| Literature DB >> 21801078 |
A Veršilovskis1, B Huybrecht, E K Tangni, L Pussemier, S De Saeger, A Callebaut.
Abstract
Seven commercially available deoxynivalenol (DON) and zearalenone (ZEN) immunoaffinity columns (IACs) were tested for cross-reactivity to conjugated forms (3-acetyl-deoxynivalenol, 15-acetyl-deoxynivalenol, DON-3-glucoside, DON-3-glucuronide, ZEN-glucosides, ZEN-glucuronide) and metabolites (de-epoxydeoxynivalenol, α-zearalenol, β-zearalenol) and nivalenol (NIV), using a semi-quantitative multi-mycotoxin ultra-performance liquid chromatography-tandem mass spectrometry method. The DON IACs showed cross-reactivity for nearly all DON derivatives tested. The ZEN IACs showed limited cross-reactivity to some of the ZEN derivatives. The IACs were evaluated for their potential use as sample clean-up for mycotoxins in serum.Entities:
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Year: 2011 PMID: 21801078 DOI: 10.1080/19440049.2011.603364
Source DB: PubMed Journal: Food Addit Contam Part A Chem Anal Control Expo Risk Assess ISSN: 1944-0057