Literature DB >> 20680210

Potassium carbonate-silica: a highly effective stationary phase for the chromatographic removal of organotin impurities.

David C Harrowven1, Dennis P Curran, Sarah L Kostiuk, Ian L Wallis-Guy, Sally Whiting, Kerri J Stenning, Bencan Tang, Emma Packard, Lana Nanson.   

Abstract

Organotin impurities in product mixtures can be reduced from stoichiometric levels to approximately 15 parts per million by column chromatography using 10% w/w anhydrous potassium carbonate-silica as a stationary phase.

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Year:  2010        PMID： 20680210     DOI： 10.1039/c0cc01328e

Source DB:  PubMed          Journal:  Chem Commun (Camb)        ISSN： 1359-7345            Impact factor:   6.222


  10 in total

1.  Synthesis of 6-substituted 1-oxoindanoyl isoleucine conjugates and modeling studies with the COI1-JAZ co-receptor complex of lima bean.

Authors:  Yoko Nakamura; Christian Paetz; Wolfgang Brandt; Anja David; Martha Rendón-Anaya; Alfredo Herrera-Estrella; Axel Mithöfer; Wilhelm Boland
Journal:  J Chem Ecol       Date:  2014-07-10       Impact factor: 2.626

2.  Chemoselectivity in the Kosugi-Migita-Stille coupling of bromophenyl triflates and bromo-nitrophenyl triflates with (ethenyl)tributyltin.

Authors:  Nurul N Ansari; Matthew M Cummings; Björn C G Söderberg
Journal:  Tetrahedron       Date:  2018-04-10       Impact factor: 2.457

3.  Copper-Catalyzed Stille Cross-Coupling Reaction and Application in the Synthesis of the Spliceostatin Core Structure.

Authors:  Arun K Ghosh; Joshua R Born; Anne M Veitschegger; Melissa S Jurica
Journal:  J Org Chem       Date:  2020-06-09       Impact factor: 4.354

4.  Electrophilic Activation of [1.1.1]Propellane for the Synthesis of Nitrogen-Substituted Bicyclo[1.1.1]pentanes.

Authors:  Sarah Livesley; Alistair J Sterling; Craig M Robertson; William R F Goundry; James A Morris; Fernanda Duarte; Christophe Aïssa
Journal:  Angew Chem Int Ed Engl       Date:  2021-11-26       Impact factor: 16.823

5.  Synthesis and Characterization of a Specific Iodine-125-Labeled TRPC5 Radioligand.

Authors:  Yanbo Yu; Qianwa Liang; Lixia Du; Hao Jiang; Jiwei Gu; Hongzhen Hu; Zhude Tu
Journal:  ChemMedChem       Date:  2020-09-02       Impact factor: 3.540

6.  Concise synthesis of the A/BCD-ring fragment of gambieric acid A.

Authors:  Haruhiko Fuwa; Ryo Fukazawa; Makoto Sasaki
Journal:  Front Chem       Date:  2015-01-13       Impact factor: 5.221

7.  Blue-to-Green Emitting Neutral Ir(III) Complexes Bearing Pentafluorosulfanyl Groups: A Combined Experimental and Theoretical Study.

Authors:  Amlan K Pal; Adam F Henwood; David B Cordes; Alexandra M Z Slawin; Ifor D W Samuel; Eli Zysman-Colman
Journal:  Inorg Chem       Date:  2017-06-14       Impact factor: 5.165

8.  Synthesis of 19-substituted geldanamycins with altered conformations and their binding to heat shock protein Hsp90.

Authors:  Russell R A Kitson; Chuan-Hsin Chang; Rui Xiong; Huw E L Williams; Adrienne L Davis; William Lewis; Donna L Dehn; David Siegel; S Mark Roe; Chrisostomos Prodromou; David Ross; Christopher J Moody
Journal:  Nat Chem       Date:  2013-03-10       Impact factor: 24.427

9.  An improved route to 19-substituted geldanamycins as novel Hsp90 inhibitors--potential therapeutics in cancer and neurodegeneration.

Authors:  Russell R A Kitson; Christopher J Moody
Journal:  Chem Commun (Camb)       Date:  2013-10-04       Impact factor: 6.222

10.  Synthesis, Properties, and Light-Emitting Electrochemical Cell (LEEC) Device Fabrication of Cationic Ir(III) Complexes Bearing Electron-Withdrawing Groups on the Cyclometallating Ligands.

Authors:  Amlan K Pal; David B Cordes; Alexandra M Z Slawin; Cristina Momblona; Enrique Ortı; Ifor D W Samuel; Henk J Bolink; Eli Zysman-Colman
Journal:  Inorg Chem       Date:  2016-09-28       Impact factor: 5.165
  10 in total

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