 (13)	B13—B15—B13i	113.70 (9)
MgFix—B4—B4xi	5.94 (12)	B13xxv—B15—B13i	66.30 (9)
B8viii—B4—B4xi	124.26 (7)	B13—B15—B13xiii	113.70 (9)
MgFix—B4—B10i	117.38 (9)	B13xxv—B15—B13xiii	66.30 (9)
B8viii—B4—B10i	64.19 (5)	B13i—B15—B13xiii	66.30 (9)
B4xi—B4—B10i	119.25 (8)	B13—B15—B13xvi	66.30 (9)
MgFix—B4—B3	120.31 (8)	B13xxv—B15—B13xvi	113.70 (9)
B8viii—B4—B3	59.50 (5)	B13i—B15—B13xvi	113.70 (9)
B4xi—B4—B3	121.87 (8)	B13xiii—B15—B13xvi	180.00 (7)
B10i—B4—B3	112.45 (10)	B13—B15—B13xv	66.30 (9)
MgFix—B4—B11	128.71 (13)	B13xxv—B15—B13xv	113.70 (9)
B8viii—B4—B11	105.81 (11)	B13i—B15—B13xv	180.0
B4xi—B4—B11	123.93 (7)	B13xiii—B15—B13xv	113.70 (9)
B10i—B4—B11	59.96 (5)	B13xvi—B15—B13xv	66.30 (9)
B3—B4—B11	103.54 (10)	B13—B15—MgDxxviii	112.88 (2)
MgFix—B4—B12	128.43 (11)	B13xxv—B15—MgDxxviii	67.12 (2)
B8viii—B4—B12	100.79 (10)	B13i—B15—MgDxxviii	123.64 (6)
B4xi—B4—B12	123.92 (6)	B13xiii—B15—MgDxxviii	67.12 (2)
B10i—B4—B12	109.08 (10)	B13xvi—B15—MgDxxviii	112.88 (2)
B3—B4—B12	53.19 (5)	B13xv—B15—MgDxxviii	56.36 (6)
B11—B4—B12	60.10 (6)	B13—B15—MgDviii	67.12 (2)
MgFix—B4—MgN	76.30 (9)	B13xxv—B15—MgDviii	112.88 (2)
B8viii—B4—MgN	128.49 (5)	B13i—B15—MgDviii	56.36 (6)
B4xi—B4—MgN	73.12 (6)	B13xiii—B15—MgDviii	112.88 (2)
B10i—B4—MgN	65.58 (3)	B13xvi—B15—MgDviii	67.12 (2)
B3—B4—MgN	157.83 (9)	B13xv—B15—MgDviii	123.64 (6)
B11—B4—MgN	55.46 (3)	MgDxxviii—B15—MgDviii	180.00 (2)
B12—B4—MgN	105.46 (4)	B13—B15—MgDx	56.36 (6)
MgFix—B4—MgNx	72.59 (9)	B13xxv—B15—MgDx	123.64 (6)
B8viii—B4—MgNx	123.78 (5)	B13i—B15—MgDx	67.12 (2)
B4xi—B4—MgNx	69.42 (6)	B13xiii—B15—MgDx	67.12 (2)
B10i—B4—MgNx	164.11 (8)	B13xvi—B15—MgDx	112.88 (2)
B3—B4—MgNx	67.89 (3)	B13xv—B15—MgDx	112.88 (2)
B11—B4—MgNx	104.20 (4)	MgDxxviii—B15—MgDx	119.089 (4)
B12—B4—MgNx	57.55 (3)	MgDviii—B15—MgDx	60.911 (4)
MgN—B4—MgNx	107.70 (4)	B13—B15—MgDxxix	123.64 (6)
MgFix—B4—MgFxii	78.50 (14)	B13xxv—B15—MgDxxix	56.36 (6)
B8viii—B4—MgFxii	162.81 (12)	B13i—B15—MgDxxix	112.88 (2)
B4xi—B4—MgFxii	72.57 (5)	B13xiii—B15—MgDxxix	112.88 (2)
B10i—B4—MgFxii	112.77 (4)	B13xvi—B15—MgDxxix	67.12 (2)
B3—B4—MgFxii	110.31 (4)	B13xv—B15—MgDxxix	67.12 (2)
B11—B4—MgFxii	61.31 (3)	MgDxxviii—B15—MgDxxix	60.911 (4)
B12—B4—MgFxii	63.43 (3)	MgDviii—B15—MgDxxix	119.089 (4)
MgN—B4—MgFxii	55.650 (18)	MgDx—B15—MgDxxix	180.0
MgNx—B4—MgFxii	55.090 (17)	B13—B15—MgDxxx	112.88 (2)
B7—B5—B6i	123.62 (4)	B13xxv—B15—MgDxxx	67.12 (2)
B7—B5—B6xiii	123.62 (4)	B13i—B15—MgDxxx	67.12 (2)
B6i—B5—B6xiii	105.19 (6)	B13xiii—B15—MgDxxx	123.64 (6)
B7—B5—B6xiv	124.46 (6)	B13xvi—B15—MgDxxx	56.36 (6)
B6i—B5—B6xiv	58.71 (3)	B13xv—B15—MgDxxx	112.88 (2)
B6xiii—B5—B6xiv	58.71 (3)	MgDxxviii—B15—MgDxxx	119.087 (4)
B7—B5—B5xv	121.31 (3)	MgDviii—B15—MgDxxx	60.913 (4)
B6i—B5—B5xv	106.42 (3)	MgDx—B15—MgDxxx	119.087 (4)
B6xiii—B5—B5xv	59.22 (3)	MgDxxix—B15—MgDxxx	60.913 (4)
B6xiv—B5—B5xv	106.09 (3)	B13—B15—MgDxxvii	67.12 (2)
B7—B5—B5xvi	121.31 (3)	B13xxv—B15—MgDxxvii	112.88 (2)
B6i—B5—B5xvi	59.22 (3)	B13i—B15—MgDxxvii	112.88 (2)
B6xiii—B5—B5xvi	106.42 (3)	B13xiii—B15—MgDxxvii	56.36 (6)
B6xiv—B5—B5xvi	106.09 (3)	B13xvi—B15—MgDxxvii	123.64 (6)
B5xv—B5—B5xvi	60.0	B13xv—B15—MgDxxvii	67.12 (2)
B8—B6—B6xvii	122.451 (10)	MgDxxviii—B15—MgDxxvii	60.913 (4)
B8—B6—B6xviii	122.451 (10)	MgDviii—B15—MgDxxvii	119.087 (4)
B6xvii—B6—B6xviii	106.67 (5)	MgDx—B15—MgDxxvii	60.913 (4)
B8—B6—B5xiii	118.10 (5)	MgDxxix—B15—MgDxxvii	119.087 (4)
B6xvii—B6—B5xiii	61.65 (4)	MgDxxx—B15—MgDxxvii	180.0
B6xviii—B6—B5xiii	110.24 (4)	B11—MgN—B12x	119.24 (4)
B8—B6—B5i	118.10 (5)	B11—MgN—B1	118.93 (3)
B6xvii—B6—B5i	110.24 (4)	B12x—MgN—B1	115.77 (3)
B6xviii—B6—B5i	61.65 (4)	B11—MgN—B1iii	118.93 (3)
B5xiii—B6—B5i	61.56 (6)	B12x—MgN—B1iii	115.77 (3)
B8—B6—B5xix	121.78 (6)	B1—MgN—B1iii	49.37 (3)
B6xvii—B6—B5xix	59.64 (4)	B11—MgN—MgD	177.10 (4)
B6xviii—B6—B5xix	59.64 (4)	B12x—MgN—MgD	57.86 (3)
B5xiii—B6—B5xix	111.27 (5)	B1—MgN—MgD	63.62 (2)
B5i—B6—B5xix	111.27 (5)	B1iii—MgN—MgD	63.62 (2)
B8—B6—MgFxv	50.190 (19)	B11—MgN—MgE	64.09 (3)
B6xvii—B6—MgFxv	72.291 (16)	B12x—MgN—MgE	176.67 (4)
B6xviii—B6—MgFxv	148.36 (6)	B1—MgN—MgE	61.29 (3)
B5xiii—B6—MgFxv	97.17 (3)	B1iii—MgN—MgE	61.29 (3)
B5i—B6—MgFxv	149.54 (4)	MgD—MgN—MgE	118.81 (3)
B5xix—B6—MgFxv	96.33 (3)	B11—MgN—B9i	84.13 (2)
B8—B6—MgFxvii	50.190 (19)	B12x—MgN—B9i	117.75 (2)
B6xvii—B6—MgFxvii	148.36 (6)	B1—MgN—B9i	47.02 (2)
B6xviii—B6—MgFxvii	72.291 (16)	B1iii—MgN—B9i	92.73 (3)
B5xiii—B6—MgFxvii	149.54 (4)	MgD—MgN—B9i	97.25 (2)
B5i—B6—MgFxvii	97.17 (3)	MgE—MgN—B9i	61.754 (19)
B5xix—B6—MgFxvii	96.33 (3)	B11—MgN—B9xiii	84.13 (2)
MgFxv—B6—MgFxvii	92.16 (3)	B12x—MgN—B9xiii	117.76 (2)
B1xiii—B7—B1xx	61.48 (5)	B1—MgN—B9xiii	92.73 (3)
B1xiii—B7—B5	120.12 (5)	B1iii—MgN—B9xiii	47.02 (2)
B1xx—B7—B5	120.12 (5)	MgD—MgN—B9xiii	97.25 (2)
B1xiii—B7—B9xxi	112.88 (5)	MgE—MgN—B9xiii	61.75 (2)
B1xx—B7—B9xxi	112.88 (5)	B9i—MgN—B9xiii	121.67 (4)
B5—B7—B9xxi	117.39 (5)	B11—MgN—B10i	46.85 (2)
B1xiii—B7—B2xx	111.52 (4)	B12x—MgN—B10i	118.88 (2)
B1xx—B7—B2xx	60.55 (3)	B1—MgN—B10i	84.46 (2)
B5—B7—B2xx	118.63 (3)	B1iii—MgN—B10i	119.73 (3)
B9xxi—B7—B2xx	63.45 (3)	MgD—MgN—B10i	133.77 (2)
B1xiii—B7—B2xiii	60.55 (3)	MgE—MgN—B10i	63.11 (2)
B1xx—B7—B2xiii	111.52 (4)	B9i—MgN—B10i	39.60 (2)
B5—B7—B2xiii	118.63 (3)	B9xiii—MgN—B10i	117.92 (3)
B9xxi—B7—B2xiii	63.45 (3)	B11—MgN—B10xiii	46.85 (2)
B2xx—B7—B2xiii	114.24 (6)	B12x—MgN—B10xiii	118.88 (2)
B4xxii—B8—B4v	116.74 (11)	B1—MgN—B10xiii	119.73 (3)
B4xxii—B8—B6	113.05 (7)	B1iii—MgN—B10xiii	84.46 (2)
B4v—B8—B6	113.05 (7)	MgD—MgN—B10xiii	133.77 (2)
B4xxii—B8—B3xxii	65.71 (4)	MgE—MgN—B10xiii	63.11 (2)
B4v—B8—B3xxii	117.78 (7)	B9i—MgN—B10xiii	117.92 (3)
B6—B8—B3xxii	122.01 (5)	B9xiii—MgN—B10xiii	39.60 (2)
B4xxii—B8—B3v	117.78 (7)	B10i—MgN—B10xiii	90.36 (4)
B4v—B8—B3v	65.71 (4)	B11—MgN—MgFix	64.45 (2)
B6—B8—B3v	122.01 (5)	B12x—MgN—MgFix	65.47 (2)
B3xxii—B8—B3v	62.03 (4)	B1—MgN—MgFix	122.12 (3)
B4xxii—B8—B10x	62.12 (4)	B1iii—MgN—MgFix	171.44 (4)
B4v—B8—B10x	62.12 (4)	MgD—MgN—MgFix	113.23 (2)
B6—B8—B10x	111.38 (5)	MgE—MgN—MgFix	117.17 (3)
B3xxii—B8—B10x	115.72 (5)	B9i—MgN—MgFix	79.61 (3)
B3v—B8—B10x	115.72 (5)	B9xiii—MgN—MgFix	140.86 (4)
B4xxii—B8—MgFxvii	130.76 (6)	B10i—MgN—MgFix	55.88 (2)
B4v—B8—MgFxvii	19.76 (7)	B10xiii—MgN—MgFix	102.45 (3)
B6—B8—MgFxvii	93.38 (4)	B11—MgN—MgFxii	64.45 (2)
B3xxii—B8—MgFxvii	133.21 (5)	B12x—MgN—MgFxii	65.47 (2)
B3v—B8—MgFxvii	73.74 (3)	B1—MgN—MgFxii	171.44 (4)
B10x—B8—MgFxvii	69.85 (2)	B1iii—MgN—MgFxii	122.11 (3)
B4xxii—B8—MgFxv	19.76 (7)	MgD—MgN—MgFxii	113.23 (2)
B4v—B8—MgFxv	130.76 (6)	MgE—MgN—MgFxii	117.17 (3)
B6—B8—MgFxv	93.38 (4)	B9i—MgN—MgFxii	140.86 (4)
B3xxii—B8—MgFxv	73.75 (3)	B9xiii—MgN—MgFxii	79.61 (3)
B3v—B8—MgFxv	133.21 (5)	B10i—MgN—MgFxii	102.45 (3)
B10x—B8—MgFxv	69.85 (2)	B10xiii—MgN—MgFxii	55.88 (3)
MgFxvii—B8—MgFxv	138.80 (4)	MgFix—MgN—MgFxii	66.38 (6)
B10—B9—B7xxi	115.70 (6)	B13x—MgD—B12x	114.60 (5)
B10—B9—B2xxiii	119.39 (3)	B13x—MgD—B2iii	87.88 (3)
B7xxi—B9—B2xxiii	58.63 (3)	B12x—MgD—B2iii	126.690 (19)
B10—B9—B2xxiv	119.39 (3)	B13x—MgD—B2	87.87 (3)
B7xxi—B9—B2xxiv	58.63 (3)	B12x—MgD—B2	126.688 (19)
B2xxiii—B9—B2xxiv	106.56 (5)	B2iii—MgD—B2	100.24 (3)
B10—B9—B1xiii	127.63 (5)	B13x—MgD—MgN	174.71 (5)
B7xxi—B9—B1xiii	108.72 (5)	B12x—MgD—MgN	60.12 (3)
B2xxiii—B9—B1xiii	63.89 (3)	B2iii—MgD—MgN	95.50 (2)
B2xxiv—B9—B1xiii	106.56 (4)	B2—MgD—MgN	95.50 (2)
B10—B9—B1xx	127.63 (5)	B13x—MgD—B3xxii	46.76 (4)
B7xxi—B9—B1xx	108.72 (5)	B12x—MgD—B3xxii	148.02 (3)
B2xxiii—B9—B1xx	106.56 (4)	B2iii—MgD—B3xxii	44.26 (2)
B2xxiv—B9—B1xx	63.89 (3)	B2—MgD—B3xxii	82.68 (2)
B1xiii—B9—B1xx	53.79 (4)	MgN—MgD—B3xxii	137.67 (3)
B10—B9—MgNxiii	70.21 (3)	B13x—MgD—B3v	46.76 (4)
B7xxi—B9—MgNxiii	123.97 (2)	B12x—MgD—B3v	148.01 (3)
B2xxiii—B9—MgNxiii	70.30 (2)	B2iii—MgD—B3v	82.69 (2)
B2xxiv—B9—MgNxiii	168.97 (5)	B2—MgD—B3v	44.26 (2)
B1xiii—B9—MgNxiii	62.45 (3)	MgN—MgD—B3v	137.67 (3)
B1xx—B9—MgNxiii	106.35 (4)	B3xxii—MgD—B3v	45.13 (3)
B10—B9—MgNi	70.21 (3)	B13x—MgD—B2iv	114.786 (18)
B7xxi—B9—MgNi	123.96 (2)	B12x—MgD—B2iv	83.08 (2)
B2xxiii—B9—MgNi	168.97 (5)	B2iii—MgD—B2iv	132.27 (3)
B2xxiv—B9—MgNi	70.30 (2)	B2—MgD—B2iv	44.13 (3)
B1xiii—B9—MgNi	106.35 (4)	MgN—MgD—B2iv	65.670 (17)
B1xx—B9—MgNi	62.45 (2)	B3xxii—MgD—B2iv	126.73 (2)
MgNxiii—B9—MgNi	110.67 (4)	B3v—MgD—B2iv	84.42 (2)
B10—B9—MgExxv	72.18 (5)	B13x—MgD—B2xxxi	114.788 (17)
B7xxi—B9—MgExxv	172.12 (5)	B12x—MgD—B2xxxi	83.09 (2)
B2xxiii—B9—MgExxv	118.38 (3)	B2iii—MgD—B2xxxi	44.13 (3)
B2xxiv—B9—MgExxv	118.38 (3)	B2—MgD—B2xxxi	132.27 (3)
B1xiii—B9—MgExxv	64.40 (4)	MgN—MgD—B2xxxi	65.671 (17)
B1xx—B9—MgExxv	64.40 (4)	B3xxii—MgD—B2xxxi	84.42 (2)
MgNxiii—B9—MgExxv	57.40 (2)	B3v—MgD—B2xxxi	126.73 (2)
MgNi—B9—MgExxv	57.40 (2)	B2iv—MgD—B2xxxi	129.90 (4)
B9—B10—B4xx	122.86 (7)	B13x—MgD—B13xxxii	74.41 (7)
B9—B10—B4xiii	122.86 (7)	B12x—MgD—B13xxxii	45.88 (4)
B4xx—B10—B4xiii	101.83 (10)	B2iii—MgD—B13xxxii	105.88 (4)
B9—B10—B8x	129.29 (6)	B2—MgD—B13xxxii	147.57 (5)
B4xx—B10—B8x	53.69 (3)	MgN—MgD—B13xxxii	100.70 (4)
B4xiii—B10—B8x	53.69 (3)	B3xxii—MgD—B13xxxii	102.92 (4)
B9—B10—B11xiii	123.43 (5)	B3v—MgD—B13xxxii	120.58 (4)
B4xx—B10—B11xiii	107.57 (7)	B2iv—MgD—B13xxxii	120.15 (4)
B4xiii—B10—B11xiii	62.05 (5)	B2xxxi—MgD—B13xxxii	80.14 (4)
B8x—B10—B11xiii	99.81 (4)	B13x—MgD—B13v	74.41 (7)
B9—B10—B11i	123.43 (5)	B12x—MgD—B13v	45.88 (4)
B4xx—B10—B11i	62.05 (5)	B2iii—MgD—B13v	147.58 (5)
B4xiii—B10—B11i	107.57 (7)	B2—MgD—B13v	105.88 (4)
B8x—B10—B11i	99.81 (4)	MgN—MgD—B13v	100.70 (4)
B11xiii—B10—B11i	59.53 (6)	B3xxii—MgD—B13v	120.58 (4)
B9—B10—MgFxxiv	104.31 (3)	B3v—MgD—B13v	102.92 (4)
B4xx—B10—MgFxxiv	114.64 (5)	B2iv—MgD—B13v	80.14 (4)
B4xiii—B10—MgFxxiv	18.67 (6)	B2xxxi—MgD—B13v	120.15 (4)
B8x—B10—MgFxxiv	61.81 (3)	B13xxxii—MgD—B13v	43.64 (8)
B11xiii—B10—MgFxxiv	72.62 (5)	B13x—MgD—B3x	110.61 (4)
B11i—B10—MgFxxiv	125.02 (5)	B12x—MgD—B3x	43.372 (16)
B9—B10—MgFxxvi	104.31 (3)	B2iii—MgD—B3x	84.05 (2)
B4xx—B10—MgFxxvi	18.67 (6)	B2—MgD—B3x	161.26 (3)
B4xiii—B10—MgFxxvi	114.64 (5)	MgN—MgD—B3x	65.84 (2)
B8x—B10—MgFxxvi	61.81 (3)	B3xxii—MgD—B3x	111.948 (17)
B11xiii—B10—MgFxxvi	125.02 (5)	B3v—MgD—B3x	154.04 (3)
B11i—B10—MgFxxvi	72.62 (5)	B2iv—MgD—B3x	120.70 (3)
MgFxxiv—B10—MgFxxvi	123.00 (7)	B2xxxi—MgD—B3x	43.13 (2)
B9—B10—MgNxiii	70.19 (3)	B13xxxii—MgD—B3x	43.36 (4)
B4xx—B10—MgNxiii	165.69 (7)	B13v—MgD—B3x	77.40 (4)
B4xiii—B10—MgNxiii	72.08 (4)	MgN—MgE—MgNxv	116.996 (14)
B8x—B10—MgNxiii	124.636 (18)	MgN—MgE—MgNxvi	116.996 (14)
B11xiii—B10—MgNxiii	58.12 (3)	MgNxv—MgE—MgNxvi	116.996 (14)
B11i—B10—MgNxiii	106.76 (4)	MgN—MgE—B1xxxiii	141.06 (3)
MgFxxiv—B10—MgNxiii	63.10 (3)	MgNxv—MgE—B1xxxiii	58.125 (18)
MgFxxvi—B10—MgNxiii	173.22 (4)	MgNxvi—MgE—B1xxxiii	95.06 (2)
B9—B10—MgNi	70.19 (3)	MgN—MgE—B1xvi	141.06 (3)
B4xx—B10—MgNi	72.08 (4)	MgNxv—MgE—B1xvi	95.06 (2)
B4xiii—B10—MgNi	165.69 (7)	MgNxvi—MgE—B1xvi	58.125 (18)
B8x—B10—MgNi	124.633 (19)	B1xxxiii—MgE—B1xvi	42.37 (3)
B11xiii—B10—MgNi	106.76 (4)	MgN—MgE—B1xv	95.06 (2)
B11i—B10—MgNi	58.12 (3)	MgNxv—MgE—B1xv	58.125 (18)
MgFxxiv—B10—MgNi	173.22 (3)	MgNxvi—MgE—B1xv	141.06 (3)
MgFxxvi—B10—MgNi	63.10 (3)	B1xxxiii—MgE—B1xv	47.71 (3)
MgNxiii—B10—MgNi	110.64 (4)	B1xvi—MgE—B1xv	83.14 (3)
B9—B10—MgExxv	68.99 (4)	MgN—MgE—B1	58.125 (18)
B4xx—B10—MgExxv	119.62 (3)	MgNxv—MgE—B1	141.06 (3)
B4xiii—B10—MgExxv	119.62 (3)	MgNxvi—MgE—B1	95.06 (2)
B8x—B10—MgExxv	161.71 (5)	B1xxxiii—MgE—B1	99.95 (4)
B11xiii—B10—MgExxv	64.60 (3)	B1xvi—MgE—B1	83.14 (3)
B11i—B10—MgExxv	64.60 (4)	B1xv—MgE—B1	83.14 (3)
MgFxxiv—B10—MgExxv	118.01 (4)	MgN—MgE—B1ii	95.06 (2)
MgFxxvi—B10—MgExxv	118.01 (4)	MgNxv—MgE—B1ii	141.06 (3)
MgNxiii—B10—MgExxv	56.760 (19)	MgNxvi—MgE—B1ii	58.125 (18)
MgNi—B10—MgExxv	56.760 (19)	B1xxxiii—MgE—B1ii	83.14 (3)
B14—B11—B11xv	59.37 (3)	B1xvi—MgE—B1ii	47.71 (3)
B14—B11—B11xvi	59.37 (3)	B1xv—MgE—B1ii	99.95 (4)
B11xv—B11—B11xvi	60.0	B1—MgE—B1ii	42.37 (3)
B14—B11—B10i	104.96 (3)	MgN—MgE—B1iii	58.125 (18)
B11xv—B11—B10i	116.29 (3)	MgNxv—MgE—B1iii	95.06 (2)
B11xvi—B11—B10i	60.24 (3)	MgNxvi—MgE—B1iii	141.06 (3)
B14—B11—B10xiii	104.96 (3)	B1xxxiii—MgE—B1iii	83.14 (3)
B11xv—B11—B10xiii	60.24 (3)	B1xvi—MgE—B1iii	99.95 (4)
B11xvi—B11—B10xiii	116.29 (3)	B1xv—MgE—B1iii	42.37 (3)
B10i—B11—B10xiii	139.88 (6)	B1—MgE—B1iii	47.71 (3)
B14—B11—B4	101.71 (6)	B1ii—MgE—B1iii	83.14 (3)
B11xv—B11—B4	159.56 (6)	MgN—MgE—B11	53.72 (3)
B11xvi—B11—B4	104.99 (5)	MgNxv—MgE—B11	93.44 (3)
B10i—B11—B4	57.99 (3)	MgNxvi—MgE—B11	93.44 (3)
B10xiii—B11—B4	138.11 (7)	B1xxxiii—MgE—B11	151.02 (3)
B14—B11—B4iii	101.71 (6)	B1xvi—MgE—B11	151.02 (3)
B11xv—B11—B4iii	104.99 (5)	B1xv—MgE—B11	124.451 (19)
B11xvi—B11—B4iii	159.56 (6)	B1—MgE—B11	106.82 (2)
B10i—B11—B4iii	138.11 (7)	B1ii—MgE—B11	124.451 (19)
B10xiii—B11—B4iii	57.99 (3)	B1iii—MgE—B11	106.82 (2)
B4—B11—B4iii	85.45 (7)	MgN—MgE—B11xvi	93.44 (3)
B14—B11—B12	54.95 (4)	MgNxv—MgE—B11xvi	93.44 (3)
B11xv—B11—B12	106.29 (3)	MgNxvi—MgE—B11xvi	53.72 (3)
B11xvi—B11—B12	106.29 (3)	B1xxxiii—MgE—B11xvi	124.451 (19)
B10i—B11—B12	109.46 (3)	B1xvi—MgE—B11xvi	106.82 (2)
B10xiii—B11—B12	109.46 (3)	B1xv—MgE—B11xvi	151.02 (3)
B4—B11—B12	62.52 (4)	B1—MgE—B11xvi	124.451 (19)
B4iii—B11—B12	62.52 (4)	B1ii—MgE—B11xvi	106.82 (2)
B14—B11—MgN	179.96 (4)	B1iii—MgE—B11xvi	151.02 (3)
B11xv—B11—MgN	120.61 (2)	B11—MgE—B11xvi	44.94 (4)
B11xvi—B11—MgN	120.61 (2)	MgN—MgE—B11xv	93.44 (3)
B10i—B11—MgN	75.04 (3)	MgNxv—MgE—B11xv	53.72 (3)
B10xiii—B11—MgN	75.04 (3)	MgNxvi—MgE—B11xv	93.44 (3)
B4—B11—MgN	78.32 (6)	B1xxxiii—MgE—B11xv	106.82 (2)
B4iii—B11—MgN	78.32 (6)	B1xvi—MgE—B11xv	124.451 (19)
B12—B11—MgN	125.09 (5)	B1xv—MgE—B11xv	106.82 (2)
B14—B11—MgE	117.77 (5)	B1—MgE—B11xv	151.02 (3)
B11xv—B11—MgE	67.529 (18)	B1ii—MgE—B11xv	151.02 (3)
B11xvi—B11—MgE	67.529 (18)	B1iii—MgE—B11xv	124.451 (19)
B10i—B11—MgE	71.32 (3)	B11—MgE—B11xv	44.94 (4)
B10xiii—B11—MgE	71.32 (3)	B11xvi—MgE—B11xv	44.94 (4)
B4—B11—MgE	122.02 (4)	B4ix—MgF—B4xxxiv	168.1 (2)
B4iii—B11—MgE	122.02 (4)	B4ix—MgF—B8xviii	41.91 (9)
B12—B11—MgE	172.71 (5)	B4xxxiv—MgF—B8xviii	149.94 (15)
MgN—B11—MgE	62.20 (3)	B4ix—MgF—B8xvi	149.94 (15)
B14—B11—MgFix	115.56 (4)	B4xxxiv—MgF—B8xvi	41.91 (9)
B11xv—B11—MgFix	174.67 (2)	B8xviii—MgF—B8xvi	108.26 (8)
B11xvi—B11—MgFix	116.63 (3)	B4ix—MgF—B10xxx	138.86 (5)
B10i—B11—MgFix	62.39 (4)	B4xxxiv—MgF—B10xxx	43.94 (5)
B10xiii—B11—MgFix	124.40 (5)	B8xviii—MgF—B10xxx	118.52 (6)
B4—B11—MgFix	15.14 (6)	B8xvi—MgF—B10xxx	48.34 (3)
B4iii—B11—MgFix	77.15 (5)	B4ix—MgF—B10vi	43.94 (5)
B12—B11—MgFix	70.17 (3)	B4xxxiv—MgF—B10vi	138.86 (5)
MgN—B11—MgFix	64.47 (3)	B8xviii—MgF—B10vi	48.34 (3)
MgE—B11—MgFix	115.69 (3)	B8xvi—MgF—B10vi	118.52 (6)
B14—B11—MgFxii	115.56 (4)	B10xxx—MgF—B10vi	161.61 (9)
B11xv—B11—MgFxii	116.63 (3)	B4ix—MgF—B3xxxiv	140.10 (5)
B11xvi—B11—MgFxii	174.67 (2)	B4xxxiv—MgF—B3xxxiv	42.02 (5)
B10i—B11—MgFxii	124.40 (5)	B8xviii—MgF—B3xxxiv	124.98 (6)
B10xiii—B11—MgFxii	62.38 (4)	B8xvi—MgF—B3xxxiv	44.71 (3)
B4—B11—MgFxii	77.15 (5)	B10xxx—MgF—B3xxxiv	80.62 (2)
B4iii—B11—MgFxii	15.14 (6)	B10vi—MgF—B3xxxiv	97.21 (3)
B12—B11—MgFxii	70.17 (3)	B4ix—MgF—B3ix	42.02 (5)
MgN—B11—MgFxii	64.47 (3)	B4xxxiv—MgF—B3ix	140.10 (5)
MgE—B11—MgFxii	115.69 (3)	B8xviii—MgF—B3ix	44.71 (3)
MgFix—B11—MgFxii	66.39 (7)	B8xvi—MgF—B3ix	124.98 (6)
B3—B12—B3iii	146.17 (6)	B10xxx—MgF—B3ix	97.21 (3)
B3—B12—B14	102.69 (3)	B10vi—MgF—B3ix	80.62 (2)
B3iii—B12—B14	102.69 (3)	B3xxxiv—MgF—B3ix	166.54 (8)
B3—B12—B13i	60.28 (6)	B4ix—MgF—B11ix	36.14 (8)
B3iii—B12—B13i	116.54 (6)	B4xxxiv—MgF—B11ix	133.97 (13)
B14—B12—B13i	59.73 (6)	B8xviii—MgF—B11ix	74.07 (2)
B3—B12—B13xiii	116.54 (6)	B8xvi—MgF—B11ix	156.36 (3)
B3iii—B12—B13xiii	60.28 (6)	B10xxx—MgF—B11ix	151.91 (6)
B14—B12—B13xiii	59.73 (6)	B10vi—MgF—B11ix	44.99 (2)
B13i—B12—B13xiii	59.03 (10)	B3xxxiv—MgF—B11ix	113.96 (3)
B3—B12—B11	106.11 (3)	B3ix—MgF—B11ix	73.87 (3)
B3iii—B12—B11	106.11 (3)	B4ix—MgF—B11xxxv	133.97 (13)
B14—B12—B11	58.40 (6)	B4xxxiv—MgF—B11xxxv	36.14 (8)
B13i—B12—B11	109.88 (5)	B8xviii—MgF—B11xxxv	156.36 (3)
B13xiii—B12—B11	109.88 (5)	B8xvi—MgF—B11xxxv	74.07 (2)
B3—B12—B4	59.07 (3)	B10xxx—MgF—B11xxxv	44.99 (2)
B3iii—B12—B4	135.93 (6)	B10vi—MgF—B11xxxv	151.91 (6)
B14—B12—B4	100.36 (6)	B3xxxiv—MgF—B11xxxv	73.87 (3)
B13i—B12—B4	107.50 (6)	B3ix—MgF—B11xxxv	113.96 (3)
B13xiii—B12—B4	159.29 (8)	B11ix—MgF—B11xxxv	113.61 (7)
B11—B12—B4	57.38 (4)	B4ix—MgF—MgNix	84.73 (8)
B3—B12—B4iii	135.93 (6)	B4xxxiv—MgF—MgNix	88.78 (8)
B3iii—B12—B4iii	59.07 (3)	B8xviii—MgF—MgNix	109.16 (2)
B14—B12—B4iii	100.36 (6)	B8xvi—MgF—MgNix	108.26 (2)
B13i—B12—B4iii	159.29 (8)	B10xxx—MgF—MgNix	131.26 (4)
B13xiii—B12—B4iii	107.50 (6)	B10vi—MgF—MgNix	61.02 (2)
B11—B12—B4iii	57.38 (4)	B3xxxiv—MgF—MgNix	63.62 (2)
B4—B12—B4iii	80.20 (6)	B3ix—MgF—MgNix	124.93 (4)
B3—B12—MgDx	73.69 (3)	B11ix—MgF—MgNix	51.08 (3)
B3iii—B12—MgDx	73.69 (3)	B11xxxv—MgF—MgNix	91.66 (4)
B14—B12—MgDx	123.91 (6)	B4ix—MgF—MgNxxxv	88.78 (8)
B13i—B12—MgDx	72.09 (5)	B4xxxiv—MgF—MgNxxxv	84.72 (8)
B13xiii—B12—MgDx	72.09 (5)	B8xviii—MgF—MgNxxxv	108.26 (2)
B11—B12—MgDx	177.69 (5)	B8xvi—MgF—MgNxxxv	109.16 (2)
B4—B12—MgDx	121.11 (4)	B10xxx—MgF—MgNxxxv	61.02 (2)
B4iii—B12—MgDx	121.11 (4)	B10vi—MgF—MgNxxxv	131.26 (4)
B3—B12—MgNx	78.53 (3)	B3xxxiv—MgF—MgNxxxv	124.93 (4)
B3iii—B12—MgNx	78.53 (3)	B3ix—MgF—MgNxxxv	63.62 (2)
B14—B12—MgNx	174.07 (6)	B11ix—MgF—MgNxxxv	91.66 (4)
B13i—B12—MgNx	125.07 (6)	B11xxxv—MgF—MgNxxxv	51.07 (3)
B13xiii—B12—MgNx	125.08 (6)	MgNix—MgF—MgNxxxv	113.62 (6)