Literature DB >> 21449603

A method for the deprotection of alkylpinacolyl boronate esters.

Jing Sun1, Michael T Perfetti, Webster L Santos.   

Abstract

A two-step procedure for deprotection of alkylpinacolyl boronate esters via transesterification with diethanolamine followed by hydrolysis was successfully developed with the advantages of tolerance to various functional groups, short reaction time, and ease of product isolation.
© 2011 American Chemical Society

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Year:  2011        PMID： 21449603      PMCID： PMC3092631          DOI： 10.1021/jo200250y

Source DB:  PubMed          Journal:  J Org Chem        ISSN： 0022-3263            Impact factor:   4.354


  20 in total

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4.  Thermal, catalytic, regiospecific functionalization of alkanes

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5.  Palladium-catalyzed, direct boronic acid synthesis from aryl chlorides: a simplified route to diverse boronate ester derivatives.

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6.  Catalytic, Regiospecific End-Functionalization of Alkanes: Rhenium-Catalyzed Borylation under Photochemical Conditions.

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Authors:  David M Knapp; Eric P Gillis; Martin D Burke
Journal:  J Am Chem Soc       Date:  2009-05-27       Impact factor: 15.419

9.  Acylamino boronic acids and difluoroborane analogues of amino acids: potent inhibitors of chymotrypsin and elastase.

Authors:  D H Kinder; J A Katzenellenbogen
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10.  Differentially protected benzenediboronic acids: divalent cross-coupling modules for the efficient synthesis of boron-substituted oligoarenes.

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Journal:  Org Lett       Date:  2008-01-10       Impact factor: 6.005
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  8 in total

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3.  Boryl (Hetero)aryne Precursors as Versatile Arylation Reagents: Synthesis through C-H Activation and Orthogonal Reactivity.

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Journal:  Antimicrob Agents Chemother       Date:  2017-04-24       Impact factor: 5.191

5.  Copper-catalyzed synthesis of allenylboronic acids. Access to sterically encumbered homopropargylic alcohols and amines by propargylboration.

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6.  Diboronate Fluorophore for the Measurement of l-Glucose and Other Carbohydrates and Its Interaction with Albumin.

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Journal:  ACS Omega       Date:  2022-07-06

7.  Diversity-oriented synthesis of peptide-boronic acids by a versatile building-block approach.

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Journal:  Chem Sci       Date:  2020-08-21       Impact factor: 9.825

8.  A catalytic, enantioselective formal synthesis of (+)-dichroanone and (+)-taiwaniaquinone H.

Authors:  Samantha E Shockley; Jeffrey C Holder; Brian M Stoltz
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  8 in total

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