Literature DB >> 21243088

Continuous-Wave Operation of a Frequency-Tunable 460-GHz Second-Harmonic Gyrotron for Enhanced Nuclear Magnetic Resonance.

Antonio C Torrezan1, Seong-Tae Han, Ivan Mastovsky, Michael A Shapiro, Jagadishwar R Sirigiri, Richard J Temkin, Alexander B Barnes, Robert G Griffin.   

Abstract

The design, operation, and characterization of a continuous-wave (CW) tunable second-harmonic 460-GHz gyrotron are reported. The gyrotron is intended to be used as a submillimeter-wave source for 700-MHz nuclear magnetic resonance experiments with sensitivity enhanced by dynamic nuclear polarization. The gyrotron operates in the whispering-gallery mode TE(11,2) and has generated 16 W of output power with a 13-kV 100-mA electron beam. The start oscillation current measured over a range of magnetic field values is in good agreement with theoretical start currents obtained from linear theory for successive high-order axial modes TE(11,2,q). The minimum start current is 27 mA. Power and frequency tuning measurements as a function of the electron cyclotron frequency have also been carried out. A smooth frequency tuning range of 1 GHz was obtained for the operating second-harmonic mode either by magnetic field tuning or beam voltage tuning. Long-term CW operation was evaluated during an uninterrupted period of 48 h, where the gyrotron output power and frequency were kept stable to within ±0.7% and ±6 ppm, respectively, by a computerized control system. Proper operation of an internal quasi-optical mode converter implemented to transform the operating whispering-gallery mode to a Gaussian-like beam was also verified. Based on the images of the gyrotron output beam taken with a pyroelectric camera, the Gaussian-like mode content of the output beam was computed to be 92% with an ellipticity of 12%.

Entities:  

Year:  2010        PMID: 21243088      PMCID: PMC3021140          DOI: 10.1109/TPS.2010.2046617

Source DB:  PubMed          Journal:  IEEE Trans Plasma Sci IEEE Nucl Plasma Sci Soc        ISSN: 0093-3813            Impact factor:   1.222


  8 in total

1.  Ultrawide band multifrequency high-field EMR technique: A methodology for increasing spectroscopic information.

Authors:  A K Hassan; L A Pardi; J Krzystek; A Sienkiewicz; P Goy; M Rohrer; L C Brunel
Journal:  J Magn Reson       Date:  2000-02       Impact factor: 2.229

2.  Dynamic nuclear polarization with a cyclotron resonance maser at 5 T.

Authors: 
Journal:  Phys Rev Lett       Date:  1993-11-22       Impact factor: 9.161

Review 3.  Dynamic nuclear polarization at high magnetic fields.

Authors:  Thorsten Maly; Galia T Debelouchina; Vikram S Bajaj; Kan-Nian Hu; Chan-Gyu Joo; Melody L Mak-Jurkauskas; Jagadishwar R Sirigiri; Patrick C A van der Wel; Judith Herzfeld; Richard J Temkin; Robert G Griffin
Journal:  J Chem Phys       Date:  2008-02-07       Impact factor: 3.488

4.  Continuous-Wave Operation of a 460-GHz Second Harmonic Gyrotron Oscillator.

Authors:  Melissa K Hornstein; Vikram S Bajaj; Robert G Griffin; Richard J Temkin
Journal:  IEEE Trans Plasma Sci IEEE Nucl Plasma Sci Soc       Date:  2006-06       Impact factor: 1.222

5.  Operational Characteristics of a 14-W 140-GHz Gyrotron for Dynamic Nuclear Polarization.

Authors:  Colin D Joye; Robert G Griffin; Melissa K Hornstein; Kan-Nian Hu; Kenneth E Kreischer; Melanie Rosay; Michael A Shapiro; Jagadishwar R Sirigiri; Richard J Temkin; Paul P Woskov
Journal:  IEEE Trans Plasma Sci IEEE Nucl Plasma Sci Soc       Date:  2006-06       Impact factor: 1.222

6.  In situ temperature jump high-frequency dynamic nuclear polarization experiments: enhanced sensitivity in liquid-state NMR spectroscopy.

Authors:  Chan-Gyu Joo; Kan-Nian Hu; Jeffrey A Bryant; Robert G Griffin
Journal:  J Am Chem Soc       Date:  2006-07-26       Impact factor: 15.419

7.  250GHz CW gyrotron oscillator for dynamic nuclear polarization in biological solid state NMR.

Authors:  Vikram S Bajaj; Melissa K Hornstein; Kenneth E Kreischer; Jagadishwar R Sirigiri; Paul P Woskov; Melody L Mak-Jurkauskas; Judith Herzfeld; Richard J Temkin; Robert G Griffin
Journal:  J Magn Reson       Date:  2007-09-20       Impact factor: 2.229

8.  Corrugated Waveguide and Directional Coupler for CW 250-GHz Gyrotron DNP Experiments.

Authors:  Paul P Woskov; Vikram S Bajaj; Melissa K Hornstein; Richard J Temkin; Robert G Griffin
Journal:  IEEE Trans Microw Theory Tech       Date:  2005-06       Impact factor: 3.599

  8 in total
  8 in total

1.  2H-DNP-enhanced 2H-13C solid-state NMR correlation spectroscopy.

Authors:  Thorsten Maly; Loren B Andreas; Albert A Smith; Robert G Griffin
Journal:  Phys Chem Chem Phys       Date:  2010-05-11       Impact factor: 3.676

2.  Topical Developments in High-Field Dynamic Nuclear Polarization.

Authors:  Vladimir K Michaelis; Ta-Chung Ong; Matthew K Kiesewetter; Derik K Frantz; Joseph J Walish; Enrico Ravera; Claudio Luchinat; Timothy M Swager; Robert G Griffin
Journal:  Isr J Chem       Date:  2014-02-13       Impact factor: 3.333

3.  Solid effect in magic angle spinning dynamic nuclear polarization.

Authors:  Björn Corzilius; Albert A Smith; Robert G Griffin
Journal:  J Chem Phys       Date:  2012-08-07       Impact factor: 3.488

Review 4.  Polarizing agents and mechanisms for high-field dynamic nuclear polarization of frozen dielectric solids.

Authors:  Kan-Nian Hu
Journal:  Solid State Nucl Magn Reson       Date:  2011-08-06       Impact factor: 2.293

5.  Observation of strongly forbidden solid effect dynamic nuclear polarization transitions via electron-electron double resonance detected NMR.

Authors:  Albert A Smith; Björn Corzilius; Olesya Haze; Timothy M Swager; Robert G Griffin
Journal:  J Chem Phys       Date:  2013-12-07       Impact factor: 3.488

6.  Second Harmonic 527-GHz Gyrotron for DNP-NMR: Design and Experimental Results.

Authors:  Sudheer K Jawla; Robert G Griffin; Ivan A Mastovsky; Michael A Shapiro; Richard J Temkin
Journal:  IEEE Trans Electron Devices       Date:  2019-12-10       Impact factor: 2.917

Review 7.  High frequency dynamic nuclear polarization: New directions for the 21st century.

Authors:  Robert G Griffin; Timothy M Swager; Richard J Temkin
Journal:  J Magn Reson       Date:  2019-07-12       Impact factor: 2.734

8.  Broadband terahertz-power extracting by using electron cyclotron maser.

Authors:  Shi Pan; Chao-Hai Du; Xiang-Bo Qi; Pu-Kun Liu
Journal:  Sci Rep       Date:  2017-08-04       Impact factor: 4.379

  8 in total

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