Strength enhancement of a biomedical titanium alloy through a modified accumulative roll bonding technique.

The strength of a biomedical β-type alloy, Ti-25Nb-3Zr-3Mo-2Sn, was enhanced through severe plastic deformation using a modified accumulative roll bonding technique. Incremental strength increases were observed after each cycle, while ductility initially fell but showed some recovery with further cycles. After 4 cycles there was a 70% improvement in the ultimate tensile strength to 1220 MPa, a two-fold increase in the 0.5% proof stress to 946 MPa and the ductility was 4.5%. The microstructure comprised of ultrafine grain β grains heavily elongated in the rolling direction with a fine dispersion of nanocrystalline α phase precipitates on the β grain boundaries. Shear bands formed in order to accommodate large plastic strains during processing and the grains within the bands were significantly finer than the surrounding matrix.