Literature DB >> 22719275

Na(7)Mg(13)Nd(PO(4))(12).

Hasna Jerbi1, Mourad Hidouri, Ben Amara Mongi.   

Abstract

Investigations of the quasi-ternary system Na(3)PO(4)-Mg(3)(PO(4))(2)-NdPO(4) allowed us to obtain the new phosphate hepta-sodium trideca-magnesium neodymium dodeca-kis-phosphate, Na(7)Mg(13)Nd(PO(4))(12), by applying a flux method. The crystal structure is isotypic with that of the previously reported Na(7)Mg(13)Ln(PO(4))(12) (Ln = Eu, La) compounds. It consists of a complex three-dimensional framework built up from an NdO(8) polyhedron (m symmetry), an MO(6) octa-hedron statistically occupied by M = Mg and Na, and eight MgO(x) (x = 5, 6) polyhedra (four with site symmetry m), linked either directely by sharing corners, edges and faces, or by one of the eight unique PO(4) tetra-hedra through common corners. Two of the PO(4) tetra-hedra are statisticaly disordered over a mirror plane. The whole structure can be described as resutling from an assembly of two types of structural units, viz [Mg(4)MP(4)O(22)](∞) (2) layers extending parallel to (100) and stacked along [100], and [Mg(4)NdP(4)O(36)](∞) (1) undulating chains running along the [010] direction. The six different Na(+) cations (five with site symmetry m and one with 0.5 occupancy) are situated in six distinct cavities delimited by the framework. The structure was refined from data of a racemic twin.

Entities:  

Year:  2012        PMID： 22719275      PMCID： PMC3379054          DOI： 10.1107/S1600536812017850

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN： 1600-5368


Related literature

For the synthesis and luminescent properties of new phosphates for optical devices, see: Ngee et al. (2009 ▶); Shinde et al. (2011 ▶). The title structure is isotypic with Na7Mg13 Ln(PO4)12 (Ln = La, Eu) (Jerbi et al., 2010 ▶). For P—O distances in orthophosphates, see: Baur (1974 ▶). For Mg—O distances, see: Ben Amara et al. (1983 ▶); Jaulmes et al. (1997 ▶); Klevtsova et al. (1980 ▶), For Na—O distances, see: Donnay & Allmann (1970 ▶), and for Nd—O distances, see: Albrand et al. (1974 ▶).

Experimental

Crystal data

Na7Mg13Nd(PO4)12 M = 1760.84 Orthorhombic, a = 10.301 (3) Å b = 15.461 (4) Å c = 23.384 (6) Å V = 3724.2 (17) Å3 Z = 4 Mo Kα radiation μ = 2.38 mm−1 T = 293 K 0.40 × 0.22 × 0.17 mm

Data collection

Bruker–Nonius KappaCCD diffractometer Absorption correction: analytical (Alcock, 1970 ▶) T min = 0.716, T max = 0.878 44522 measured reflections 11948 independent reflections 8244 reflections with I > 2σ(I) R int = 0.103

Refinement

R[F 2 > 2σ(F 2)] = 0.057 wR(F 2) = 0.107 S = 1.05 11948 reflections 424 parameters 1 restraint Δρmax = 2.37 e Å−3 Δρmin = −2.23 e Å−3 Absolute structure: Flack (1983 ▶), 5847 Friedel pairs Flack parameter: 0.257 (9) Data collection: COLLECT (Nonius, 1998 ▶); cell refinement: SCALEPACK (Otwinowski & Minor, 1997 ▶); data reduction: SCALEPACK and DENZO (Otwinowski & Minor, 1997 ▶); program(s) used to solve structure: SIR92 (Altomare et al., 1993 ▶); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 ▶); molecular graphics: DIAMOND (Brandenburg, 1998 ▶); software used to prepare material for publication: SHELXL97. Crystal structure: contains datablock(s) global, I. DOI: 10.1107/S1600536812017850/wm2593sup1.cif Structure factors: contains datablock(s) I. DOI: 10.1107/S1600536812017850/wm2593Isup2.hkl Additional supplementary materials: crystallographic information; 3D view; checkCIF report
Na7Mg13Nd(PO4)12Dx = 3.140 Mg m−3
Mr = 1760.84Melting point: 1007 K
Orthorhombic, Cmc21Mo Kα radiation, λ = 0.71069 Å
Hall symbol: C 2c -2Cell parameters from 44599 reflections
a = 10.301 (3) Åθ = 2.4–40°
b = 15.461 (4) ŵ = 2.38 mm−1
c = 23.384 (6) ÅT = 293 K
V = 3724.2 (17) Å3Parallelepiped, purple
Z = 40.40 × 0.22 × 0.17 mm
F(000) = 3428
Bruker–Nonius KappaCCD diffractometer11948 independent reflections
Radiation source: fine-focus sealed tube8244 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.103
non–profiled ω scansθmax = 40.0°, θmin = 3.2°
Absorption correction: analytical (Alcock, 1970)h = −12→18
Tmin = 0.716, Tmax = 0.878k = −27→27
44522 measured reflectionsl = −42→42
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.057w = 1/[σ2(Fo2) + (0.0124P)2 + 42.9558P] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.107(Δ/σ)max = 0.001
S = 1.05Δρmax = 2.37 e Å−3
11948 reflectionsΔρmin = −2.23 e Å−3
424 parametersAbsolute structure: Flack (1983), 5847 Friedel pairs
1 restraintFlack parameter: 0.257 (9)
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.
xyzUiso*/UeqOcc. (<1)
Nd0.00000.54408 (2)0.000015 (13)0.00904 (5)
P10.21976 (9)0.43115 (7)0.05989 (4)0.00612 (16)
O110.1824 (3)0.3576 (2)0.09995 (13)0.0116 (6)
O120.3671 (3)0.4462 (2)0.05621 (14)0.0129 (6)
O130.1558 (3)0.41806 (18)0.00077 (17)0.0125 (5)
O140.1526 (3)0.5162 (2)0.08102 (14)0.0112 (5)
P20.74694 (10)0.46442 (7)0.22216 (5)0.00978 (18)
O210.7715 (4)0.5517 (2)0.19519 (16)0.0232 (8)
O220.7106 (3)0.4816 (2)0.28494 (15)0.0191 (7)
O230.6391 (3)0.4113 (2)0.19233 (14)0.0125 (6)
O240.8668 (3)0.4038 (2)0.21746 (13)0.0107 (5)
P30.24602 (11)0.70154 (7)0.98592 (4)0.00913 (18)
O310.2995 (3)0.6688 (2)0.04252 (14)0.0168 (7)
O320.1777 (4)0.6272 (2)0.95352 (15)0.0170 (7)
O330.3605 (3)0.7387 (2)0.95155 (16)0.0153 (6)
O340.1511 (3)0.7784 (2)0.98766 (14)0.0160 (7)
P40.23934 (11)0.72710 (8)0.81954 (5)0.0116 (2)
O410.3634 (4)0.6820 (3)0.8390 (2)0.0337 (12)
O420.2489 (5)0.7603 (3)0.75815 (16)0.0286 (9)
O430.1310 (3)0.6600 (2)0.82915 (14)0.0143 (6)
O440.2043 (4)0.8076 (2)0.85537 (15)0.0210 (8)
P50.00000.72322 (10)0.11586 (7)0.0069 (3)
O510.00000.6619 (3)0.0654 (2)0.0144 (8)
O520.00000.8177 (3)0.09809 (19)0.0105 (8)
O530.1213 (3)0.7066 (2)0.15281 (15)0.0132 (6)
P60.50000.64818 (10)0.16991 (6)0.0060 (2)
O610.6206 (3)0.7003 (2)0.15437 (17)0.0180 (7)
O620.50000.5682 (3)0.1316 (2)0.0294 (14)
O630.50000.6231 (4)0.2330 (2)0.0169 (10)
P70.02504 (19)0.55827 (15)0.36368 (10)0.0078 (5)0.50
O710.00000.5300 (3)0.3018 (2)0.0166 (9)
O72X−0.020 (3)0.6490 (5)0.3742 (4)0.037 (6)0.50
O73X0.0621 (7)0.4980 (6)0.3999 (3)0.0252 (18)0.50
O74X0.1652 (7)0.5446 (5)0.3848 (3)0.0177 (12)*0.50
P80.5147 (8)0.53079 (15)0.39974 (9)0.0120 (12)0.50
O810.50000.5645 (4)0.3388 (2)0.0255 (13)
O82X0.4470 (6)0.5929 (4)0.4417 (3)0.0130 (12)0.50
O83X0.3373 (6)0.5306 (4)0.4107 (3)0.0141 (12)0.50
O84X0.5429 (8)0.4411 (6)0.4069 (4)0.037 (2)*0.50
Mg10.00000.40172 (15)0.28024 (9)0.0100 (4)
Mg20.50000.43819 (13)0.13099 (9)0.0072 (4)
Mg30.00000.85120 (14)0.01707 (9)0.0082 (4)
Mg40.00000.78245 (17)0.39476 (10)0.0115 (4)
Mg50.76130 (15)0.29805 (10)0.17575 (7)0.0091 (3)
Mg60.2319 (3)0.63904 (12)0.43096 (8)0.0284 (5)
Mg70.34561 (18)0.60958 (11)0.28670 (8)0.0187 (4)
Mg80.24440 (18)0.61726 (10)0.11851 (7)0.0155 (3)
Mg0.2460 (2)0.56877 (13)0.87518 (8)0.0254 (5)0.50
Na0.2460 (2)0.56877 (13)0.87518 (8)0.0254 (5)0.50
Na10.00000.0937 (2)0.78091 (13)0.0195 (6)
Na20.00000.2634 (2)0.40137 (14)0.0226 (7)
Na30.00000.4531 (3)0.14512 (14)0.0235 (8)
Na40.50000.4330 (2)0.52265 (14)0.0230 (6)
Na50.50000.7765 (2)0.05347 (18)0.0352 (9)
Na60.9685 (5)0.6495 (4)0.2386 (2)0.0455 (19)0.50
U11U22U33U12U13U23
Nd0.00955 (11)0.00944 (11)0.00815 (11)0.0000.0000.00003 (13)
P10.0045 (4)0.0058 (4)0.0080 (4)−0.0004 (3)−0.0007 (3)0.0007 (3)
O110.0116 (14)0.0103 (14)0.0129 (14)−0.0008 (11)−0.0013 (11)0.0024 (11)
O120.0077 (12)0.0131 (15)0.0180 (14)0.0004 (10)−0.0045 (11)0.0040 (12)
O130.0140 (12)0.0133 (12)0.0101 (11)0.0056 (9)−0.0042 (14)−0.0014 (15)
O140.0107 (13)0.0078 (12)0.0152 (14)0.0017 (10)0.0009 (11)−0.0026 (11)
P20.0077 (4)0.0110 (5)0.0107 (4)0.0020 (4)0.0012 (3)0.0015 (4)
O210.032 (2)0.0138 (16)0.0238 (18)−0.0055 (15)−0.0075 (15)0.0097 (14)
O220.0187 (16)0.0227 (18)0.0158 (16)0.0043 (13)0.0081 (13)−0.0005 (14)
O230.0083 (13)0.0147 (15)0.0146 (15)0.0024 (11)0.0001 (10)0.0006 (12)
O240.0075 (12)0.0174 (14)0.0073 (12)0.0037 (11)0.0006 (10)0.0014 (11)
P30.0102 (4)0.0082 (4)0.0090 (4)−0.0014 (3)0.0035 (4)0.0002 (3)
O310.0216 (17)0.0185 (16)0.0102 (14)−0.0027 (13)0.0001 (12)0.0042 (12)
O320.0230 (17)0.0127 (15)0.0152 (15)−0.0051 (13)−0.0003 (13)−0.0008 (12)
O330.0140 (14)0.0133 (15)0.0187 (15)0.0007 (12)0.0105 (12)0.0022 (12)
O340.0102 (13)0.0164 (15)0.0213 (17)0.0026 (11)0.0038 (11)−0.0065 (12)
P40.0090 (4)0.0146 (5)0.0113 (5)0.0012 (4)−0.0023 (4)−0.0070 (4)
O410.0142 (16)0.044 (3)0.043 (2)0.0165 (17)−0.0161 (17)−0.036 (2)
O420.041 (2)0.031 (2)0.0138 (18)−0.0208 (19)0.0055 (17)−0.0077 (15)
O430.0123 (13)0.0217 (17)0.0088 (13)−0.0002 (12)−0.0021 (11)−0.0017 (12)
O440.028 (2)0.0195 (18)0.0151 (16)0.0066 (15)−0.0036 (14)−0.0102 (13)
P50.0079 (6)0.0051 (6)0.0076 (6)0.0000.0000.0011 (5)
O510.021 (2)0.0100 (19)0.012 (2)0.0000.000−0.0024 (16)
O520.015 (2)0.0055 (18)0.0110 (19)0.0000.0000.0003 (15)
O530.0095 (14)0.0115 (15)0.0185 (15)−0.0013 (11)−0.0040 (11)0.0006 (12)
P60.0053 (6)0.0062 (6)0.0065 (6)0.0000.0000.0004 (5)
O610.0110 (15)0.0175 (17)0.0255 (19)−0.0056 (12)−0.0036 (13)0.0066 (14)
O620.071 (5)0.006 (2)0.012 (2)0.0000.000−0.0005 (18)
O630.019 (2)0.023 (3)0.009 (2)0.0000.0000.0034 (18)
P70.0061 (12)0.0098 (9)0.0075 (8)0.0002 (6)0.0002 (6)−0.0024 (7)
O710.027 (3)0.014 (2)0.0083 (19)0.0000.000−0.0022 (16)
O72X0.051 (18)0.012 (3)0.047 (5)0.011 (5)0.000 (5)−0.012 (3)
O73X0.019 (3)0.049 (5)0.008 (3)0.021 (3)0.001 (2)0.007 (3)
P80.012 (4)0.0146 (9)0.0094 (7)−0.0055 (11)0.0032 (9)−0.0058 (6)
O810.021 (3)0.049 (4)0.007 (2)0.0000.000−0.007 (2)
O82X0.014 (3)0.018 (3)0.007 (3)−0.001 (2)−0.004 (2)−0.006 (2)
O83X0.009 (3)0.011 (3)0.023 (3)−0.004 (2)0.007 (2)−0.003 (2)
Mg10.0107 (9)0.0119 (10)0.0072 (9)0.0000.0000.0004 (8)
Mg20.0089 (9)0.0069 (9)0.0057 (8)0.0000.000−0.0012 (7)
Mg30.0084 (9)0.0100 (9)0.0063 (8)0.0000.0000.0006 (7)
Mg40.0047 (8)0.0212 (12)0.0085 (9)0.0000.0000.0029 (8)
Mg50.0094 (6)0.0081 (6)0.0097 (6)0.0007 (5)0.0006 (5)0.0002 (5)
Mg60.0638 (15)0.0095 (8)0.0119 (8)0.0020 (9)0.0194 (9)0.0014 (6)
Mg70.0232 (9)0.0122 (8)0.0207 (9)−0.0036 (6)0.0076 (7)−0.0063 (7)
Mg80.0256 (8)0.0089 (7)0.0121 (7)−0.0053 (6)0.0074 (6)−0.0026 (6)
Mg0.0535 (14)0.0087 (8)0.0140 (8)0.0107 (8)−0.0124 (9)−0.0020 (7)
Na0.0535 (14)0.0087 (8)0.0140 (8)0.0107 (8)−0.0124 (9)−0.0020 (7)
Na10.0121 (12)0.0292 (17)0.0172 (14)0.0000.000−0.0063 (13)
Na20.0154 (14)0.0356 (19)0.0167 (15)0.0000.0000.0073 (14)
Na30.0152 (15)0.043 (2)0.0125 (14)0.0000.0000.0112 (14)
Na40.0312 (17)0.0170 (14)0.0208 (15)0.0000.000−0.0035 (12)
Na50.0243 (17)0.0295 (19)0.052 (2)0.0000.000−0.0176 (17)
Na60.047 (5)0.057 (3)0.032 (3)0.009 (3)0.000 (2)0.029 (3)
Nd—O512.379 (5)P8—Mg6vii3.185 (7)
Nd—O32i2.487 (4)P8—Nav3.219 (7)
Nd—O32ii2.487 (4)O81—P8vii1.525 (6)
Nd—O14iii2.499 (3)O81—Mg72.121 (4)
Nd—O142.499 (3)O81—Mg7vii2.121 (4)
Nd—O73Xiv2.513 (7)O81—Na1x2.796 (7)
Nd—O73Xv2.513 (7)O82X—O82Xvii1.091 (13)
Nd—O13iii2.525 (3)O82X—P8vii1.428 (7)
Nd—O132.525 (3)O82X—O83X1.652 (9)
Nd—P1iii3.1834 (12)O82X—Mg3xiii2.037 (6)
Nd—P13.1834 (12)O82X—Mg62.342 (7)
Nd—Na33.673 (3)O82X—Na2xvi2.853 (8)
P1—O111.523 (3)O83X—P8vii1.546 (10)
P1—O121.538 (3)O83X—Nav1.984 (7)
P1—O131.545 (4)O83X—Mgv1.984 (7)
P1—O141.565 (3)O83X—Mg62.052 (7)
P1—Na33.035 (3)O84X—O84Xvii0.885 (17)
P1—Mg83.197 (2)O84X—P8vii1.517 (10)
P1—Na5vi3.296 (3)O84X—Naix2.303 (9)
O11—Mg5vii2.079 (3)O84X—Mgix2.303 (9)
O11—Na5vi2.507 (4)O84X—Mg4viii2.509 (10)
O11—Na32.613 (4)O84X—Na42.745 (10)
O12—Mg3viii2.206 (4)Mg1—O24xviii2.010 (3)
O12—Mg22.224 (3)Mg1—O24vii2.010 (3)
O12—Na4ix2.445 (4)Mg1—O43iv2.010 (4)
O13—Mg6v2.015 (4)Mg1—O43v2.010 (4)
O13—Na5vi2.981 (5)Mg1—P2xviii3.0952 (17)
O14—Mg82.026 (3)Mg1—P2vii3.0952 (17)
O14—Na32.381 (4)Mg1—P7iii3.119 (3)
P2—O211.511 (4)Mg1—Na33.258 (4)
P2—O221.538 (4)Mg1—Nav3.400 (3)
P2—O231.547 (4)Mg1—Mgv3.400 (3)
P2—O241.554 (3)Mg2—O52viii2.015 (5)
P2—Mg52.796 (2)Mg2—O23vii2.070 (4)
P2—Mg7vii2.868 (2)Mg2—O12vii2.224 (3)
P2—Na1x3.027 (2)Mg2—Mg3viii2.984 (3)
P2—Mg1xi3.0952 (17)Mg2—Na4ix3.222 (4)
P2—Na3xi3.174 (2)Mg2—Na1x3.540 (4)
O21—Mg8vii2.066 (4)Mg2—Mg5vii3.610 (2)
O21—Mg7vii2.614 (5)Mg2—Mg53.610 (2)
O21—Na62.727 (7)Mg3—O82Xxxi2.037 (6)
O22—Mg7vii2.062 (4)Mg3—O82Xxxii2.037 (6)
O22—Naix2.293 (4)Mg3—O34i2.040 (3)
O22—Mgix2.293 (4)Mg3—O34ii2.040 (3)
O22—Na1x2.464 (4)Mg3—O12xxiii2.206 (4)
O23—Mg22.070 (4)Mg3—O12xix2.206 (4)
O23—Mg52.191 (4)Mg3—Mg2xix2.984 (3)
O23—Na1x2.520 (4)Mg3—Na2iv3.234 (4)
O24—Mg1xi2.010 (3)Mg3—Na4xxii3.338 (4)
O24—Mg52.192 (4)Mg3—Mg6xxi3.421 (3)
O24—Na3xi2.308 (4)Mg4—O33xxi1.984 (4)
P3—O31xii1.521 (3)Mg4—O33xxii1.984 (4)
P3—O331.538 (3)Mg4—O41xxi1.995 (4)
P3—O341.540 (3)Mg4—O41xxii1.995 (4)
P3—O321.546 (4)Mg4—O72Xiii2.129 (8)
P3—Mg6xiii2.789 (2)Mg4—O84Xxix2.509 (10)
P3—Na2xiv3.260 (2)Mg4—O84Xxxiii2.509 (10)
P3—Na5xii3.269 (3)Mg4—Na1iv3.279 (4)
P3—Na4xv3.451 (2)Mg4—Mg6iii3.368 (3)
O31—P3ii1.521 (3)Mg4—Mg63.368 (3)
O31—Mg82.029 (4)Mg4—Mgxxii3.514 (3)
O31—Na4ix2.638 (4)Mg5—O61xxiv2.004 (4)
O31—Na52.665 (4)Mg5—O11vii2.079 (3)
O32—Mg2.160 (4)Mg5—O53viii2.089 (4)
O32—Ndxii2.487 (4)Mg5—O42ix2.130 (4)
O32—Na2xiv2.775 (5)Mg5—Mg8viii3.104 (2)
O33—Mg4xiii1.984 (4)Mg5—Na3xi3.508 (3)
O33—Mg6xiii2.171 (4)Mg5—Na6xxiv3.612 (5)
O33—Na5xii2.844 (5)Mg5—Na5viii3.786 (4)
O34—Mg3xii2.040 (3)Mg6—O13xxv2.015 (4)
O34—Mg6xiii2.200 (4)Mg6—O44xxii2.058 (4)
O34—Na2xiv2.629 (4)Mg6—O33xxii2.171 (4)
P4—O411.525 (4)Mg6—O34xxii2.200 (4)
P4—O421.528 (4)Mg6—O72Xiii2.56 (2)
P4—O431.540 (4)Mg6—P3xxii2.789 (2)
P4—O441.543 (4)Mg6—P8vii3.185 (7)
P4—Mg2.773 (2)Mg7—O22vii2.062 (4)
P4—Mg7xiii2.780 (2)Mg7—O44xxii2.117 (4)
P4—Na2xiv3.124 (2)Mg7—O42xxii2.332 (5)
O41—Mg4xiii1.995 (4)Mg7—O21vii2.614 (5)
O41—Mg2.289 (6)Mg7—P4xxii2.780 (2)
O41—Na1xvi2.386 (5)Mg7—P2vii2.868 (2)
O42—Mg5xv2.130 (4)Mg7—Mg7vii3.181 (4)
O42—Mg7xiii2.332 (5)Mg7—Na6vii3.481 (6)
O42—Na6xvii2.696 (7)Mg7—Na1x3.525 (4)
O43—Mg1xiv2.010 (4)Mg7—Mgv3.597 (3)
O43—Mg2.133 (4)Mg8—O21vii2.066 (4)
O43—Na2xiv2.465 (4)Mg8—O61vii2.070 (4)
O44—Mg6xiii2.058 (4)Mg8—Mg5xix3.104 (2)
O44—Mg7xiii2.117 (4)Mg8—Na4ix3.544 (3)
O44—Na2xiv2.606 (5)Mg8—Na6vii3.598 (6)
P5—O511.513 (5)Mg—O74Xxxv1.954 (8)
P5—O521.519 (5)Mg—O83Xxxv1.984 (7)
P5—O53iii1.541 (3)Mg—O73Xxxv2.233 (7)
P5—O531.541 (3)Mg—O22xv2.293 (4)
P5—Mg8iii3.004 (2)Mg—O84Xxv2.303 (9)
P5—Mg83.004 (2)Mg—P8xv2.962 (7)
P5—Mg33.042 (3)Mg—P7xxv3.018 (3)
P5—Na6vii3.106 (5)Mg—Mg1xiv3.400 (3)
P5—Na6xviii3.106 (5)Na1—O41xxvi2.386 (5)
O52—Mg31.964 (5)Na1—O41vi2.386 (5)
O52—Mg2xix2.015 (5)Na1—O22xxvii2.464 (4)
O53—Mg82.040 (4)Na1—O22xxviii2.464 (4)
O53—Mg5xix2.089 (4)Na1—O23xxvii2.520 (4)
O53—Na6vii2.380 (6)Na1—O23xxviii2.520 (4)
O53—Na6xviii2.699 (6)Na1—O81xxvii2.796 (7)
P6—O61vii1.524 (4)Na1—P2xxvii3.027 (2)
P6—O611.524 (4)Na1—P2xxviii3.027 (2)
P6—O621.526 (5)Na1—Mg4xiv3.279 (4)
P6—O631.526 (5)Na1—P8xxviii3.384 (4)
P6—Mg82.934 (2)Na1—P8xxvii3.384 (4)
P6—Mg8vii2.934 (2)Na2—O43iv2.465 (4)
P6—Na53.369 (5)Na2—O43v2.465 (4)
O61—Mg5xx2.004 (4)Na2—O44iv2.606 (5)
O61—Mg8vii2.070 (4)Na2—O44v2.606 (5)
O61—Na52.915 (6)Na2—O34iv2.629 (4)
O62—Mg22.011 (6)Na2—O34v2.629 (4)
O62—Na4ix2.548 (6)Na2—O32v2.775 (5)
O62—Mg82.757 (3)Na2—O32iv2.775 (5)
O62—Mg8vii2.757 (3)Na2—O82Xvi2.853 (8)
O63—Mg7vii2.037 (4)Na2—O82Xxxvi2.853 (8)
O63—Mg72.037 (4)Na2—P4iv3.124 (2)
P7—P7iii0.516 (4)Na2—P4v3.124 (2)
P7—O73X1.316 (8)Na3—O24vii2.308 (4)
P7—O72Xiii1.424 (7)Na3—O24xviii2.308 (4)
P7—O72X1.497 (12)Na3—O14iii2.381 (4)
P7—O711.534 (5)Na3—O11iii2.613 (4)
P7—O74X1.540 (7)Na3—P1iii3.035 (3)
P7—O73Xiii1.546 (7)Na3—P2vii3.174 (2)
P7—O74Xiii2.032 (7)Na3—P2xviii3.174 (2)
P7—Mg62.929 (3)Na3—Na5vi3.470 (5)
P7—Nav3.018 (3)Na4—O12xv2.445 (4)
P7—Mgv3.018 (3)Na4—O12xxv2.445 (4)
P7—Mg13.119 (3)Na4—O62xv2.548 (6)
O71—P7iii1.534 (5)Na4—O31xxv2.638 (4)
O71—Mg12.046 (5)Na4—O31xv2.638 (4)
O71—Na6xviii2.387 (7)Na4—O84Xvii2.745 (10)
O71—Na6vii2.387 (7)Na4—Mg2xv3.222 (4)
O72X—O72Xiii0.41 (6)Na4—P8vii3.251 (4)
O72X—P7iii1.424 (7)Na4—Na5xv3.319 (5)
O72X—Mg42.129 (8)Na4—Mg3xiii3.338 (4)
O72X—Mg6iii2.56 (2)Na5—O11xvi2.507 (4)
O73X—O73Xiii1.279 (14)Na5—O11xxiii2.507 (4)
O73X—O74X1.332 (11)Na5—O31vii2.665 (4)
O73X—P7iii1.546 (7)Na5—O33ii2.844 (5)
O73X—Nav2.233 (7)Na5—O33xxix2.844 (5)
O73X—Mgv2.233 (7)Na5—O61vii2.915 (6)
O73X—Ndxiv2.513 (7)Na5—O13xxiii2.981 (5)
O74X—Mg61.941 (8)Na5—O13xvi2.981 (5)
O74X—Nav1.954 (8)Na5—P3ii3.269 (3)
O74X—Mgv1.954 (8)Na5—P3xxix3.269 (3)
O74X—P7iii2.032 (7)Na6—Na6xxx0.649 (11)
P8—P8vii0.304 (16)Na6—O53vii2.380 (6)
P8—O84X1.426 (10)Na6—O71xi2.387 (7)
P8—O82Xvii1.428 (7)Na6—O42xxxi2.696 (7)
P8—O84Xvii1.517 (10)Na6—O53xi2.699 (6)
P8—O811.525 (6)Na6—P5xi3.106 (5)
P8—O82X1.540 (7)Na6—P7vii3.247 (5)
P8—O83Xvii1.546 (10)Na6—P7xi3.298 (5)
P8—O83X1.846 (10)Na6—Mg7vii3.481 (6)
P8—Naix2.962 (7)Na6—Mg8vii3.598 (6)
P8—Mgix2.962 (7)Na6—Mg5xx3.612 (5)
O51—Nd—O32i83.43 (11)O34xxii—Mg6—O72Xiii138.2 (2)
O51—Nd—O32ii83.43 (11)O82X—Mg6—O72Xiii151.8 (3)
O32i—Nd—O32ii94.83 (17)O63—Mg7—O22vii107.8 (2)
O51—Nd—O14iii69.20 (11)O63—Mg7—O44xxii126.5 (2)
O32i—Nd—O14iii87.56 (11)O22vii—Mg7—O44xxii121.83 (17)
O32ii—Nd—O14iii152.10 (10)O63—Mg7—O8178.59 (17)
O51—Nd—O1469.20 (11)O22vii—Mg7—O8184.7 (2)
O32i—Nd—O14152.10 (10)O44xxii—Mg7—O8186.87 (19)
O32ii—Nd—O1487.56 (11)O63—Mg7—O42xxii93.50 (19)
O14iii—Nd—O1477.97 (14)O22vii—Mg7—O42xxii134.79 (17)
O51—Nd—O73Xiv142.9 (2)O44xxii—Mg7—O42xxii66.04 (15)
O32i—Nd—O73Xiv62.54 (18)O81—Mg7—O42xxii139.5 (2)
O32ii—Nd—O73Xiv85.0 (2)O63—Mg7—O21vii83.75 (16)
O14iii—Nd—O73Xiv120.1 (2)O22vii—Mg7—O21vii61.68 (13)
O14—Nd—O73Xiv145.25 (18)O44xxii—Mg7—O21vii135.69 (17)
O51—Nd—O73Xv142.9 (2)O81—Mg7—O21vii134.72 (19)
O32i—Nd—O73Xv85.0 (2)O42xxii—Mg7—O21vii82.42 (14)
O32ii—Nd—O73Xv62.54 (18)O14—Mg8—O3193.14 (15)
O14iii—Nd—O73Xv145.25 (18)O14—Mg8—O53113.75 (15)
O14—Nd—O73Xv120.1 (2)O31—Mg8—O53104.63 (16)
O51—Nd—O13iii125.91 (10)O14—Mg8—O21vii87.71 (16)
O32i—Nd—O13iii86.19 (11)O31—Mg8—O21vii167.17 (18)
O32ii—Nd—O13iii150.44 (11)O53—Mg8—O21vii86.66 (16)
O14iii—Nd—O13iii57.41 (11)O14—Mg8—O61vii165.25 (16)
O14—Nd—O13iii105.15 (11)O31—Mg8—O61vii85.58 (16)
O73Xiv—Nd—O13iii69.2 (2)O53—Mg8—O61vii80.71 (14)
O73Xv—Nd—O13iii88.21 (19)O21vii—Mg8—O61vii90.34 (17)
O51—Nd—O13125.91 (10)O14—Mg8—O62106.35 (15)
O32i—Nd—O13150.44 (11)O31—Mg8—O6286.43 (16)
O32ii—Nd—O1386.19 (11)O53—Mg8—O62137.41 (16)
O14iii—Nd—O13105.15 (11)O21vii—Mg8—O6281.06 (17)
O14—Nd—O1357.41 (11)O61vii—Mg8—O6258.92 (15)
O73Xiv—Nd—O1388.21 (19)O74Xxxv—Mg—O83Xxxv57.2 (3)
O73Xv—Nd—O1369.2 (2)O74Xxxv—Mg—O43114.5 (2)
O13iii—Nd—O1378.96 (13)O83Xxxv—Mg—O43170.6 (3)
O11—P1—O12113.35 (18)O74Xxxv—Mg—O3298.0 (2)
O11—P1—O13110.18 (18)O83Xxxv—Mg—O3297.0 (2)
O12—P1—O13112.99 (18)O43—Mg—O3288.34 (15)
O11—P1—O14108.76 (18)O74Xxxv—Mg—O73Xxxv36.3 (3)
O12—P1—O14109.08 (18)O83Xxxv—Mg—O73Xxxv86.3 (3)
O13—P1—O14101.78 (16)O43—Mg—O73Xxxv88.0 (3)
O21—P2—O22106.5 (2)O32—Mg—O73Xxxv72.4 (2)
O21—P2—O23113.9 (2)O74Xxxv—Mg—O41162.5 (3)
O22—P2—O23110.3 (2)O83Xxxv—Mg—O41119.8 (2)
O21—P2—O24112.1 (2)O43—Mg—O4166.51 (14)
O22—P2—O24111.42 (19)O32—Mg—O4199.53 (16)
O23—P2—O24102.61 (18)O73Xxxv—Mg—O41153.8 (3)
O31xii—P3—O33107.5 (2)O74Xxxv—Mg—O22xv83.3 (2)
O31xii—P3—O34117.7 (2)O83Xxxv—Mg—O22xv91.7 (2)
O33—P3—O34102.28 (19)O43—Mg—O22xv82.45 (14)
O31xii—P3—O32110.1 (2)O32—Mg—O22xv170.34 (17)
O33—P3—O32111.7 (2)O73Xxxv—Mg—O22xv104.3 (2)
O34—P3—O32107.3 (2)O41—Mg—O22xv79.46 (16)
O41—P4—O42112.4 (3)O74Xxxv—Mg—O84Xxv107.8 (3)
O41—P4—O43104.8 (2)O83Xxxv—Mg—O84Xxv50.7 (3)
O42—P4—O43114.2 (2)O43—Mg—O84Xxv137.0 (3)
O41—P4—O44113.7 (2)O32—Mg—O84Xxv93.5 (3)
O42—P4—O44104.7 (2)O73Xxxv—Mg—O84Xxv133.4 (3)
O43—P4—O44107.1 (2)O41—Mg—O84Xxv70.8 (3)
O51—P5—O52112.9 (3)O22xv—Mg—O84Xxv95.2 (3)
O51—P5—O53iii109.44 (18)O41xxvi—Na1—O41vi72.3 (2)
O52—P5—O53iii108.27 (17)O41xxvi—Na1—O22xxvii140.18 (17)
O51—P5—O53109.44 (18)O41vi—Na1—O22xxvii74.28 (14)
O52—P5—O53108.27 (17)O41xxvi—Na1—O22xxviii74.28 (14)
O53iii—P5—O53108.4 (3)O41vi—Na1—O22xxviii140.18 (17)
O61vii—P6—O61109.1 (3)O22xxvii—Na1—O22xxviii123.4 (2)
O61vii—P6—O62106.7 (2)O41xxvi—Na1—O23xxvii145.3 (2)
O61—P6—O62106.7 (2)O41vi—Na1—O23xxvii98.65 (13)
O61vii—P6—O63111.39 (19)O22xxvii—Na1—O23xxvii61.06 (12)
O61—P6—O63111.39 (19)O22xxviii—Na1—O23xxvii121.17 (16)
O62—P6—O63111.2 (3)O41xxvi—Na1—O23xxviii98.65 (14)
O73X—P7—O72Xiii126.7 (7)O41vi—Na1—O23xxviii145.3 (2)
O73X—P7—O72X130.4 (5)O22xxvii—Na1—O23xxviii121.17 (16)
O73X—P7—O71117.0 (4)O22xxviii—Na1—O23xxviii61.06 (12)
O72Xiii—P7—O71115.9 (5)O23xxvii—Na1—O23xxviii69.34 (17)
O72X—P7—O71111.7 (5)O41xxvi—Na1—O81xxvii102.98 (19)
O72Xiii—P7—O74X96.5 (11)O41vi—Na1—O81xxvii102.98 (19)
O72X—P7—O74X111.4 (10)O22xxvii—Na1—O81xxvii64.39 (11)
O71—P7—O74X114.9 (3)O22xxviii—Na1—O81xxvii64.39 (11)
O72Xiii—P7—O73Xiii118.5 (9)O23xxvii—Na1—O81xxvii111.76 (16)
O72X—P7—O73Xiii107.2 (9)O23xxviii—Na1—O81xxvii111.76 (16)
O71—P7—O73Xiii104.3 (3)O43iv—Na2—O43v66.40 (17)
O74X—P7—O73Xiii106.6 (4)O43iv—Na2—O44iv58.49 (12)
O73X—P7—O74Xiii92.9 (4)O43v—Na2—O44iv111.21 (16)
O72Xiii—P7—O74Xiii91.4 (11)O43iv—Na2—O44v111.21 (16)
O72X—P7—O74Xiii76.0 (10)O43v—Na2—O44v58.49 (12)
O71—P7—O74Xiii92.1 (2)O44iv—Na2—O44v107.7 (2)
O74X—P7—O74Xiii144.3 (5)O43iv—Na2—O34iv108.65 (10)
O84X—P8—O82Xvii121.1 (5)O43v—Na2—O34iv165.5 (2)
P8vii—P8—O84Xvii66.9 (4)O44iv—Na2—O34iv74.65 (12)
O82Xvii—P8—O84Xvii130.2 (5)O44v—Na2—O34iv133.75 (17)
O84X—P8—O81117.6 (5)O43iv—Na2—O34v165.5 (2)
O82Xvii—P8—O81116.1 (4)O43v—Na2—O34v108.65 (10)
O84Xvii—P8—O81112.1 (5)O44iv—Na2—O34v133.75 (17)
O84X—P8—O82X128.5 (5)O44v—Na2—O34v74.65 (12)
O84Xvii—P8—O82X108.8 (6)O34iv—Na2—O34v72.59 (16)
O81—P8—O82X109.7 (4)O43iv—Na2—O32v111.67 (17)
O84X—P8—O83Xvii77.2 (5)O43v—Na2—O32v69.32 (12)
O82Xvii—P8—O83Xvii67.4 (4)O44iv—Na2—O32v166.14 (17)
O84Xvii—P8—O83Xvii111.5 (5)O44v—Na2—O32v84.56 (11)
O81—P8—O83Xvii104.7 (4)O34iv—Na2—O32v101.72 (15)
O82X—P8—O83Xvii110.0 (4)O34v—Na2—O32v54.69 (11)
O84X—P8—O83X100.6 (5)O43iv—Na2—O32iv69.32 (12)
O82Xvii—P8—O83X100.3 (4)O43v—Na2—O32iv111.67 (17)
O84Xvii—P8—O83X66.1 (5)O44iv—Na2—O32iv84.56 (11)
O81—P8—O83X91.8 (4)O44v—Na2—O32iv166.14 (17)
O82X—P8—O83X57.6 (4)O34iv—Na2—O32iv54.69 (11)
O83Xvii—P8—O83X162.4 (5)O34v—Na2—O32iv101.72 (15)
O24xviii—Mg1—O24vii86.12 (19)O32v—Na2—O32iv82.55 (18)
O24xviii—Mg1—O43iv87.97 (13)O43iv—Na2—O82Xvi124.47 (17)
O24vii—Mg1—O43iv151.84 (19)O43v—Na2—O82Xvi140.8 (2)
O24xviii—Mg1—O43v151.84 (19)O44iv—Na2—O82Xvi65.98 (16)
O24vii—Mg1—O43v87.97 (13)O44v—Na2—O82Xvi84.37 (18)
O43iv—Mg1—O43v84.4 (2)O34iv—Na2—O82Xvi53.55 (16)
O24xviii—Mg1—O7199.48 (16)O34v—Na2—O82Xvi68.42 (16)
O24vii—Mg1—O7199.48 (16)O32v—Na2—O82Xvi122.98 (17)
O43iv—Mg1—O71108.65 (16)O32iv—Na2—O82Xvi106.98 (16)
O43v—Mg1—O71108.65 (16)O43iv—Na2—O82Xxxvi140.8 (2)
O62—Mg2—O52viii158.0 (2)O43v—Na2—O82Xxxvi124.47 (17)
O62—Mg2—O23101.27 (16)O44iv—Na2—O82Xxxvi84.37 (18)
O52viii—Mg2—O2394.54 (15)O44v—Na2—O82Xxxvi65.98 (16)
O62—Mg2—O23vii101.27 (16)O34iv—Na2—O82Xxxvi68.42 (16)
O52viii—Mg2—O23vii94.54 (15)O34v—Na2—O82Xxxvi53.55 (16)
O23—Mg2—O23vii87.7 (2)O32v—Na2—O82Xxxvi106.98 (16)
O62—Mg2—O1287.15 (16)O32iv—Na2—O82Xxxvi122.98 (17)
O52viii—Mg2—O1275.59 (14)O82Xvi—Na2—O82Xxxvi22.1 (3)
O23—Mg2—O12169.17 (16)O24vii—Na3—O24xviii72.97 (18)
O23vii—Mg2—O1297.46 (13)O24vii—Na3—O14iii171.6 (2)
O62—Mg2—O12vii87.15 (16)O24xviii—Na3—O14iii101.77 (11)
O52viii—Mg2—O12vii75.59 (14)O24vii—Na3—O14101.77 (11)
O23—Mg2—O12vii97.46 (13)O24xviii—Na3—O14171.6 (2)
O23vii—Mg2—O12vii169.17 (16)O14iii—Na3—O1482.65 (18)
O12—Mg2—O12vii75.97 (18)O24vii—Na3—O11iii122.51 (19)
O52—Mg3—O82Xxxi161.1 (2)O24xviii—Na3—O11iii71.46 (12)
O52—Mg3—O82Xxxii161.1 (2)O14iii—Na3—O11iii60.14 (11)
O82Xxxi—Mg3—O82Xxxii31.1 (4)O14—Na3—O11iii116.87 (17)
O52—Mg3—O34i100.35 (15)O24vii—Na3—O1171.46 (12)
O82Xxxi—Mg3—O34i74.8 (2)O24xviii—Na3—O11122.51 (19)
O82Xxxii—Mg3—O34i98.4 (2)O14iii—Na3—O11116.87 (17)
O52—Mg3—O34ii100.35 (15)O14—Na3—O1160.14 (11)
O82Xxxi—Mg3—O34ii98.4 (2)O11iii—Na3—O1191.98 (18)
O82Xxxii—Mg3—O34ii74.8 (2)O12xv—Na4—O12xxv68.10 (16)
O34i—Mg3—O34ii99.4 (2)O12xv—Na4—O62xv71.64 (14)
O52—Mg3—O12xxiii77.01 (14)O12xxv—Na4—O62xv71.64 (14)
O82Xxxi—Mg3—O12xxiii104.0 (2)O12xv—Na4—O31xxv146.90 (16)
O82Xxxii—Mg3—O12xxiii84.9 (2)O12xxv—Na4—O31xxv87.77 (11)
O34i—Mg3—O12xxiii168.63 (15)O62xv—Na4—O31xxv79.58 (13)
O34ii—Mg3—O12xxiii91.93 (13)O12xv—Na4—O31xv87.77 (11)
O52—Mg3—O12xix77.01 (14)O12xxv—Na4—O31xv146.90 (16)
O82Xxxi—Mg3—O12xix84.9 (2)O62xv—Na4—O31xv79.58 (13)
O82Xxxii—Mg3—O12xix104.0 (2)O31xxv—Na4—O31xv103.03 (19)
O34i—Mg3—O12xix91.93 (13)O12xv—Na4—O84X101.0 (2)
O34ii—Mg3—O12xix168.63 (15)O12xxv—Na4—O84X111.8 (2)
O12xxiii—Mg3—O12xix76.70 (17)O62xv—Na4—O84X170.47 (19)
O33xxi—Mg4—O33xxii92.9 (2)O31xxv—Na4—O84X109.1 (2)
O33xxi—Mg4—O41xxi88.36 (17)O31xv—Na4—O84X94.3 (2)
O33xxii—Mg4—O41xxi173.5 (2)O12xv—Na4—O84Xvii111.8 (2)
O33xxi—Mg4—O41xxii173.5 (2)O12xxv—Na4—O84Xvii101.0 (2)
O33xxii—Mg4—O41xxii88.36 (17)O62xv—Na4—O84Xvii170.47 (18)
O41xxi—Mg4—O41xxii89.7 (3)O31xxv—Na4—O84Xvii94.3 (2)
O33xxi—Mg4—O72X85.5 (6)O31xv—Na4—O84Xvii109.1 (2)
O33xxii—Mg4—O72X93.5 (6)O84X—Na4—O84Xvii18.5 (4)
O41xxi—Mg4—O72X93.0 (6)O11xvi—Na5—O11xxiii97.14 (19)
O41xxii—Mg4—O72X100.8 (6)O11xvi—Na5—O31159.2 (2)
O33xxi—Mg4—O72Xiii93.5 (6)O11xxiii—Na5—O3176.89 (11)
O33xxii—Mg4—O72Xiii85.5 (6)O11xvi—Na5—O31vii76.89 (11)
O41xxi—Mg4—O72Xiii100.8 (6)O11xxiii—Na5—O31vii159.2 (2)
O41xxii—Mg4—O72Xiii93.0 (6)O31—Na5—O31vii101.6 (2)
O72X—Mg4—O72Xiii11.1 (15)O11xvi—Na5—O33ii147.69 (19)
O33xxi—Mg4—O84Xxix102.3 (2)O11xxiii—Na5—O33ii95.00 (11)
O33xxii—Mg4—O84Xxix87.6 (2)O31—Na5—O33ii53.08 (11)
O41xxi—Mg4—O84Xxix85.9 (3)O31vii—Na5—O33ii100.52 (15)
O41xxii—Mg4—O84Xxix71.3 (3)O11xvi—Na5—O33xxix95.00 (11)
O72X—Mg4—O84Xxix172.1 (5)O11xxiii—Na5—O33xxix147.69 (19)
O72Xiii—Mg4—O84Xxix163.0 (7)O31—Na5—O33xxix100.52 (15)
O33xxi—Mg4—O84Xxxiii87.6 (2)O31vii—Na5—O33xxix53.08 (11)
O33xxii—Mg4—O84Xxxiii102.3 (2)O33ii—Na5—O33xxix60.72 (15)
O41xxi—Mg4—O84Xxxiii71.3 (3)O11xvi—Na5—O6162.08 (13)
O41xxii—Mg4—O84Xxxiii85.9 (3)O11xxiii—Na5—O6199.82 (18)
O72X—Mg4—O84Xxxiii163.0 (7)O31—Na5—O6198.93 (17)
O72Xiii—Mg4—O84Xxxiii172.1 (5)O31vii—Na5—O6159.67 (13)
O84Xxix—Mg4—O84Xxxiii20.3 (4)O33ii—Na5—O61144.13 (18)
O61xxiv—Mg5—O11vii87.23 (15)O33xxix—Na5—O61112.32 (12)
O61xxiv—Mg5—O53viii81.09 (15)O11xvi—Na5—O61vii99.82 (18)
O11vii—Mg5—O53viii105.84 (15)O11xxiii—Na5—O61vii62.08 (13)
O61xxiv—Mg5—O42ix86.34 (19)O31—Na5—O61vii59.67 (13)
O11vii—Mg5—O42ix166.46 (18)O31vii—Na5—O61vii98.93 (17)
O53viii—Mg5—O42ix84.92 (16)O33ii—Na5—O61vii112.32 (12)
O61xxiv—Mg5—O23174.75 (16)O33xxix—Na5—O61vii144.13 (18)
O11vii—Mg5—O2387.55 (13)O61—Na5—O61vii50.43 (16)
O53viii—Mg5—O23100.94 (14)O11xvi—Na5—O13xxiii102.48 (15)
O42ix—Mg5—O2398.63 (18)O11xxiii—Na5—O13xxiii53.73 (12)
O61xxiv—Mg5—O24111.86 (16)O31—Na5—O13xxiii90.11 (11)
O11vii—Mg5—O2484.91 (13)O31vii—Na5—O13xxiii146.76 (19)
O53viii—Mg5—O24163.94 (15)O33ii—Na5—O13xxiii62.13 (12)
O42ix—Mg5—O2486.44 (15)O33xxix—Na5—O13xxiii94.41 (16)
O23—Mg5—O2467.04 (12)O61—Na5—O13xxiii149.41 (17)
O74X—Mg6—O13xxv89.1 (2)O61vii—Na5—O13xxiii113.70 (11)
O74X—Mg6—O83X56.3 (3)O11xvi—Na5—O13xvi53.73 (12)
O13xxv—Mg6—O83X92.0 (2)O11xxiii—Na5—O13xvi102.48 (15)
O74X—Mg6—O44xxii86.4 (2)O31—Na5—O13xvi146.76 (19)
O13xxv—Mg6—O44xxii174.7 (2)O31vii—Na5—O13xvi90.11 (11)
O83X—Mg6—O44xxii87.8 (2)O33ii—Na5—O13xvi94.41 (16)
O74X—Mg6—O33xxii128.5 (3)O33xxix—Na5—O13xvi62.13 (12)
O13xxv—Mg6—O33xxii91.79 (15)O61—Na5—O13xvi113.70 (11)
O83X—Mg6—O33xxii173.9 (2)O61vii—Na5—O13xvi149.41 (17)
O44xxii—Mg6—O33xxii88.92 (16)O13xxiii—Na5—O13xvi65.17 (14)
O74X—Mg6—O34xxii164.9 (3)Na6xxx—Na6—O53vii112.87 (15)
O13xxv—Mg6—O34xxii88.80 (15)Na6xxx—Na6—O71xi82.19 (13)
O83X—Mg6—O34xxii108.8 (2)O53vii—Na6—O71xi149.5 (3)
O44xxii—Mg6—O34xxii96.32 (17)Na6xxx—Na6—O42xxxi147.02 (18)
O33xxii—Mg6—O34xxii66.49 (13)O53vii—Na6—O42xxxi67.95 (17)
O74X—Mg6—O82X99.5 (3)O71xi—Na6—O42xxxi114.2 (2)
O13xxv—Mg6—O82X98.5 (2)Na6xxx—Na6—O53xi54.33 (13)
O83X—Mg6—O82X43.6 (2)O53vii—Na6—O53xi58.54 (18)
O44xxii—Mg6—O82X85.0 (2)O71xi—Na6—O53xi129.4 (3)
O33xxii—Mg6—O82X131.0 (2)O42xxxi—Na6—O53xi116.5 (2)
O34xxii—Mg6—O82X66.03 (19)Na6xxx—Na6—O21138.10 (16)
O74X—Mg6—O72Xiii57.0 (3)O53vii—Na6—O2166.58 (18)
O13xxv—Mg6—O72Xiii96.6 (4)O71xi—Na6—O2184.4 (2)
O83X—Mg6—O72Xiii112.4 (3)O42xxxi—Na6—O2174.1 (2)
O44xxii—Mg6—O72Xiii78.6 (4)O53xi—Na6—O21109.8 (2)
O33xxii—Mg6—O72Xiii71.9 (2)
  1 in total

1.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290
  1 in total
  2 in total

1.  Optimization of cell adhesion on mg based implant materials by pre-incubation under cell culture conditions.

Authors:  Regine Willumeit; Anneke Möhring; Frank Feyerabend
Journal:  Int J Mol Sci       Date:  2014-05-05       Impact factor: 5.923

2.  Synthesis and crystal structure of a new magnesium phosphate Na3RbMg7(PO4)6.

Authors:  Teycir Ben Hamed; Amal Boukhris; Abdessalem Badri; Mongi Ben Amara
Journal:  Acta Crystallogr E Crystallogr Commun       Date:  2017-05-05
  2 in total

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