B Henriques1, D Soares, F S Silva. 1. Center for Mechanical and Materials Technologies, University of Minho, Campus de Azurém, 4800-058 Guimarães, Portugal. brunohenriques@dem.uminho.pt
Abstract
OBJECTIVES: The purpose of this study was to compare the microstructure, hardness, corrosion resistance and metal-porcelain bond strength of a CoCrMo dental alloy obtained by two routes, cast and hot pressing. METHODS: CoCrMo alloy substrates were obtained by casting and hot pressing. Substrates' microstructure was examined by the means of Optical Microscopy (OM) and by Scanning Electron Microscope (SEM) and Energy Dispersive X-ray Spectroscopy (EDS). Hardness tests were performed in a microhardness indenter. The electrochemical behavior of substrates was investigated through potentiodynamic tests in a saline solution (8g NaCl/L). Substrates were bonded to dental porcelain and metal-porcelain bond strength was assessed by the means of a shear test performed in a universal test machine (crosshead speed: 0.5 mm/min) until fracture. Fractured surfaces as well as undestroyed interface specimens were examined with Stereomicroscopy and SEM-EDS. Data was analyzed with Shapiro-Wilk test to test the assumption of normality. The t-test (p<0.05) was used to compare shear bond strength results. RESULTS: Cast specimens exhibited dendritic microstructures whereas hot pressed specimens exhibited a typical globular microstructure with a second phase spread through the matrix. The hardness registered for hot pressed substrates was greater than that of cast specimens, 438±24HV/1 and 324±8HV/1, respectively. Hot pressed substrates showed better corrosion properties than cast ones, i.e. higher OCP; higher corrosion potential (E(corr)) and lower current densities (i(corr)). No significant difference was found (p<0.05) in metal-ceramic bond strength between cast (116.5±6.9 MPa) and hot pressed (114.2±11.9 MPa) substrates. The failure type analysis revealed an adhesive failure for all specimens. SIGNIFICANCE: Hot pressed products arise as an alternative to cast products in dental prosthetics, as they impart enhanced mechanical and electrochemical properties to prostheses without compromising the metal-ceramic bond strength.
OBJECTIVES: The purpose of this study was to compare the microstructure, hardness, corrosion resistance and metal-porcelain bond strength of a CoCrMo dental alloy obtained by two routes, cast and hot pressing. METHODS: CoCrMo alloy substrates were obtained by casting and hot pressing. Substrates' microstructure was examined by the means of Optical Microscopy (OM) and by Scanning Electron Microscope (SEM) and Energy Dispersive X-ray Spectroscopy (EDS). Hardness tests were performed in a microhardness indenter. The electrochemical behavior of substrates was investigated through potentiodynamic tests in a saline solution (8g NaCl/L). Substrates were bonded to dental porcelain and metal-porcelain bond strength was assessed by the means of a shear test performed in a universal test machine (crosshead speed: 0.5 mm/min) until fracture. Fractured surfaces as well as undestroyed interface specimens were examined with Stereomicroscopy and SEM-EDS. Data was analyzed with Shapiro-Wilk test to test the assumption of normality. The t-test (p<0.05) was used to compare shear bond strength results. RESULTS: Cast specimens exhibited dendritic microstructures whereas hot pressed specimens exhibited a typical globular microstructure with a second phase spread through the matrix. The hardness registered for hot pressed substrates was greater than that of cast specimens, 438±24HV/1 and 324±8HV/1, respectively. Hot pressed substrates showed better corrosion properties than cast ones, i.e. higher OCP; higher corrosion potential (E(corr)) and lower current densities (i(corr)). No significant difference was found (p<0.05) in metal-ceramic bond strength between cast (116.5±6.9 MPa) and hot pressed (114.2±11.9 MPa) substrates. The failure type analysis revealed an adhesive failure for all specimens. SIGNIFICANCE: Hot pressed products arise as an alternative to cast products in dental prosthetics, as they impart enhanced mechanical and electrochemical properties to prostheses without compromising the metal-ceramic bond strength.
Authors: Elif Ece Yoldan; Nurullah Türker; Ulviye Ş Büyükkaplan; Mehmet M Özarslan; Recep Karalı; Ahmet T Deniz Journal: Scanning Date: 2020-04-29 Impact factor: 1.932