Literature DB >> 21201607

Dichlorido(4,7-diphenyl-1,10-phenanthroline-κN,N')gold(III) tetra-chloridoaurate(III).

Roya Ahmadi, Vahid Amani, Hamid Reza Khavasi.   

Abstract

In the cation of the title compound, [AuCl(2)(C(24)H(16)N(2))][AuCl(4)], the Au(III) atom is four-coordinated in a distorted square-planar configuration by two N atoms from a 4,7-diphenyl-1,10-phenanthroline ligand and two terminal Cl atoms. In the anion, the Au(III) atom has a square-planar coordination. In the crystal structure, intra- and inter-molecular C-H⋯Cl hydrogen bonds are found.

Entities:  

Year:  2008        PMID: 21201607      PMCID: PMC2960497          DOI: 10.1107/S1600536808025476

Source DB:  PubMed          Journal:  Acta Crystallogr Sect E Struct Rep Online        ISSN: 1600-5368


Related literature

For related literature, see: Hojjat Kashani et al. (2008 ▶); Mclnnes et al. (1995 ▶); Bjernemose et al. (2004 ▶); Hayoun et al. (2006 ▶); Abbate et al. (2000 ▶); Adams & Strahle (1982 ▶).

Experimental

Crystal data

[AuCl2(C24H16N2)][AuCl4] M = 939.03 Monoclinic, a = 26.2625 (16) Å b = 13.7608 (6) Å c = 14.4292 (9) Å β = 101.207 (5)° V = 5115.2 (5) Å3 Z = 8 Mo Kα radiation μ = 12.10 mm−1 T = 120 (2) K 0.43 × 0.35 × 0.30 mm

Data collection

Bruker SMART CCD area-detector diffractometer Absorption correction: numerical (X-SHAPE and X-RED; Stoe & Cie, 2005 ▶) T min = 0.580, T max = 0.640 18667 measured reflections 6864 independent reflections 6404 reflections with I > 2σ(I) R int = 0.090

Refinement

R[F 2 > 2σ(F 2)] = 0.068 wR(F 2) = 0.173 S = 1.16 6864 reflections 308 parameters H-atom parameters constrained Δρmax = 1.07 e Å−3 Δρmin = −1.02 e Å−3 Data collection: SMART (Bruker, 1998 ▶); cell refinement: SMART; data reduction: SAINT (Bruker, 1998 ▶); program(s) used to solve structure: SHELXTL (Sheldrick, 2008 ▶); program(s) used to refine structure: SHELXTL; molecular graphics: ORTEP-3 for Windows (Farrugia, 1997 ▶); software used to prepare material for publication: WinGX (Farrugia, 1999 ▶). Crystal structure: contains datablocks I, global. DOI: 10.1107/S1600536808025476/hk2509sup1.cif Structure factors: contains datablocks I. DOI: 10.1107/S1600536808025476/hk2509Isup2.hkl Additional supplementary materials: crystallographic information; 3D view; checkCIF report
[AuCl2(C24H16N2)][AuCl4]F000 = 3472
Mr = 939.03Dx = 2.439 Mg m3
Monoclinic, C2/cMo Kα radiation λ = 0.71073 Å
Hall symbol: -C 2ycCell parameters from 2231 reflections
a = 26.2625 (16) Åθ = 1.7–29.2º
b = 13.7608 (6) ŵ = 12.10 mm1
c = 14.4292 (9) ÅT = 120 (2) K
β = 101.207 (5)ºPrism, yellow
V = 5115.2 (5) Å30.43 × 0.35 × 0.30 mm
Z = 8
Bruker SMART CCD area-detector diffractometer6864 independent reflections
Radiation source: fine-focus sealed tube6404 reflections with I > 2σ(I)
Monochromator: graphiteRint = 0.090
T = 120(2) Kθmax = 29.2º
φ and ω scansθmin = 1.7º
Absorption correction: numericalshape of crystal determined optically (PROGRAM? Reference?)h = −35→35
Tmin = 0.580, Tmax = 0.640k = −18→18
18667 measured reflectionsl = −19→13
Refinement on F2Hydrogen site location: inferred from neighbouring sites
Least-squares matrix: fullH-atom parameters constrained
R[F2 > 2σ(F2)] = 0.068  w = 1/[σ2(Fo2) + (0.0977P)2 + 20.7667P] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.173(Δ/σ)max = 0.048
S = 1.16Δρmax = 1.07 e Å3
6864 reflectionsΔρmin = −1.02 e Å3
308 parametersExtinction correction: SHELXTL (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
Primary atom site location: structure-invariant direct methodsExtinction coefficient: 0.00055 (6)
Secondary atom site location: difference Fourier map
Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > 2sigma(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.
xyzUiso*/Ueq
Au10.097267 (11)−0.152249 (19)0.112685 (18)0.01435 (13)
Au20.165438 (12)0.96986 (2)0.854512 (18)0.01739 (13)
Cl10.12293 (8)−0.30783 (14)0.10295 (15)0.0240 (4)
Cl20.01813 (8)−0.20496 (16)0.12856 (16)0.0259 (4)
Cl30.21356 (9)1.10394 (18)0.83479 (15)0.0280 (4)
Cl40.23388 (10)0.87252 (19)0.84084 (16)0.0320 (5)
Cl50.11779 (10)0.83657 (16)0.87768 (15)0.0284 (5)
Cl60.09622 (8)1.06689 (16)0.86481 (15)0.0257 (4)
N10.0787 (3)−0.0088 (5)0.1182 (5)0.0160 (12)
N20.1667 (2)−0.0939 (5)0.1005 (4)0.0138 (11)
C10.0334 (3)0.0290 (6)0.1291 (6)0.0203 (15)
H10.0055−0.01170.13210.024*
C20.0279 (3)0.1283 (7)0.1359 (6)0.0193 (14)
H2−0.00410.15350.14220.023*
C30.0691 (3)0.1922 (6)0.1336 (5)0.0159 (13)
C40.0612 (3)0.2989 (6)0.1480 (5)0.0161 (13)
C50.0146 (4)0.3441 (6)0.1051 (6)0.0211 (16)
H5−0.01140.30900.06610.025*
C60.0082 (3)0.4422 (7)0.1221 (6)0.0239 (16)
H6−0.02220.47340.09370.029*
C70.0463 (4)0.4939 (6)0.1804 (6)0.0229 (16)
H70.04180.55990.18980.027*
C80.0914 (4)0.4485 (6)0.2254 (6)0.0243 (16)
H80.11670.48340.26600.029*
C90.0985 (4)0.3503 (5)0.2094 (6)0.0194 (15)
H90.12850.31910.24000.023*
C100.1156 (3)0.1527 (5)0.1165 (5)0.0127 (13)
C110.1599 (3)0.2079 (5)0.1012 (5)0.0146 (13)
H110.15770.27540.09980.018*
C120.2050 (3)0.1647 (5)0.0888 (6)0.0161 (13)
H120.23220.20290.07690.019*
C130.2106 (3)0.0604 (5)0.0940 (5)0.0125 (12)
C140.2567 (3)0.0094 (5)0.0877 (5)0.0139 (12)
C150.3067 (3)0.0582 (5)0.0815 (5)0.0133 (12)
C160.3258 (3)0.1344 (6)0.1443 (5)0.0178 (14)
H160.30660.15770.18740.021*
C170.3743 (3)0.1738 (6)0.1401 (6)0.0194 (14)
H170.38680.22540.17960.023*
C180.4039 (3)0.1381 (6)0.0787 (6)0.0202 (15)
H180.43660.16370.07820.024*
C190.3838 (3)0.0621 (6)0.0167 (5)0.0195 (14)
H190.40320.0384−0.02580.023*
C200.3364 (3)0.0230 (5)0.0182 (5)0.0146 (13)
H200.3236−0.0272−0.02300.018*
C210.2552 (3)−0.0924 (6)0.0870 (5)0.0160 (13)
H210.2849−0.12740.08230.019*
C220.2093 (3)−0.1420 (6)0.0935 (5)0.0170 (14)
H220.2089−0.20960.09290.020*
C230.1672 (3)0.0044 (5)0.1023 (4)0.0129 (13)
C240.1190 (3)0.0514 (5)0.1122 (5)0.0113 (12)
U11U22U33U12U13U23
Au10.01838 (19)0.01279 (17)0.01316 (17)−0.00363 (8)0.00622 (12)−0.00142 (9)
Au20.0225 (2)0.01961 (19)0.00978 (17)0.00323 (9)0.00248 (12)−0.00040 (9)
Cl10.0312 (9)0.0133 (8)0.0308 (9)−0.0030 (7)0.0144 (8)0.0002 (7)
Cl20.0258 (9)0.0216 (9)0.0340 (10)−0.0098 (7)0.0152 (8)−0.0046 (8)
Cl30.0315 (10)0.0319 (11)0.0216 (8)−0.0063 (8)0.0079 (8)0.0042 (8)
Cl40.0382 (12)0.0347 (11)0.0229 (9)0.0178 (10)0.0057 (9)−0.0016 (9)
Cl50.0424 (12)0.0248 (10)0.0176 (8)−0.0076 (8)0.0050 (8)−0.0014 (7)
Cl60.0248 (9)0.0259 (10)0.0272 (9)0.0051 (7)0.0066 (8)−0.0032 (8)
N10.023 (3)0.012 (3)0.016 (3)−0.002 (2)0.010 (2)0.002 (2)
N20.015 (3)0.016 (3)0.013 (2)−0.003 (2)0.007 (2)0.001 (2)
C10.022 (4)0.017 (4)0.024 (4)−0.005 (3)0.009 (3)−0.003 (3)
C20.012 (3)0.026 (4)0.022 (3)0.000 (3)0.008 (3)−0.003 (3)
C30.015 (3)0.016 (3)0.016 (3)0.003 (3)0.001 (3)0.004 (3)
C40.024 (3)0.014 (3)0.014 (3)0.004 (3)0.011 (3)−0.002 (3)
C50.027 (4)0.018 (4)0.018 (3)0.005 (3)0.007 (3)−0.003 (3)
C60.025 (4)0.027 (4)0.023 (4)0.014 (3)0.015 (3)0.004 (3)
C70.038 (5)0.016 (3)0.021 (3)0.001 (3)0.022 (3)−0.002 (3)
C80.031 (4)0.016 (3)0.025 (4)−0.003 (3)0.003 (3)−0.004 (3)
C90.030 (4)0.012 (3)0.016 (3)0.002 (3)0.002 (3)−0.001 (3)
C100.014 (3)0.014 (3)0.012 (3)−0.002 (2)0.007 (2)0.000 (2)
C110.016 (3)0.015 (3)0.015 (3)0.002 (2)0.006 (3)0.002 (3)
C120.015 (3)0.012 (3)0.022 (3)−0.006 (2)0.006 (3)0.002 (3)
C130.009 (3)0.015 (3)0.015 (3)−0.001 (2)0.006 (2)0.000 (3)
C140.018 (3)0.012 (3)0.012 (3)−0.002 (2)0.003 (3)−0.001 (2)
C150.007 (3)0.017 (3)0.015 (3)0.003 (2)0.001 (2)0.003 (3)
C160.016 (3)0.018 (3)0.017 (3)0.002 (3)−0.001 (3)0.002 (3)
C170.021 (4)0.015 (3)0.022 (3)−0.001 (3)0.006 (3)0.000 (3)
C180.019 (4)0.016 (3)0.026 (4)−0.001 (3)0.005 (3)−0.001 (3)
C190.019 (3)0.024 (4)0.016 (3)−0.001 (3)0.005 (3)−0.001 (3)
C200.018 (3)0.018 (3)0.010 (3)−0.001 (2)0.008 (3)−0.001 (2)
C210.017 (3)0.016 (3)0.018 (3)0.002 (2)0.009 (3)−0.001 (3)
C220.024 (4)0.016 (3)0.013 (3)0.004 (3)0.008 (3)0.002 (3)
C230.018 (3)0.017 (3)0.005 (3)0.003 (3)0.004 (2)−0.004 (3)
C240.015 (3)0.009 (3)0.011 (3)−0.006 (2)0.007 (2)0.001 (2)
Au1—N22.032 (6)C10—C111.442 (10)
Au1—N12.039 (7)C11—C121.367 (10)
Au1—Cl22.2546 (19)C11—H110.9300
Au1—Cl12.257 (2)C12—C131.444 (10)
Au2—Cl42.281 (2)C12—H120.9300
Au2—Cl52.281 (2)C13—C231.401 (9)
Au2—Cl62.284 (2)C13—C141.417 (10)
Au2—Cl32.285 (2)C14—C211.400 (10)
C1—N11.335 (10)C14—C151.494 (10)
C1—C21.379 (11)C15—C201.398 (9)
C1—H10.9300C15—C161.412 (11)
C2—C31.399 (10)C16—C171.395 (11)
C2—H20.9300C16—H160.9300
C3—C101.403 (10)C17—C181.378 (12)
C3—C41.502 (10)C17—H170.9300
C4—C91.381 (11)C18—C191.411 (11)
C4—C51.404 (11)C18—H180.9300
C5—C61.389 (11)C19—C201.361 (10)
C5—H50.9300C19—H190.9300
C6—C71.373 (14)C20—H200.9300
C6—H60.9300C21—C221.405 (11)
C7—C81.383 (13)C21—H210.9300
C7—H70.9300C22—N21.320 (10)
C8—C91.390 (11)C22—H220.9300
C8—H80.9300C23—N21.352 (9)
C9—H90.9300C23—C241.454 (9)
C10—C241.399 (9)C24—N11.359 (9)
N2—Au1—N181.1 (3)C11—C12—C13120.6 (7)
N2—Au1—Cl2175.42 (19)C11—C12—H12119.7
N1—Au1—Cl294.3 (2)C13—C12—H12119.7
N2—Au1—Cl194.92 (19)C23—C13—C14116.9 (7)
N1—Au1—Cl1175.95 (19)C23—C13—C12118.3 (6)
Cl2—Au1—Cl189.62 (8)C14—C13—C12124.8 (6)
Cl4—Au2—Cl590.26 (10)C21—C14—C13118.2 (7)
Cl4—Au2—Cl6178.77 (8)C21—C14—C15118.3 (7)
Cl5—Au2—Cl689.67 (9)C13—C14—C15123.5 (7)
Cl4—Au2—Cl389.96 (10)C20—C15—C16120.2 (7)
Cl5—Au2—Cl3178.75 (7)C20—C15—C14119.4 (7)
Cl6—Au2—Cl390.14 (9)C16—C15—C14120.2 (6)
N1—C1—C2120.1 (7)C17—C16—C15118.3 (7)
N1—C1—H1119.9C17—C16—H16120.8
C2—C1—H1119.9C15—C16—H16120.9
C1—C2—C3121.9 (7)C18—C17—C16121.5 (8)
C1—C2—H2119.0C18—C17—H17119.2
C3—C2—H2119.0C16—C17—H17119.2
C2—C3—C10117.7 (7)C17—C18—C19118.9 (8)
C2—C3—C4118.9 (7)C17—C18—H18120.6
C10—C3—C4123.5 (7)C19—C18—H18120.5
C9—C4—C5120.3 (7)C20—C19—C18120.9 (7)
C9—C4—C3119.3 (7)C20—C19—H19119.5
C5—C4—C3120.2 (7)C18—C19—H19119.6
C6—C5—C4118.5 (8)C19—C20—C15120.1 (7)
C6—C5—H5120.7C19—C20—H20119.9
C4—C5—H5120.8C15—C20—H20120.0
C7—C6—C5120.9 (8)C14—C21—C22120.7 (7)
C7—C6—H6119.6C14—C21—H21119.6
C5—C6—H6119.5C22—C21—H21119.7
C6—C7—C8120.6 (8)N2—C22—C21120.7 (7)
C6—C7—H7119.7N2—C22—H22119.7
C8—C7—H7119.7C21—C22—H22119.6
C7—C8—C9119.4 (8)N2—C23—C13123.6 (6)
C7—C8—H8120.3N2—C23—C24116.2 (6)
C9—C8—H8120.3C13—C23—C24120.2 (6)
C4—C9—C8120.2 (8)N1—C24—C10123.2 (7)
C4—C9—H9119.9N1—C24—C23116.0 (6)
C8—C9—H9119.9C10—C24—C23120.8 (6)
C24—C10—C3117.3 (7)C1—N1—C24119.5 (7)
C24—C10—C11117.3 (6)C1—N1—Au1127.4 (5)
C3—C10—C11125.4 (7)C24—N1—Au1113.1 (5)
C12—C11—C10122.4 (7)C22—N2—C23119.9 (6)
C12—C11—H11118.8C22—N2—Au1126.6 (5)
C10—C11—H11118.8C23—N2—Au1113.5 (5)
N1—C1—C2—C3−1.3 (13)C18—C19—C20—C150.2 (12)
C1—C2—C3—C105.0 (12)C16—C15—C20—C190.0 (11)
C1—C2—C3—C4−175.9 (8)C14—C15—C20—C19−175.1 (7)
C2—C3—C4—C9133.5 (8)C13—C14—C21—C22−0.7 (10)
C10—C3—C4—C9−47.4 (10)C15—C14—C21—C22179.4 (7)
C2—C3—C4—C5−41.7 (10)C14—C21—C22—N2−0.1 (11)
C10—C3—C4—C5137.4 (8)C14—C13—C23—N2−2.9 (10)
C9—C4—C5—C63.2 (12)C12—C13—C23—N2174.8 (7)
C3—C4—C5—C6178.3 (7)C14—C13—C23—C24178.0 (6)
C4—C5—C6—C7−0.7 (12)C12—C13—C23—C24−4.3 (10)
C5—C6—C7—C8−1.6 (13)C3—C10—C24—N13.9 (10)
C6—C7—C8—C91.5 (13)C11—C10—C24—N1−175.0 (6)
C5—C4—C9—C8−3.3 (12)C3—C10—C24—C23−175.0 (6)
C3—C4—C9—C8−178.5 (8)C11—C10—C24—C236.1 (10)
C7—C8—C9—C40.9 (13)N2—C23—C24—N1−0.2 (9)
C2—C3—C10—C24−6.1 (10)C13—C23—C24—N1179.0 (6)
C4—C3—C10—C24174.8 (7)N2—C23—C24—C10178.9 (6)
C2—C3—C10—C11172.7 (7)C13—C23—C24—C10−2.0 (10)
C4—C3—C10—C11−6.4 (11)C2—C1—N1—C24−1.2 (12)
C24—C10—C11—C12−4.0 (11)C2—C1—N1—Au1176.9 (6)
C3—C10—C11—C12177.2 (7)C10—C24—N1—C1−0.2 (11)
C10—C11—C12—C13−2.3 (11)C23—C24—N1—C1178.8 (7)
C11—C12—C13—C236.5 (11)C10—C24—N1—Au1−178.6 (5)
C11—C12—C13—C14−176.1 (7)C23—C24—N1—Au10.4 (7)
C23—C13—C14—C212.1 (10)N2—Au1—N1—C1−178.6 (7)
C12—C13—C14—C21−175.4 (7)Cl2—Au1—N1—C10.7 (7)
C23—C13—C14—C15−178.1 (6)N2—Au1—N1—C24−0.4 (5)
C12—C13—C14—C154.4 (11)Cl2—Au1—N1—C24179.0 (5)
C21—C14—C15—C2042.6 (10)C21—C22—N2—C23−0.6 (10)
C13—C14—C15—C20−137.3 (7)C21—C22—N2—Au1−178.9 (5)
C21—C14—C15—C16−132.5 (7)C13—C23—N2—C222.2 (10)
C13—C14—C15—C1647.7 (10)C24—C23—N2—C22−178.7 (6)
C20—C15—C16—C171.0 (11)C13—C23—N2—Au1−179.3 (5)
C14—C15—C16—C17176.0 (7)C24—C23—N2—Au1−0.2 (7)
C15—C16—C17—C18−2.1 (12)N1—Au1—N2—C22178.7 (6)
C16—C17—C18—C192.2 (13)N1—Au1—N2—C230.3 (5)
C17—C18—C19—C20−1.2 (12)Cl1—Au1—N2—C23179.4 (4)
D—H···AD—HH···AD···AD—H···A
C1—H1···Cl20.932.683.244 (9)120
C1—H1···Cl6i0.932.793.668 (8)159
C18—H18···Cl2ii0.932.793.653 (8)155
C22—H22···Cl10.932.663.239 (8)121
C22—H22···Cl4iii0.932.763.555 (9)143
Au1—N22.032 (6)
Au1—N12.039 (7)
Au1—Cl22.2546 (19)
Au1—Cl12.257 (2)
Au2—Cl42.281 (2)
Au2—Cl52.281 (2)
Au2—Cl62.284 (2)
Au2—Cl32.285 (2)
N2—Au1—N181.1 (3)
N2—Au1—Cl2175.42 (19)
N1—Au1—Cl294.3 (2)
N2—Au1—Cl194.92 (19)
N1—Au1—Cl1175.95 (19)
Cl2—Au1—Cl189.62 (8)
Cl4—Au2—Cl590.26 (10)
Cl4—Au2—Cl6178.77 (8)
Cl5—Au2—Cl689.67 (9)
Cl4—Au2—Cl389.96 (10)
Cl5—Au2—Cl3178.75 (7)
Cl6—Au2—Cl390.14 (9)
Table 2

Hydrogen-bond geometry (Å, °)

D—H⋯AD—HH⋯ADAD—H⋯A
C1—H1⋯Cl20.932.683.244 (9)120
C1—H1⋯Cl6i0.932.793.668 (8)159
C18—H18⋯Cl2ii0.932.793.653 (8)155
C22—H22⋯Cl10.932.663.239 (8)121
C22—H22⋯Cl4iii0.932.763.555 (9)143

Symmetry codes: (i) ; (ii) ; (iii) .

  3 in total

1.  A short history of SHELX.

Authors:  George M Sheldrick
Journal:  Acta Crystallogr A       Date:  2007-12-21       Impact factor: 2.290

2.  Gold(III) and platinum(II) polypyridyl double salts and a general metathesis route to metallophilic interactions.

Authors:  Rebecca Hayoun; Diane K Zhong; Arnold L Rheingold; Linda H Doerrer
Journal:  Inorg Chem       Date:  2006-08-07       Impact factor: 5.165

3.  1,4,10,13-Tetra-oxa-7,16-diazo-niacyclo-octadecane bis-[tetra-chloridoaurate(III)] dihydrate.

Authors:  Leila Hojjat Kashani; Mohammad Yousefi; Vahid Amani; Hamid Reza Khavasi
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2008-05-24
  3 in total
  4 in total

1.  (4,7-Diphenyl-1,10-phenanthroline-κN,N')diiodidomercury(II).

Authors:  Mohammad Yousefi; Rabin Rashidi Vahid; Vahid Amani; Mansour Arab Chamjangali; Hamid Reza Khavasi
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2008-09-27

2.  Bis[dichlorido(5,5'-dimethyl-2,2'-bi-pyridine-κN,N')gold(III)] tetra-chlorido-aurate(III) dichloridooaurate(I).

Authors:  Selvi Karaca; Mehmet Akkurt; Nasser Safari; Vahid Amani; Orhan Büyükgüngör; Anita Abedi
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2009-02-28

3.  Bis(2,6-dimethyl-pyridine-κN)gold(I) tetra-chloridoaurate(III).

Authors:  Roya Ahmadi; Leila Dehghan; Vahid Amani; Hamid Reza Khavasi
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2008-09-06

4.  Di-μ-bromido-bis-[bromido(4,7-diphenyl-1,10-phenanthroline-κ(2) N,N')cadmium].

Authors:  Sadif A Shirvan; Sara Haydari Dezfuli; Fereydoon Khazali; Manouchehr Aghajeri; Ali Borsalani
Journal:  Acta Crystallogr Sect E Struct Rep Online       Date:  2012-11-10
  4 in total

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