Literature DB >> 21354839

Heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance under ultra-high magic-angle spinning.

Venus Singh Mithu1, Subhradip Paul, Narayanan D Kurur, P K Madhu.   

Abstract

We compare in this communication several heteronuclear dipolar decoupling sequences in solid-state nuclear magnetic resonance experiments under a magic-angle spinning frequency of 60 kHz. The decoupling radiofrequency field amplitudes considered are 190 and 10 kHz. No substantial difference was found among the sequences considered here in performance barring the difference in the optimisation protocol of the various schemes, an aspect that favours the use of swept-frequency two pulse phase modulation (SW(f)-TPPM).
Copyright © 2011 Elsevier Inc. All rights reserved.

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Year:  2011        PMID: 21354839     DOI: 10.1016/j.jmr.2011.01.028

Source DB:  PubMed          Journal:  J Magn Reson        ISSN: 1090-7807            Impact factor:   2.229


  7 in total

1.  Sensitivity and resolution enhanced solid-state NMR for paramagnetic systems and biomolecules under very fast magic angle spinning.

Authors:  Sudhakar Parthasarathy; Yusuke Nishiyama; Yoshitaka Ishii
Journal:  Acc Chem Res       Date:  2013-07-26       Impact factor: 22.384

2.  Performance of RINEPT is amplified by dipolar couplings under ultrafast MAS conditions.

Authors:  Rongchun Zhang; Ayyalusamy Ramamoorthy
Journal:  J Magn Reson       Date:  2014-04-16       Impact factor: 2.229

3.  Peptide and Protein Dynamics and Low-Temperature/DNP Magic Angle Spinning NMR.

Authors:  Qing Zhe Ni; Evgeny Markhasin; Thach V Can; Björn Corzilius; Kong Ooi Tan; Alexander B Barnes; Eugenio Daviso; Yongchao Su; Judith Herzfeld; Robert G Griffin
Journal:  J Phys Chem B       Date:  2017-05-10       Impact factor: 2.991

4.  Constant-time 2D and 3D through-bond correlation NMR spectroscopy of solids under 60 kHz MAS.

Authors:  Rongchun Zhang; Ayyalusamy Ramamoorthy
Journal:  J Chem Phys       Date:  2016-01-21       Impact factor: 3.488

5.  Proton-detected 3D (1)H/(13)C/(1)H correlation experiment for structural analysis in rigid solids under ultrafast-MAS above 60 kHz.

Authors:  Rongchun Zhang; Yusuke Nishiyama; Ayyalusamy Ramamoorthy
Journal:  J Chem Phys       Date:  2015-10-28       Impact factor: 3.488

6.  A Novel High-Resolution and Sensitivity-Enhanced Three-Dimensional Solid-State NMR Experiment Under Ultrafast Magic Angle Spinning Conditions.

Authors:  Rongchun Zhang; Manoj Kumar Pandey; Yusuke Nishiyama; Ayyalusamy Ramamoorthy
Journal:  Sci Rep       Date:  2015-07-03       Impact factor: 4.379

7.  Rationalising Heteronuclear Decoupling in Refocussing Applications of Solid-State NMR Spectroscopy.

Authors:  Ilya Frantsuzov; Suresh K Vasa; Matthias Ernst; Steven P Brown; Vadim Zorin; Arno P M Kentgens; Paul Hodgkinson
Journal:  Chemphyschem       Date:  2017-01-23       Impact factor: 3.102

  7 in total

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