Literature DB >> 22392614

New kinetic-spectrophotometric method for monitoring the concentration of iodine in river and city water samples.

A Farmany1, A Khosravi, S Abbasi, J Cheraghi, R Hushmandfar, S Sobhanardakani, H Noorizadeh, S S Mortazavi.   

Abstract

A new kinetic method has been developed for the determination of iodine in water samples. The method is based on the catalytic effect of I(-) with the oxidation of Indigo Carmine (IC) by KBrO(3) in the sulfuric acid medium. The optimum conditions obtained are 0.16 M sulfuric acid, 1 × 10(-3) M of IC, 1 × 10(-2) M KBrO(3), reaction temperature of 35°C, and reaction time of 80 s at 612 nm. Under the optimized conditions, the method allowed the quantification of I(-) in a range of 12-375 ng/mL with a detection limit of 0.46 ng/mL. The method was applied to the determination of iodine in river and city water samples with the satisfactorily results.

Entities:  

Mesh:

Substances:

Year:  2012        PMID: 22392614     DOI: 10.1007/s10661-012-2574-4

Source DB:  PubMed          Journal:  Environ Monit Assess        ISSN: 0167-6369            Impact factor:   2.513


  10 in total

1.  Headspace single-drop microextraction coupled to microvolume UV-vis spectrophotometry for iodine determination.

Authors:  Francisco Pena-Pereira; Isela Lavilla; Carlos Bendicho
Journal:  Anal Chim Acta       Date:  2008-10-30       Impact factor: 6.558

2.  A sensitive colorimetric method for the micro determination of iodine in marine water.

Authors:  O Agrawal; G Sunita; V K Gupta
Journal:  Talanta       Date:  1999-07-12       Impact factor: 6.057

3.  Determination of urinary iodine by inductively coupled plasma mass spectrometry.

Authors:  P Macours; J C Aubry; B Hauquier; J M Boeynaems; S Goldman; R Moreno-Reyes
Journal:  J Trace Elem Med Biol       Date:  2008-06-05       Impact factor: 3.849

4.  Determination of selenium and iodine in human thyroids.

Authors:  Miguel Murillo; Nereida Carrión; Mercedes Quintana; Georgia Sanabria; Manuel Ríos; Leopoldo Duarte; Franklin Ablan
Journal:  J Trace Elem Med Biol       Date:  2005       Impact factor: 3.849

5.  Determination of iodine values according to Hanus using 1,3-dibromo-5,5-dimethylhydantoin (DBH): analytical methods of pharmacopeias with DBH: part 7.

Authors:  Manfred Hilp
Journal:  J Pharm Biomed Anal       Date:  2002-04-01       Impact factor: 3.935

6.  Selective preconcentration and determination of iodine species in milk samples using polymer inclusion sorbent.

Authors:  P R Bhagat; A K Pandey; R Acharya; A G C Nair; N S Rajurkar; A V R Reddy
Journal:  Talanta       Date:  2006-07-18       Impact factor: 6.057

7.  Catalytic spectrophotometric determination of iodine in coal by pyrohydrolysis decomposition.

Authors:  Daishe Wu; Haiwen Deng; Wuyi Wang; Huayun Xiao
Journal:  Anal Chim Acta       Date:  2007-08-31       Impact factor: 6.558

8.  Kinetic determination of total iodine in urine and foodstuffs using a mixed acid as a pretreatment agent.

Authors:  Takashi Tomiyasu; Misa Nonaka; Makoto Uchikado; Katsuro Anazawa; Hayao Sakamoto
Journal:  Anal Sci       Date:  2004-02       Impact factor: 2.081

9.  Determination of iodine in human milk and infant formulas.

Authors:  Luisa Maria Fernández-Sánchez; Pilar Bermejo-Barrera; José Maria Fraga-Bermudez; Joanna Szpunar; Ryszard Lobinski
Journal:  J Trace Elem Med Biol       Date:  2007-11-19       Impact factor: 3.849

10.  Single drop microextraction or solid phase microextraction-gas chromatography-mass spectrometry for the determination of iodine in pharmaceuticals, iodized salt, milk powder and vegetables involving conversion into 4-iodo-N,N-dimethylaniline.

Authors:  Paramita Das; Manju Gupta; Archana Jain; Krishna K Verma
Journal:  J Chromatogr A       Date:  2004-01-09       Impact factor: 4.759

  10 in total

北京卡尤迪生物科技股份有限公司 © 2022-2023.