Literature DB >> 20848020

Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding.

Kotaro Fujii1, Ana Lazuen Garay, Janeen Hill, Elena Sbircea, Zhigang Pan, Mingcan Xu, David C Apperley, Stuart L James, Kenneth D M Harris.   

Abstract

Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal-organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.

Entities:  

Year:  2010        PMID： 20848020     DOI： 10.1039/c0cc02635b

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  8 in total

1.  Real-time and in situ monitoring of mechanochemical milling reactions.

Authors:  Tomislav Friščić; Ivan Halasz; Patrick J Beldon; Ana M Belenguer; Frank Adams; Simon A J Kimber; Veijo Honkimäki; Robert E Dinnebier
Journal:  Nat Chem       Date:  2012-12-02       Impact factor: 24.427

2.  Mechanochemical synthesis: how grinding evolves.

Authors:  Kenneth D M Harris
Journal:  Nat Chem       Date:  2013-01       Impact factor: 24.427

3.  Ab initio random structure searching of organic molecular solids: assessment and validation against experimental data.

Authors:  Miri Zilka; Dmytro V Dudenko; Colan E Hughes; P Andrew Williams; Simone Sturniolo; W Trent Franks; Chris J Pickard; Jonathan R Yates; Kenneth D M Harris; Steven P Brown
Journal:  Phys Chem Chem Phys       Date:  2017-10-04       Impact factor: 3.676

4.  Determination of a complex crystal structure in the absence of single crystals: analysis of powder X-ray diffraction data, guided by solid-state NMR and periodic DFT calculations, reveals a new 2'-deoxyguanosine structural motif.

Authors:  Colan E Hughes; G N Manjunatha Reddy; Stefano Masiero; Steven P Brown; P Andrew Williams; Kenneth D M Harris
Journal:  Chem Sci       Date:  2017-03-16       Impact factor: 9.825

Review 5.  Advances in Solid-State Transformations of Coordination Bonds: From the Ball Mill to the Aging Chamber.

Authors:  Cristina Mottillo; Tomislav Friščić
Journal:  Molecules       Date:  2017-01-17       Impact factor: 4.411

6.  Phenomenological Inferences on the Kinetics of a Mechanically Activated Knoevenagel Condensation: Understanding the "Snowball" Kinetic Effect in Ball Milling.

Authors:  Maria Carta; Stuart L James; Francesco Delogu
Journal:  Molecules       Date:  2019-10-07       Impact factor: 4.411

7.  Solid-State Structural Properties of Alloxazine Determined from Powder XRD Data in Conjunction with DFT-D Calculations and Solid-State NMR Spectroscopy: Unraveling the Tautomeric Identity and Pathways for Tautomeric Interconversion.

Authors:  Christopher J H Smalley; Andrew J Logsdail; Colan E Hughes; Dinu Iuga; Mark T Young; Kenneth D M Harris
Journal:  Cryst Growth Des       Date:  2021-11-22       Impact factor: 4.076

Review 8.  A Comprehensive Review of Metal-Organic Framework: Synthesis, Characterization, and Investigation of Their Application in Electrochemical Biosensors for Biomedical Analysis.

Authors:  Zahra Dourandish; Somayeh Tajik; Hadi Beitollahi; Peyman Mohammadzadeh Jahani; Fariba Garkani Nejad; Iran Sheikhshoaie; Antonio Di Bartolomeo
Journal:  Sensors (Basel)       Date:  2022-03-14       Impact factor: 3.576
  8 in total

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