Literature DB >> 22462925

An in-vacuum x-ray diffraction microscope for use in the 0.7-2.9 keV range.

D J Vine1, G J Williams, J N Clark, C T Putkunz, M A Pfeifer, D Legnini, C Roehrig, E Wrobel, E Huwald, G van Riessen, B Abbey, T Beetz, J Irwin, M Feser, B Hornberger, I McNulty, K A Nugent, A G Peele.   

Abstract

A dedicated in-vacuum coherent x-ray diffraction microscope was installed at the 2-ID-B beamline of the Advanced Photon Source for use with 0.7-2.9 keV x-rays. The instrument can accommodate three common implementations of diffractive imaging; plane wave illumination; defocused-probe (Fresnel diffractive imaging) and scanning (ptychography) using either a pinhole, focused or defocused probe. The microscope design includes active feedback to limit motion of the optics with respect to the sample. Upper bounds on the relative optics-to-sample displacement have been measured to be 5.8 nm(v) and 4.4 nm(h) rms/h using capacitance micrometry and 27 nm/h using x-ray point projection imaging. The stability of the measurement platform and in-vacuum operation allows for long exposure times, high signal-to-noise and large dynamic range two-dimensional intensity measurements to be acquired. Finally, we illustrate the microscope's stability with a recent experimental result.

Entities:  

Year:  2012        PMID: 22462925     DOI: 10.1063/1.3688655

Source DB:  PubMed          Journal:  Rev Sci Instrum        ISSN: 0034-6748            Impact factor:   1.523


  6 in total

1.  Whole-cell phase contrast imaging at the nanoscale using Fresnel coherent diffractive imaging tomography.

Authors:  Michael W M Jones; Grant A van Riessen; Brian Abbey; Corey T Putkunz; Mark D Junker; Eugeniu Balaur; David J Vine; Ian McNulty; Bo Chen; Benedicta D Arhatari; Sarah Frankland; Keith A Nugent; Leann Tilley; Andrew G Peele
Journal:  Sci Rep       Date:  2013       Impact factor: 4.379

2.  X-ray ptychographic computed tomography at 16 nm isotropic 3D resolution.

Authors:  M Holler; A Diaz; M Guizar-Sicairos; P Karvinen; Elina Färm; Emma Härkönen; Mikko Ritala; A Menzel; J Raabe; O Bunk
Journal:  Sci Rep       Date:  2014-01-24       Impact factor: 4.379

3.  Mapping biological composition through quantitative phase and absorption X-ray ptychography.

Authors:  Michael W M Jones; Kirstin Elgass; Mark D Junker; Mac B Luu; Michael T Ryan; Andrew G Peele; Grant A van Riessen
Journal:  Sci Rep       Date:  2014-10-28       Impact factor: 4.379

4.  A Direct Approach to In-Plane Stress Separation using Photoelastic Ptychography.

Authors:  Nicholas Anthony; Guido Cadenazzi; Henry Kirkwood; Eric Huwald; Keith Nugent; Brian Abbey
Journal:  Sci Rep       Date:  2016-08-04       Impact factor: 4.379

5.  Fast positioning for X-ray scanning microscopy by a combined motion of sample and beam-defining optics.

Authors:  Michal Odstrcil; Maxime Lebugle; Thierry Lachat; Jörg Raabe; Mirko Holler
Journal:  J Synchrotron Radiat       Date:  2019-01-25       Impact factor: 2.616

6.  Coherent imaging at the diffraction limit.

Authors:  Pierre Thibault; Manuel Guizar-Sicairos; Andreas Menzel
Journal:  J Synchrotron Radiat       Date:  2014-08-27       Impact factor: 2.616

  6 in total

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