Literature DB >> 20820530

A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation.

Manza B J Atkinson1, Ivan Halasz, Dejan-Krešimir Bučar, Robert E Dinnebier, S V Santhana Mariappan, Anatoliy N Sokolov, Leonard R MacGillivray.   

Abstract

A bicyclobutyl that bears six carboxylic acid groups results from a trimerisation of a diene diacid in the solid state. Powder X-ray diffraction and a co-crystallisation are used to solve the structure of the diene and elucidate the stereochemistry of the bicyclobutyl, respectively.

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Year:  2010        PMID： 20820530     DOI： 10.1039/c0cc02204g

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  3 in total

1.  Crystal engineering rescues a solution organic synthesis in a cocrystallization that confirms the configuration of a molecular ladder.

Authors:  Manza B J Atkinson; S V Santhana Mariappan; Dejan-Krešimir Bučar; Jonas Baltrusaitis; Tomislav Friščić; Naif G Sinada; Leonard R MacGillivray
Journal:  Proc Natl Acad Sci U S A       Date:  2011-06-20       Impact factor: 11.205

2.  A multistep single-crystal-to-single-crystal bromodiacetylene dimerization.

Authors:  Tobias N Hoheisel; Stephen Schrettl; Roman Marty; Tanya K Todorova; Clémence Corminboeuf; Andrzej Sienkiewicz; Rosario Scopelliti; W Bernd Schweizer; Holger Frauenrath
Journal:  Nat Chem       Date:  2013-02-24       Impact factor: 24.427

3.  A biorenewable cyclobutane-containing building block synthesized from sorbic acid using photoenergy.

Authors:  Micah Mabin; Quintin Elliott; Zhihan Wang; Angel Ugrinov; Qianli R Chu
Journal:  iScience       Date:  2022-08-27
  3 in total

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