Literature DB >> 20595926

Optimization of protein crosslinking formulations for the treatment of degenerative disc disease.

Paul Slusarewicz1, Keng Zhu, Bryan Kirking, Justin Toungate, Tom Hedman.   

Abstract

STUDY
DESIGN: Biochemical studies aimed at optimization of protein crosslinking formulations for the treatment of degenerative disc disease and subsequent biomechanical testing of tissues treated with these formulations.
OBJECTIVE: To optimize protein crosslinking formulations for treatment of degenerating spinal discs. SUMMARY OF BACKGROUND DATA: Nonsurgical exogenous crosslinking therapy is a potential new, noninvasive technology for the treatment of degenerative disc disease. The technology is based on the injection of protein crosslinking reagents into the pathologic disc to restore its mechanical properties and also to potentially increase the permeability of the tissue and so facilitate the exchange of waste products and nutrients.
METHODS: Diffusion of genipin (GP) was monitored following injection into spinal discs and the effects of surfactants on diffusion studied. Formulations for GP and methylglyoxal (MG) were biochemically optimized and used to treat bovine spinal discs. Their effects on bovine anulus tissue were evaluated using a circumferential tensile test, while the GP formulation was also tested with respect to its ability to reduce disc bulge under load.
RESULTS: GP exhibited a distinct time-dependent diffusion and sodium-dodecyl-sulfate, but not Tween-20, enhanced diffusion by 30%. Two crosslinkers, GP and MG, were inhibited by amines but enhanced by phosphate ions. Both formulations could enhance a number of physical parameters of bovine anulus tissue, while the GP formulation could reduce disc bulge following injections into spinal discs.
CONCLUSION: Formulations lacking amines and containing phosphate ions appear to be promising candidates for clinical use of the crosslinkers GP and MG.

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Year:  2011        PMID: 20595926      PMCID: PMC2951499          DOI: 10.1097/BRS.0b013e3181cc3de9

Source DB:  PubMed          Journal:  Spine (Phila Pa 1976)        ISSN: 0362-2436            Impact factor:   3.468


  38 in total

1.  Control of pH alters the type of cross-linking produced by 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide (EDC) treatment of acellular matrix vascular grafts.

Authors:  P F Gratzer; J M Lee
Journal:  J Biomed Mater Res       Date:  2001

2.  Crosslinking by advanced glycation end products increases the stiffness of the collagen network in human articular cartilage: a possible mechanism through which age is a risk factor for osteoarthritis.

Authors:  Nicole Verzijl; Jeroen DeGroot; Zaken Chaya Ben; Orit Brau-Benjamin; Alice Maroudas; Ruud A Bank; Joe Mizrahi; Casper G Schalkwijk; Suzanne R Thorpe; John W Baynes; Johannes W J Bijlsma; Floris P J G Lafeber; Johan M TeKoppele
Journal:  Arthritis Rheum       Date:  2002-01

Review 3.  Protein glycation, diabetes, and aging.

Authors:  P Ulrich; A Cerami
Journal:  Recent Prog Horm Res       Date:  2001

4.  The anisotropic hydraulic permeability of human lumbar anulus fibrosus. Influence of age, degeneration, direction, and water content.

Authors:  W Y Gu; X G Mao; R J Foster; M Weidenbaum; V C Mow; B A Rawlins
Journal:  Spine (Phila Pa 1976)       Date:  1999-12-01       Impact factor: 3.468

5.  Fixation of biological tissues with a naturally occurring crosslinking agent: fixation rate and effects of pH, temperature, and initial fixative concentration.

Authors:  H W Sung; Y Chang; I L Liang; W H Chang; Y C Chen
Journal:  J Biomed Mater Res       Date:  2000-10

6.  Methylglyoxal, an endogenous aldehyde, crosslinks DNA polymerase and the substrate DNA.

Authors:  N Murata-Kamiya; H Kamiya
Journal:  Nucleic Acids Res       Date:  2001-08-15       Impact factor: 16.971

7.  Stability of a biological tissue fixed with a naturally occurring crosslinking agent (genipin).

Authors:  H W Sung; I L Liang; C N Chen; R N Huang; H F Liang
Journal:  J Biomed Mater Res       Date:  2001-06-15

Review 8.  Gene therapy for degenerative disc disease.

Authors:  S Sobajima; J S Kim; L G Gilbertson; J D Kang
Journal:  Gene Ther       Date:  2004-02       Impact factor: 5.250

9.  Proanthocyanidin: a natural crosslinking reagent for stabilizing collagen matrices.

Authors:  Bo Han; Jason Jaurequi; Bao Wei Tang; Marcel E Nimni
Journal:  J Biomed Mater Res A       Date:  2003-04-01       Impact factor: 4.396

10.  Glutaraldehyde and oxidised dextran as crosslinker reagents for chitosan-based scaffolds for cartilage tissue engineering.

Authors:  B Hoffmann; D Seitz; A Mencke; A Kokott; G Ziegler
Journal:  J Mater Sci Mater Med       Date:  2009-03-04       Impact factor: 3.896

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  6 in total

1.  Evaluation of genipin for stabilization of decellularized porcine cartilage.

Authors:  Steven Elder; Amanda Pinheiro; Christian Young; Preston Smith; Emily Wright
Journal:  J Orthop Res       Date:  2017-03-24       Impact factor: 3.494

2.  Thermal analysis reveals differential effects of various crosslinkers on bovine annulus fibrosis.

Authors:  Keng Zhu; Paul Slusarewicz; Tom Hedman
Journal:  J Orthop Res       Date:  2011-01       Impact factor: 3.494

3.  Changes in the interfacial shear resistance of disc annulus fibrosus from genipin crosslinking.

Authors:  Bryan Kirking; Thomas Hedman; John Criscione
Journal:  J Biomech       Date:  2013-10-29       Impact factor: 2.712

4.  Feasibility of the annulus fibrosus repair with in situ gelating hydrogels - A biomechanical study.

Authors:  Anne-Gita Scheibler; Tobias Götschi; Jonas Widmer; Claude Holenstein; Thomas Steffen; Roland S Camenzind; Jess G Snedeker; Mazda Farshad
Journal:  PLoS One       Date:  2018-12-06       Impact factor: 3.240

Review 5.  Advanced Strategies for the Regeneration of Lumbar Disc Annulus Fibrosus.

Authors:  Javad Tavakoli; Ashish D Diwan; Joanne L Tipper
Journal:  Int J Mol Sci       Date:  2020-07-10       Impact factor: 5.923

6.  Soft Palate Modification Using a Collagen Crosslinking Reagent for Equine Dorsal Displacement of the Soft Palate and Other Upper Airway Breathing Disorders.

Authors:  Stephanie Hunt; Jonathan Kuo; Fabio A Aristizabal; Matt Brown; Abhijit Patwardhan; Thomas Hedman
Journal:  Int J Biomater       Date:  2019-04-01
  6 in total

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