Literature DB >> 21522930

{2,6-Bis[(2,6-diphenyl-phosphan-yl)-oxy]-4-fluoro-phenyl-κP,C,P'}(6-methyl-2,2,4-trioxo-3,4-dihydro-1,2,3-oxathia-zin-3-ido-κN)palladium(II).

Benjamin F Wicker1, Rachel Seaman, Norris W Hoffman, James H Davis, Richard E Sykora.   

Abstract

The title acesulfamate complex, [Pd(C(30)H(22)FO(2)P(2))(C(4)H(4)NO(4)S)], contains a four-coordinate Pd(II) ion with the expected, although relatively distorted, square-planar geometry where the four L-Pd-L angles range from 79.58 (8) to 102.47 (7)°. The acesulfamate ligand is N-bound to Pd [Pd-N = 2.127 (2) Å] with a dihedral angle of 76.35 (6)° relative to the square plane. Relatively long phen-yl-acesulfamate C-H⋯O and phen-yl-fluorine C-H⋯F inter-actions consolidate the crystal packing.

Entities:  

Year:  2011        PMID: 21522930      PMCID: PMC3051636          DOI: 10.1107/S1600536811002911

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


  9 in total

1.  Structural properties of trans-cyclohexane-1,2-diamine complexes of copper(II) and zinc(II) acesulfamates.

Authors:  Zarife Sibel Şahin; Fatma Sevindi; Hasan İçbudak; Şamil Işık
Journal:  Acta Crystallogr C       Date:  2010-09-29       Impact factor: 1.172

2.  Sweet success: Ionic liquids derived from non-nutritive sweeteners.

Authors:  Elke B Carter; Stephanie L Culver; Phillip A Fox; Russell D Goode; Ioanna Ntai; Morgan D Tickell; Rachel K Traylor; Norris W Hoffman; James H Davis
Journal:  Chem Commun (Camb)       Date:  2004-02-10       Impact factor: 6.222

3.  Bis(acesulfamato-kappaO4)diaquabis(3-methylpyridine-kappaN)nickel(II).

Authors:  Necmi Dege; Hasan Içbudak; Elif Adiyaman
Journal:  Acta Crystallogr C       Date:  2006-12-12       Impact factor: 1.172

4.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290

5.  Pt(II) and Ag(I) complexes with acesulfame: crystal structure and a study of their antitumoral, antimicrobial and antiviral activities.

Authors:  Maurício Cavicchioli; Antonio C Massabni; Tassiele A Heinrich; Claudio M Costa-Neto; Emiliana P Abrão; Benedito A L Fonseca; Eduardo E Castellano; Pedro P Corbi; Wilton R Lustri; Clarice Q F Leite
Journal:  J Inorg Biochem       Date:  2010-01-18       Impact factor: 4.155

6.  Bis(acesulfamato-kappa2O4,N)bis(3-methylpyridine)copper(II).

Authors:  Necmi Dege; Hasan Içbudak; Elif Adiyaman
Journal:  Acta Crystallogr C       Date:  2006-08-11       Impact factor: 1.172

7.  Bis(acesulfamato-kappa2N3,O4)bis(2-aminopyrimidine-kappaN1)copper(II).

Authors:  Ahmet Bulut; Hasan Içbudak; Gözde Sezer; Canan Kazak
Journal:  Acta Crystallogr C       Date:  2005-04-23       Impact factor: 1.172

8.  Bis(acesulfamato)tetraaquacobalt(II).

Authors:  Hasan Içbudak; Ahmet Bulut; Naziye Cetin; Canan Kazak
Journal:  Acta Crystallogr C       Date:  2004-12-11       Impact factor: 1.172

9.  Di-mu-acesulfamato-kappa3N,O:O;kappa3O:N,O-bis[(acesulfamato-kappa2N,O)bis(3-methylpyridine)cadmium(II)].

Authors:  Zarife Sibel Sahin; Hasan Içbudak; Samil Işik
Journal:  Acta Crystallogr C       Date:  2009-11-07       Impact factor: 1.172

  9 in total
  1 in total

1.  {2,6-Bis[(2,6-diisopropyl-phosphan-yl)-oxy]-4-fluoro-phenyl-κ(3)P,C(1),P'}(1H-pyrazole-κN(2))nickel(II) hexa-fluoro-phosphate.

Authors:  Man-Lung Kwan; Sara J Conry; Charles S Carfagna; Loren P Press; Oleg V Ozerov; Norris W Hoffman; Richard E Sykora
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2012-09-19
  1 in total

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