| Literature DB >> 22515182 |
Meng-Yang Chang1, Tein-Wei Lee, Ming-Hao Wu.
Abstract
A straightforward synthesis of 3,8-dimethoxy-10,11-dihydrobenzo[j]fluoranthen-12-ones 1 is reported in a seven-step route from biphenyl-4,4'-diol 2 via the transformation of a double Claisen rearrangement, cross metathesis with ethyl acrylate, and polyphosphoric acid (PPA)-promoted Friedel-Crafts electrophilic benzannulation in good yields.Entities:
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Year: 2012 PMID： 22515182 DOI： 10.1021/ol3006979
Source DB: PubMed Journal: Org Lett ISSN： 1523-7052 Impact factor: 6.005