Literature DB >> 21581593

4,4'-Bipyridinium bis(perchlorate)-4-aminobenzoic acid-4,4'-bipyridine-water (1/4/2/2).

Qun-Hui Meng, Lu Han, Jian-Dong Hou, Yi-Fan Luo, Rong-Hua Zeng.   

Abstract

In the structure of the title compound, C(10)H(10)N(2) (2+)·2ClO(4) (-)·4C(7)H(7)n class="Chemical">NO(2)·2C(10)H(8)N(2)·2H(2)O, the 4,4'-bipyridinium cation has a crystallographically imposed centre of symmetry. The cation is linked by N-H⋯N hydrogen bonds to adjacent 4,4'-bipyridine mol-ecules, which in turn inter-act via O-H⋯N hydrogen bonds with 4-amino-benzoic acid mol-ecules, forming chains running parallel to [30]. The chains are further connected into a three-dimensional network by N-H⋯O and O-H⋯O hydrogen-bonding inter-actions involving the perchlorate anion, the water mol-ecules and the 4-amino-benzoic acid mol-ecules. In addition, π-π stacking inter-actions with centroid-centroid distances ranging from 3.663 (6) to 3.695 (6) Å are present. The O atoms of the perchlorate anion are disordered over two sets of positions, with refined site occupancies of 0.724 (9) and 0.276 (9).

Entities:  

Year:  2008        PMID: 21581593      PMCID: PMC2968051          DOI: 10.1107/S1600536808042207

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


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1.  4,4'-Bipyridinium bis-(μ-4-oxo-1,4-dihydropyridine-2,6-dicarboxyl-ato)bis-[aqua-hydroxido-anti-monate(III)] dihydrate.

Authors:  Janet Soleimannejad; Jafar Attar Gharamaleki; Hossein Aghabozorg; Yaghoub Mohammadzadeh Azar Golenji
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2010-03-31
  1 in total

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